RU2006112353A - Способ очистки газов, полученных из установки газификации - Google Patents
Способ очистки газов, полученных из установки газификации Download PDFInfo
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- RU2006112353A RU2006112353A RU2006112353/15A RU2006112353A RU2006112353A RU 2006112353 A RU2006112353 A RU 2006112353A RU 2006112353/15 A RU2006112353/15 A RU 2006112353/15A RU 2006112353 A RU2006112353 A RU 2006112353A RU 2006112353 A RU2006112353 A RU 2006112353A
- Authority
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- Russia
- Prior art keywords
- steam
- gas
- stream
- gasification
- carrier
- Prior art date
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- 239000007789 gas Substances 0.000 title claims 12
- 238000000034 method Methods 0.000 title claims 11
- 238000002309 gasification Methods 0.000 title claims 6
- 238000004140 cleaning Methods 0.000 title 1
- 239000002594 sorbent Substances 0.000 claims 10
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 claims 7
- 229910052717 sulfur Inorganic materials 0.000 claims 7
- 239000011593 sulfur Substances 0.000 claims 7
- 239000007787 solid Substances 0.000 claims 6
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 claims 4
- 230000015572 biosynthetic process Effects 0.000 claims 4
- 238000003786 synthesis reaction Methods 0.000 claims 4
- RWSOTUBLDIXVET-UHFFFAOYSA-N Dihydrogen sulfide Chemical compound S RWSOTUBLDIXVET-UHFFFAOYSA-N 0.000 claims 3
- 238000006243 chemical reaction Methods 0.000 claims 3
- 150000001875 compounds Chemical class 0.000 claims 3
- 229910000037 hydrogen sulfide Inorganic materials 0.000 claims 3
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 claims 2
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 claims 2
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 claims 2
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims 2
- XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical group [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 claims 2
- 229910052791 calcium Inorganic materials 0.000 claims 2
- 239000011575 calcium Substances 0.000 claims 2
- 229910002091 carbon monoxide Inorganic materials 0.000 claims 2
- 229910052736 halogen Inorganic materials 0.000 claims 2
- 150000002367 halogens Chemical class 0.000 claims 2
- 229910052759 nickel Inorganic materials 0.000 claims 2
- 230000008929 regeneration Effects 0.000 claims 2
- 238000011069 regeneration method Methods 0.000 claims 2
- 229910001887 tin oxide Inorganic materials 0.000 claims 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims 2
- 229910021532 Calcite Inorganic materials 0.000 claims 1
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical group [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 claims 1
- ZOKXTWBITQBERF-UHFFFAOYSA-N Molybdenum Chemical compound [Mo] ZOKXTWBITQBERF-UHFFFAOYSA-N 0.000 claims 1
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 claims 1
- 229910002092 carbon dioxide Inorganic materials 0.000 claims 1
- 239000001569 carbon dioxide Substances 0.000 claims 1
- 239000003054 catalyst Substances 0.000 claims 1
- 230000003197 catalytic effect Effects 0.000 claims 1
- 229910017052 cobalt Inorganic materials 0.000 claims 1
- 239000010941 cobalt Substances 0.000 claims 1
- GUTLYIVDDKVIGB-UHFFFAOYSA-N cobalt atom Chemical compound [Co] GUTLYIVDDKVIGB-UHFFFAOYSA-N 0.000 claims 1
- 229910052802 copper Inorganic materials 0.000 claims 1
- 239000010949 copper Substances 0.000 claims 1
- 229910000514 dolomite Inorganic materials 0.000 claims 1
- 239000010459 dolomite Substances 0.000 claims 1
- 239000000428 dust Substances 0.000 claims 1
- 229910052739 hydrogen Inorganic materials 0.000 claims 1
- 150000002431 hydrogen Chemical class 0.000 claims 1
- 239000001257 hydrogen Substances 0.000 claims 1
- 229910052751 metal Inorganic materials 0.000 claims 1
- 239000002184 metal Substances 0.000 claims 1
- 229910052750 molybdenum Inorganic materials 0.000 claims 1
- 239000011733 molybdenum Substances 0.000 claims 1
- 238000000746 purification Methods 0.000 claims 1
- 150000004760 silicates Chemical class 0.000 claims 1
- XOLBLPGZBRYERU-UHFFFAOYSA-N tin dioxide Chemical compound O=[Sn]=O XOLBLPGZBRYERU-UHFFFAOYSA-N 0.000 claims 1
- QHGNHLZPVBIIPX-UHFFFAOYSA-N tin(ii) oxide Chemical class [Sn]=O QHGNHLZPVBIIPX-UHFFFAOYSA-N 0.000 claims 1
- 239000004408 titanium dioxide Substances 0.000 claims 1
- 239000011787 zinc oxide Substances 0.000 claims 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10K—PURIFYING OR MODIFYING THE CHEMICAL COMPOSITION OF COMBUSTIBLE GASES CONTAINING CARBON MONOXIDE
- C10K1/00—Purifying combustible gases containing carbon monoxide
- C10K1/20—Purifying combustible gases containing carbon monoxide by treating with solids; Regenerating spent purifying masses
- C10K1/26—Regeneration of the purifying material contains also apparatus for the regeneration of the purifying material
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/34—Chemical or biological purification of waste gases
- B01D53/46—Removing components of defined structure
- B01D53/48—Sulfur compounds
- B01D53/50—Sulfur oxides
- B01D53/508—Sulfur oxides by treating the gases with solids
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/34—Chemical or biological purification of waste gases
- B01D53/46—Removing components of defined structure
- B01D53/68—Halogens or halogen compounds
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10J—PRODUCTION OF PRODUCER GAS, WATER-GAS, SYNTHESIS GAS FROM SOLID CARBONACEOUS MATERIAL, OR MIXTURES CONTAINING THESE GASES; CARBURETTING AIR OR OTHER GASES
- C10J3/00—Production of combustible gases containing carbon monoxide from solid carbonaceous fuels
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10J—PRODUCTION OF PRODUCER GAS, WATER-GAS, SYNTHESIS GAS FROM SOLID CARBONACEOUS MATERIAL, OR MIXTURES CONTAINING THESE GASES; CARBURETTING AIR OR OTHER GASES
- C10J3/00—Production of combustible gases containing carbon monoxide from solid carbonaceous fuels
- C10J3/02—Fixed-bed gasification of lump fuel
- C10J3/06—Continuous processes
- C10J3/14—Continuous processes using gaseous heat-carriers
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10J—PRODUCTION OF PRODUCER GAS, WATER-GAS, SYNTHESIS GAS FROM SOLID CARBONACEOUS MATERIAL, OR MIXTURES CONTAINING THESE GASES; CARBURETTING AIR OR OTHER GASES
- C10J3/00—Production of combustible gases containing carbon monoxide from solid carbonaceous fuels
- C10J3/72—Other features
- C10J3/82—Gas withdrawal means
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10K—PURIFYING OR MODIFYING THE CHEMICAL COMPOSITION OF COMBUSTIBLE GASES CONTAINING CARBON MONOXIDE
- C10K3/00—Modifying the chemical composition of combustible gases containing carbon monoxide to produce an improved fuel, e.g. one of different calorific value, which may be free from carbon monoxide
- C10K3/02—Modifying the chemical composition of combustible gases containing carbon monoxide to produce an improved fuel, e.g. one of different calorific value, which may be free from carbon monoxide by catalytic treatment
- C10K3/04—Modifying the chemical composition of combustible gases containing carbon monoxide to produce an improved fuel, e.g. one of different calorific value, which may be free from carbon monoxide by catalytic treatment reducing the carbon monoxide content, e.g. water-gas shift [WGS]
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10J—PRODUCTION OF PRODUCER GAS, WATER-GAS, SYNTHESIS GAS FROM SOLID CARBONACEOUS MATERIAL, OR MIXTURES CONTAINING THESE GASES; CARBURETTING AIR OR OTHER GASES
- C10J2300/00—Details of gasification processes
- C10J2300/09—Details of the feed, e.g. feeding of spent catalyst, inert gas or halogens
- C10J2300/0953—Gasifying agents
- C10J2300/0973—Water
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10J—PRODUCTION OF PRODUCER GAS, WATER-GAS, SYNTHESIS GAS FROM SOLID CARBONACEOUS MATERIAL, OR MIXTURES CONTAINING THESE GASES; CARBURETTING AIR OR OTHER GASES
- C10J2300/00—Details of gasification processes
- C10J2300/09—Details of the feed, e.g. feeding of spent catalyst, inert gas or halogens
- C10J2300/0983—Additives
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E20/00—Combustion technologies with mitigation potential
- Y02E20/16—Combined cycle power plant [CCPP], or combined cycle gas turbine [CCGT]
- Y02E20/18—Integrated gasification combined cycle [IGCC], e.g. combined with carbon capture and storage [CCS]
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Combustion & Propulsion (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Biomedical Technology (AREA)
- Environmental & Geological Engineering (AREA)
- Analytical Chemistry (AREA)
- Industrial Gases (AREA)
- Treating Waste Gases (AREA)
- Catalysts (AREA)
Claims (10)
1. Способ очистки газов, полученных из установки газификации, где топливо газифицируют с получением неочищенного синтез-газа, содержащего монооксид углерода и пар, в присутствии содержащего кальций соединения и пара, галогенсодержащие соединения удаляются из неочищенного синтез-газа, который направляют на стадию конверсии водяного газа, заключающуюся в каталитической конверсии монооксида углерода и пара, содержащихся в неочищенном синтез-газе, в диоксид углерода и водород, полученный таким образом конвертированный газ контактирует с твердым сорбентом серы, с последующим удалением очищенного конвертированного газа из твердого сорбента серы и регенерацией твердого сорбента серы, отличающийся тем, что регенерация твердого сорбента серы проводится путем пропускания потока пара через твердый сорбент серы в направлении, противоположном направлению потока конвертированного газа, при условиях, при которых образуется поток содержащего сероводород пара, и полученный таким образом поток содержащего сероводород пара направляется непосредственно на стадию газификации.
2. Способ по п.1, отличающийся тем, что в качестве содержащего кальций соединения используют доломит или кальцит.
3. Способ по п.1, отличающийся тем, что до удаления галогенов из неочищенного синтез-газа удаляют пыль и мелкодисперсную золу.
4. Способ по п.1, отличающийся тем, что стадию конверсии водяного газа проводят в присутствии катализатора, включающего молибден на носителе, при необходимости содержащего кобальт или никель.
5. Способ по п.1, отличающийся тем, что твердый сорбент серы включает оксиды олова на носителе или многослойные сорбенты на носителе.
6. Способ по п.5, отличающийся тем, что многослойный сорбент включает первый слой сорбента на основе оксида олова, конечный слой металла и по меньшей мере один промежуточный слой.
7. Способ по п.6, отличающийся тем, что конечный слой представляет собой медь или никель на носителе и последний промежуточный слой, находящийся перед конечным слоем, представляет собой слой оксида цинка.
8. Способ по п.5, отличающийся тем, что носитель выбран из группы, включающей глины, силикаты, оксид алюминия и диоксид титана.
9. Способ по п.1, отличающийся тем, что газификация проводится в реакторе с газификацией в потоке.
10. Способ по п.1 или 9, отличающийся тем, что давление потока содержащего сероводород пара из твердого сорбента серы эквивалентно давлению в реакторе газификации.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DKPA200500553 | 2005-04-15 | ||
| DKPA200500553 | 2005-04-15 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| RU2006112353A true RU2006112353A (ru) | 2007-11-10 |
| RU2417825C2 RU2417825C2 (ru) | 2011-05-10 |
Family
ID=37055672
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| RU2006112353/05A RU2417825C2 (ru) | 2005-04-15 | 2006-04-14 | Способ очистки газов, полученных из установки газификации |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US7618558B2 (ru) |
| CN (1) | CN1880412B (ru) |
| CA (1) | CA2543499C (ru) |
| DE (1) | DE102006017680B4 (ru) |
| RU (1) | RU2417825C2 (ru) |
| UA (1) | UA91821C2 (ru) |
| ZA (1) | ZA200603020B (ru) |
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| CN101312784B (zh) * | 2005-11-23 | 2011-06-22 | 国际壳牌研究有限公司 | 通过矿物碳酸盐化隔离二氧化碳的方法 |
| ES2822323T3 (es) * | 2006-09-25 | 2021-04-30 | Ohio State Innovation Foundation | Proceso de ciclado de calcio para la producción de hidrógeno de alta pureza |
| JP5522724B2 (ja) * | 2006-12-08 | 2014-06-18 | シエル・インターナシヨネイル・リサーチ・マーチヤツピイ・ベー・ウイ | 精製合成ガス流の製造方法 |
| US8328889B2 (en) * | 2007-12-12 | 2012-12-11 | Kellogg Brown & Root Llc | Efficiency of gasification processes |
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| CA2718536C (en) * | 2008-04-01 | 2014-06-03 | Greatpoint Energy, Inc. | Sour shift process for the removal of carbon monoxide from a gas stream |
| DE102008049579A1 (de) * | 2008-09-30 | 2010-04-01 | Uhde Gmbh | Heißgasreinigung |
| CN102438941A (zh) * | 2008-10-13 | 2012-05-02 | 俄亥俄州立大学研究基金会 | 结合二氧化碳、硫和卤化物捕获的用于生产高纯度氢气的钙循环工艺 |
| BRPI0919624A2 (pt) * | 2008-10-22 | 2015-12-01 | Southern Res Inst | processo de descontaminação de gás de síntese. |
| WO2010075027A1 (en) * | 2008-12-15 | 2010-07-01 | Katana Energy Llc | Emissions free sulfuric acid and sodium bisulfite production for desalination from gasification acid gas |
| US8343243B2 (en) * | 2009-03-31 | 2013-01-01 | General Electric Company | Method and apparatus for blending lignite and coke slurries |
| WO2011000792A2 (en) * | 2009-06-30 | 2011-01-06 | Shell Internationale Research Maatschappij B.V. | Process to prepare a hydrogen rich gas mixture |
| US8313641B2 (en) | 2010-06-30 | 2012-11-20 | Uop Llc | Adsorbent for feed and products purification in a reforming process |
| US8314277B2 (en) | 2010-06-30 | 2012-11-20 | Uop Llc | Adsorbent for feed and products purification in benzene saturation process |
| NL2008313C2 (en) * | 2012-02-17 | 2013-09-02 | Stichting Energie | Water gas shift process. |
| JP2014015499A (ja) * | 2012-07-06 | 2014-01-30 | Hitachi Ltd | ガス化方法とそのシステム、石炭ガス化複合発電方法とそのシステム。 |
| FR2997414B1 (fr) * | 2012-10-31 | 2015-10-02 | Ifp Energies Now | Procede ameliore de conversion d'une charge contenant de la biomasse pour la production d'hydrocarbures par voie de synthese fischer-tropsch |
| JP6025603B2 (ja) * | 2013-02-21 | 2016-11-16 | 三菱重工業株式会社 | Ｃｏシフト反応装置及びｃｏシフト変換方法 |
| JP6496104B2 (ja) * | 2014-02-18 | 2019-04-03 | クラリアント触媒株式会社 | ハロゲン化合物吸収剤およびそれを用いた合成ガスの製造方法 |
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| GB201519133D0 (en) | 2015-10-29 | 2015-12-16 | Johnson Matthey Plc | Process |
| UA123999C2 (uk) | 2015-10-29 | 2021-07-07 | Джонсон Метті Паблік Лімітед Компані | Каталізатор конверсії водяного газу |
| GB201519139D0 (en) | 2015-10-29 | 2015-12-16 | Johnson Matthey Plc | Process |
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| US10344231B1 (en) | 2018-10-26 | 2019-07-09 | Greatpoint Energy, Inc. | Hydromethanation of a carbonaceous feedstock with improved carbon utilization |
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| WO1996030465A1 (en) | 1995-03-30 | 1996-10-03 | Enviropower Inc. | Method for feeding regeneration offgas into a gasifier |
| CN1114583C (zh) * | 1998-10-06 | 2003-07-16 | 王国良 | 利用原煤独立制造甲醇的方法 |
| JP2002363578A (ja) * | 2001-06-01 | 2002-12-18 | Babcock Hitachi Kk | 水素・一酸化炭素混合ガスの製造方法および製造装置ならびに燃料・電力併産プラント |
| CN1213131C (zh) * | 2003-06-25 | 2005-08-03 | 中国科学院山西煤炭化学研究所 | 一种高温煤气脱硫除尘一体化方法及其设备 |
| RU41307U1 (ru) * | 2004-06-17 | 2004-10-20 | Открытое акционерное общество Украинский институт по проектированию нефтеперерабатывающих и нефтехимических предприятий (Укрнефтехимпроект) | Установка получения газов различной теплотворной способности из нефтяных остатков |
-
2006
- 2006-04-07 US US11/399,373 patent/US7618558B2/en not_active Expired - Fee Related
- 2006-04-12 DE DE102006017680.4A patent/DE102006017680B4/de not_active Expired - Fee Related
- 2006-04-13 ZA ZA200603020A patent/ZA200603020B/xx unknown
- 2006-04-13 CA CA2543499A patent/CA2543499C/en not_active Expired - Fee Related
- 2006-04-14 RU RU2006112353/05A patent/RU2417825C2/ru not_active IP Right Cessation
- 2006-04-14 CN CN2006100841854A patent/CN1880412B/zh not_active Expired - Fee Related
- 2006-04-14 UA UAA200604176A patent/UA91821C2/ru unknown
Also Published As
| Publication number | Publication date |
|---|---|
| CN1880412A (zh) | 2006-12-20 |
| DE102006017680B4 (de) | 2016-07-14 |
| US7618558B2 (en) | 2009-11-17 |
| RU2417825C2 (ru) | 2011-05-10 |
| US20060233687A1 (en) | 2006-10-19 |
| CN1880412B (zh) | 2012-01-11 |
| UA91821C2 (ru) | 2010-09-10 |
| DE102006017680A1 (de) | 2006-10-19 |
| ZA200603020B (en) | 2007-06-27 |
| CA2543499C (en) | 2014-04-08 |
| CA2543499A1 (en) | 2006-10-15 |
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| MM4A | The patent is invalid due to non-payment of fees |
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