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RU2007104471A - METHOD FOR PRODUCING 3,4-FULLERO [60] TETRAHYDROTHIOPHEN-1-OH - Google Patents

METHOD FOR PRODUCING 3,4-FULLERO [60] TETRAHYDROTHIOPHEN-1-OH Download PDF

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Publication number
RU2007104471A
RU2007104471A RU2007104471/04A RU2007104471A RU2007104471A RU 2007104471 A RU2007104471 A RU 2007104471A RU 2007104471/04 A RU2007104471/04 A RU 2007104471/04A RU 2007104471 A RU2007104471 A RU 2007104471A RU 2007104471 A RU2007104471 A RU 2007104471A
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RU
Russia
Prior art keywords
fullero
tetrahydrothiophen
producing
zrcl
dimethyl sulfoxide
Prior art date
Application number
RU2007104471/04A
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Russian (ru)
Other versions
RU2342381C2 (en
Inventor
Усеин Меметович Джемилев (RU)
Усеин Меметович Джемилев
Айрат Рамилевич Туктаров (RU)
Айрат Рамилевич Туктаров
Галина Аркадьевна Джемилева (RU)
Галина Аркадьевна Джемилева
Асхат Габдрахманович Ибрагимов (RU)
Асхат Габдрахманович Ибрагимов
Марко Пудас (FI)
Марко Пудас
Original Assignee
Институт нефтехимии и катализа РАН (RU)
Институт нефтехимии и катализа РАН
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Priority to RU2007104471/04A priority Critical patent/RU2342381C2/en
Publication of RU2007104471A publication Critical patent/RU2007104471A/en
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Publication of RU2342381C2 publication Critical patent/RU2342381C2/en

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  • Heterocyclic Carbon Compounds Containing A Hetero Ring Having Oxygen Or Sulfur (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Claims (1)

Способ получения 3,4-фуллеро[60]тетрагидротиофен-1-она (1),The method of obtaining 3,4-fullero [60] tetrahydrothiophen-1-one (1),
Figure 00000001
Figure 00000001
 путем взаимодействия фуллерена С60 с диметилсульфоксидом в присутствии катализатора цирконацендихлорида Cp2ZrCl2, взятыми в мольном соотношении С60: диметилсульфоксид: Cp2ZrCl2 = 0,01:(0,045-0,055):(0,0015-0,0025), в среде толуола, при комнатной температуре (~20°С) в течение 66-78 ч.by the interaction of fullerene C 60 with dimethyl sulfoxide in the presence of a catalyst of zirconacene dichloride Cp 2 ZrCl 2 taken in a molar ratio of C 60 : dimethyl sulfoxide: Cp 2 ZrCl 2 = 0.01: (0.045-0.055) :( 0.0015-0.0025), in toluene, at room temperature (~ 20 ° C) for 66-78 hours
RU2007104471/04A 2007-02-05 2007-02-05 Method of obtaining 3,4-fullero[60]tetrahydrothiophen-1-on RU2342381C2 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
RU2007104471/04A RU2342381C2 (en) 2007-02-05 2007-02-05 Method of obtaining 3,4-fullero[60]tetrahydrothiophen-1-on

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
RU2007104471/04A RU2342381C2 (en) 2007-02-05 2007-02-05 Method of obtaining 3,4-fullero[60]tetrahydrothiophen-1-on

Publications (2)

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RU2007104471A true RU2007104471A (en) 2008-08-10
RU2342381C2 RU2342381C2 (en) 2008-12-27

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Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5372798A (en) * 1994-03-08 1994-12-13 Exxon Research And Engineering Company Fullerene compositions and preparation
RU2188154C2 (en) * 2000-07-14 2002-08-27 Институт нефтехимии и катализа АН РБ и УНЦ РАН Method of synthesis of fullerene[60] sulfoxides
RU2191182C1 (en) * 2001-05-14 2002-10-20 Институт нефтехимии и катализа АН РБ и УНЦ РАН METHOD OF SYNTHESIS OF 2,3-FULLERENO[60]-2,3,4,7-TETRA-HYDRO-1H-λ6-THIEPINE-1,1-DIOXIDE

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Effective date: 20090206