RO87021B - Procedeu de preparare a acidului 2(6-metoxi-2-naftil)-propionic - Google Patents
Procedeu de preparare a acidului 2(6-metoxi-2-naftil)-propionicInfo
- Publication number
- RO87021B RO87021B RO109274A RO10927482A RO87021B RO 87021 B RO87021 B RO 87021B RO 109274 A RO109274 A RO 109274A RO 10927482 A RO10927482 A RO 10927482A RO 87021 B RO87021 B RO 87021B
- Authority
- RO
- Romania
- Prior art keywords
- methoxy
- formula
- preparation
- general formula
- compound
- Prior art date
Links
- XBDQKXXYIPTUBI-UHFFFAOYSA-N Propionic acid Substances CCC(O)=O XBDQKXXYIPTUBI-UHFFFAOYSA-N 0.000 title 1
- WYURNTSHIVDZCO-UHFFFAOYSA-N Tetrahydrofuran Chemical compound C1CCOC1 WYURNTSHIVDZCO-UHFFFAOYSA-N 0.000 abstract 2
- 150000001875 compounds Chemical class 0.000 abstract 2
- 125000002887 hydroxy group Chemical group [H]O* 0.000 abstract 2
- CMWTZPSULFXXJA-UHFFFAOYSA-N 2-(6-methoxy-2-naphthalenyl)propanoic acid Chemical compound C1=C(C(C)C(O)=O)C=CC2=CC(OC)=CC=C21 CMWTZPSULFXXJA-UHFFFAOYSA-N 0.000 abstract 1
- MBKVMGBEKHSWNJ-UHFFFAOYSA-N C1=C([Zn])C=CC2=CC(OC)=CC=C21 Chemical compound C1=C([Zn])C=CC2=CC(OC)=CC=C21 MBKVMGBEKHSWNJ-UHFFFAOYSA-N 0.000 abstract 1
- 239000002253 acid Substances 0.000 abstract 1
- 125000000217 alkyl group Chemical group 0.000 abstract 1
- 125000000539 amino acid group Chemical group 0.000 abstract 1
- 125000003118 aryl group Chemical group 0.000 abstract 1
- 125000005842 heteroatom Chemical group 0.000 abstract 1
- 125000000623 heterocyclic group Chemical group 0.000 abstract 1
- 150000002902 organometallic compounds Chemical class 0.000 abstract 1
- 150000003839 salts Chemical class 0.000 abstract 1
- LMBFAGIMSUYTBN-MPZNNTNKSA-N teixobactin Chemical compound C([C@H](C(=O)N[C@@H]([C@@H](C)CC)C(=O)N[C@@H](CO)C(=O)N[C@H](CCC(N)=O)C(=O)N[C@H]([C@@H](C)CC)C(=O)N[C@@H]([C@@H](C)CC)C(=O)N[C@@H](CO)C(=O)N[C@H]1C(N[C@@H](C)C(=O)N[C@@H](C[C@@H]2NC(=N)NC2)C(=O)N[C@H](C(=O)O[C@H]1C)[C@@H](C)CC)=O)NC)C1=CC=CC=C1 LMBFAGIMSUYTBN-MPZNNTNKSA-N 0.000 abstract 1
- YLQBMQCUIZJEEH-UHFFFAOYSA-N tetrahydrofuran Natural products C=1C=COC=1 YLQBMQCUIZJEEH-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F13/00—Compounds containing elements of Groups 7 or 17 of the Periodic Table
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C49/00—Ketones; Ketenes; Dimeric ketenes; Ketonic chelates
- C07C49/76—Ketones containing a keto group bound to a six-membered aromatic ring
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C309/00—Sulfonic acids; Halides, esters, or anhydrides thereof
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C43/00—Ethers; Compounds having groups, groups or groups
- C07C43/30—Compounds having groups
- C07C43/313—Compounds having groups containing halogen
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C43/00—Ethers; Compounds having groups, groups or groups
- C07C43/30—Compounds having groups
- C07C43/315—Compounds having groups containing oxygen atoms singly bound to carbon atoms not being acetal carbon atoms
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
- C07C45/004—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reaction with organometalhalides
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
- C07C45/51—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by pyrolysis, rearrangement or decomposition
- C07C45/54—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by pyrolysis, rearrangement or decomposition of compounds containing doubly bound oxygen atoms, e.g. esters
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C47/00—Compounds having —CHO groups
- C07C47/20—Unsaturated compounds having —CHO groups bound to acyclic carbon atoms
- C07C47/277—Unsaturated compounds having —CHO groups bound to acyclic carbon atoms containing ether groups, groups, groups, or groups
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D317/00—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms
- C07D317/02—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms having the hetero atoms in positions 1 and 2
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D317/00—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms
- C07D317/02—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms having the hetero atoms in positions 1 and 2
- C07D317/06—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms having the hetero atoms in positions 1 and 2 condensed with carbocyclic rings or ring systems
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D317/00—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms
- C07D317/08—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms having the hetero atoms in positions 1 and 3
- C07D317/10—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms having the hetero atoms in positions 1 and 3 not condensed with other rings
- C07D317/14—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms having the hetero atoms in positions 1 and 3 not condensed with other rings with substituted hydrocarbon radicals attached to ring carbon atoms
- C07D317/18—Radicals substituted by singly bound oxygen or sulfur atoms
- C07D317/24—Radicals substituted by singly bound oxygen or sulfur atoms esterified
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F3/00—Compounds containing elements of Groups 2 or 12 of the Periodic Table
- C07F3/02—Magnesium compounds
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F3/00—Compounds containing elements of Groups 2 or 12 of the Periodic Table
- C07F3/06—Zinc compounds
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Acyclic And Carbocyclic Compounds In Medicinal Compositions (AREA)
- Pyrane Compounds (AREA)
- Heterocyclic Compounds That Contain Two Or More Ring Oxygen Atoms (AREA)
- Ultra Sonic Daignosis Equipment (AREA)
- Luminescent Compositions (AREA)
- Seasonings (AREA)
- Transmission And Conversion Of Sensor Element Output (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Preparation Of Compounds By Using Micro-Organisms (AREA)
- Peptides Or Proteins (AREA)
- Medicines Containing Antibodies Or Antigens For Use As Internal Diagnostic Agents (AREA)
Abstract
Inventia se refera la un procedeu de preparare a acidului 2-(6-metoxi-2-naftil)-propionoc cu formula generala I (vezi formula) sau o sare acceptabila farmaceutic a acestuia prin prepararea unui compus cu formula generala Ii (vezi formula) în care Z este un rest amino al unui acid, grupele hidroxi sau grupa hidroxi protejata la care în scopul obtinerii unu singur stereoizomer al compusului cu formula II, se trateaza un compus organometalic ales dintre bromura sau clorura de '-(6-metoxi-2-naftil)-mangan si di-(6-metoxi-2-naftil)-zinc cu o substanta optic activa cu formula generala III în care Z este definit ca mai sus si Y este (vezi formula) halogen, preferabil clor sau brom sau un grup cu formula -N)R') (R'' în care R' si R'' sînt alchil sau aril luate împreuna cu N formeaza o parte heterociclica care poate contine si alti atomi hetero sau aciloxi, în tetrahidrofuran la temperaturi cuprinse între -70 degree C si temperatura camerei.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US32967281A | 1981-12-11 | 1981-12-11 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| RO87021A RO87021A (ro) | 1985-05-20 |
| RO87021B true RO87021B (ro) | 1985-05-31 |
Family
ID=23286496
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| RO109274A RO87021B (ro) | 1981-12-11 | 1982-12-09 | Procedeu de preparare a acidului 2(6-metoxi-2-naftil)-propionic |
Country Status (29)
| Country | Link |
|---|---|
| EP (1) | EP0081993B1 (ro) |
| JP (4) | JPS58135833A (ro) |
| KR (1) | KR890000375B1 (ro) |
| AT (1) | ATE36517T1 (ro) |
| AU (1) | AU560800B2 (ro) |
| CA (2) | CA1259627A (ro) |
| CS (1) | CS259510B2 (ro) |
| DD (1) | DD206372A5 (ro) |
| DE (1) | DE3278907D1 (ro) |
| DK (6) | DK551782A (ro) |
| ES (1) | ES518086A0 (ro) |
| FI (2) | FI901487A0 (ro) |
| GR (1) | GR77059B (ro) |
| HK (1) | HK51489A (ro) |
| HU (1) | HU191621B (ro) |
| IE (1) | IE53922B1 (ro) |
| IL (1) | IL67455A (ro) |
| IN (1) | IN156354B (ro) |
| IT (1) | IT1155421B (ro) |
| MX (1) | MX159862A (ro) |
| NO (1) | NO156650C (ro) |
| NZ (1) | NZ202773A (ro) |
| PH (5) | PH20529A (ro) |
| PL (1) | PL142997B1 (ro) |
| PT (1) | PT75973B (ro) |
| RO (1) | RO87021B (ro) |
| SG (1) | SG3089G (ro) |
| SU (1) | SU1577694A3 (ro) |
| ZA (1) | ZA829101B (ro) |
Families Citing this family (20)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| NZ198271A (en) * | 1980-09-11 | 1985-05-31 | Syntex Pharma Int | Preparation of alpha-aromatic-substituted alkanoic acids and intermediates |
| IT1208109B (it) * | 1983-11-23 | 1989-06-06 | Alfa Chem Ital | Procedimento per la risoluzione ottica di acidi arilpropionici |
| DE3461525D1 (en) * | 1984-02-02 | 1987-01-15 | Zambon Spa | Process for preparing alpha-arylalkanoic acids |
| IT1173216B (it) * | 1984-02-03 | 1987-06-18 | Zambon Spa | Processo per la preparazione di acidi alfa-idrossiaril-alcanoici |
| IT1174084B (it) * | 1984-05-10 | 1987-07-01 | Blaschim Spa | Procentimento per preparare il naproxen |
| US4670586A (en) * | 1984-09-12 | 1987-06-02 | Nippon Chemicals Co., Ltd. | Method for the production of α-aryl-alkanoic acid |
| IT1190362B (it) * | 1985-05-30 | 1988-02-16 | Zambon Spa | Preparazione del (6-metossi-2-naftil)-(1-bormoetil)-chetone e dei suoi derivati |
| IT1188181B (it) * | 1985-07-31 | 1988-01-07 | Zambon Spa | Processo per la preparazione di acidi carbossilici otticamente attivi e relativi intermedi |
| IT1198237B (it) * | 1986-12-23 | 1988-12-21 | Zambon Spa | Intermedi per la sintesi di composti organici |
| WO1989010350A1 (en) * | 1988-04-21 | 1989-11-02 | Ici Australia Operations Proprietary Limited | Preparation of an epoxide |
| IT1240228B (it) * | 1989-01-25 | 1993-11-27 | Syntex Inc | Preparazione di acidi alfa-metilarenacetici. |
| IT1251958B (it) * | 1991-10-18 | 1995-05-27 | Zambon Spa | Processo per la dealogenazione di derivati del naftalene |
| WO1995033707A1 (fr) * | 1994-06-08 | 1995-12-14 | Shionogi & Co., Ltd. | Procede de fabrication d'ester 4-oxo-2 alcenoique |
| JP3744060B2 (ja) * | 1996-06-20 | 2006-02-08 | ダイソー株式会社 | アシルオキシスルホン酸エステル誘導体の製造法 |
| WO2003014056A1 (fr) * | 2001-08-08 | 2003-02-20 | Kaneka Corporation | Procede de production d'un acide carboxylique 2-substitue optiquement actif |
| MXPA04001253A (es) * | 2001-08-09 | 2004-06-03 | Ono Pharmaceutical Co | Derivados de acidos carboxilicos y agente farmaceutico que comprende los mismos como ingrediente activo. |
| SK16482002A3 (sk) * | 2002-11-20 | 2004-06-08 | Slovakofarma, A. S. | Spôsob prípravy substituovaných derivátov 2-aryl alkánových kyselín |
| CN106496092B (zh) * | 2016-08-30 | 2019-03-29 | 江苏宇田医药有限公司 | 一种用于合成西洛多辛的中间体的制备方法 |
| CN112110801B (zh) * | 2020-10-09 | 2022-07-19 | 浙江工业大学 | 一种γ-芳基取代酮类化合物的合成方法 |
| CN114644554A (zh) * | 2020-12-21 | 2022-06-21 | 上海医药工业研究院 | (s)-氟比洛芬的制备方法及其中间体 |
Family Cites Families (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3637767A (en) * | 1968-07-30 | 1972-01-25 | Syntex Corp | 2-(6'-methoxynaphth-2'-yl)propylene oxide and 5'-halo derivatives |
| ES455064A1 (es) * | 1977-01-17 | 1978-02-01 | Valles Quimica | Nuevo procedimiento para la obtencion del acido (d)-2(6-me- toxi-2-naftil)-propionico. |
| JPS5519214A (en) * | 1978-07-27 | 1980-02-09 | Ono Pharmaceut Co Ltd | 2-acyl-6-aminomethylphenol derivative and its preparation |
| JPS55130934A (en) * | 1979-03-31 | 1980-10-11 | Masao Sato | Ketone synthesis from grignard reagent and acid halide |
| IE50897B1 (en) * | 1980-02-26 | 1986-08-06 | Blaschim Spa | Process for preparing esters of alkanoic acids via rearrangement of alpha-haloketals |
| IT1212408B (it) * | 1980-02-26 | 1989-11-22 | Blaschim Spa | Processo per la produzione di acidi alcanoici alfa sostituiti. |
| NZ198271A (en) * | 1980-09-11 | 1985-05-31 | Syntex Pharma Int | Preparation of alpha-aromatic-substituted alkanoic acids and intermediates |
| JPS5798232A (en) * | 1980-11-10 | 1982-06-18 | Sagami Chem Res Center | 1-(6-methoxy-2-naphthyl)-2-oxy-1-alkanone acetal |
| IL65629A (en) * | 1981-04-30 | 1987-08-31 | Syntex Pharma Int | Preparation of alpha-arylalkanoic acids and esters and salts thereof |
| JPS5810525A (ja) * | 1981-06-15 | 1983-01-21 | Sagami Chem Res Center | 光学活性な１−芳香族基置換−１−アルカノン類の製造方法 |
-
1982
- 1982-12-07 FI FI901487A patent/FI901487A0/fi not_active Application Discontinuation
- 1982-12-07 FI FI824203A patent/FI82680C/fi not_active IP Right Cessation
- 1982-12-08 MX MX195510A patent/MX159862A/es unknown
- 1982-12-09 PH PH28253A patent/PH20529A/en unknown
- 1982-12-09 RO RO109274A patent/RO87021B/ro unknown
- 1982-12-10 AT AT82306603T patent/ATE36517T1/de not_active IP Right Cessation
- 1982-12-10 PT PT75973A patent/PT75973B/pt not_active IP Right Cessation
- 1982-12-10 DK DK551782A patent/DK551782A/da not_active Application Discontinuation
- 1982-12-10 CS CS829038A patent/CS259510B2/cs unknown
- 1982-12-10 GR GR70038A patent/GR77059B/el unknown
- 1982-12-10 DD DD82245847A patent/DD206372A5/de not_active IP Right Cessation
- 1982-12-10 IL IL67455A patent/IL67455A/xx not_active IP Right Cessation
- 1982-12-10 PL PL1982239456A patent/PL142997B1/pl unknown
- 1982-12-10 EP EP82306603A patent/EP0081993B1/en not_active Expired
- 1982-12-10 NO NO824175A patent/NO156650C/no unknown
- 1982-12-10 AU AU91464/82A patent/AU560800B2/en not_active Ceased
- 1982-12-10 ES ES518086A patent/ES518086A0/es active Granted
- 1982-12-10 NZ NZ202773A patent/NZ202773A/en unknown
- 1982-12-10 ZA ZA829101A patent/ZA829101B/xx unknown
- 1982-12-10 HU HU823988A patent/HU191621B/hu not_active IP Right Cessation
- 1982-12-10 IN IN1435/CAL/82A patent/IN156354B/en unknown
- 1982-12-10 JP JP57216765A patent/JPS58135833A/ja active Granted
- 1982-12-10 KR KR8205541A patent/KR890000375B1/ko not_active Expired
- 1982-12-10 IT IT24665/82A patent/IT1155421B/it active
- 1982-12-10 IE IE2945/82A patent/IE53922B1/en not_active IP Right Cessation
- 1982-12-10 SU SU823524059A patent/SU1577694A3/ru active
- 1982-12-10 DE DE8282306603T patent/DE3278907D1/de not_active Expired
- 1982-12-10 CA CA000417445A patent/CA1259627A/en not_active Expired
-
1983
- 1983-03-27 PH PH30451A patent/PH21336A/en unknown
-
1984
- 1984-03-27 PH PH30452A patent/PH20059A/en unknown
- 1984-03-27 PH PH30453A patent/PH20169A/en unknown
-
1985
- 1985-07-18 PH PH32535A patent/PH22187A/en unknown
-
1988
- 1988-08-17 DK DK461488A patent/DK461488D0/da not_active Application Discontinuation
- 1988-08-17 DK DK461388A patent/DK461388A/da not_active Application Discontinuation
- 1988-08-17 DK DK461288A patent/DK461288A/da not_active Application Discontinuation
- 1988-08-17 DK DK461588A patent/DK461588A/da not_active Application Discontinuation
- 1988-08-17 DK DK461188A patent/DK461188D0/da not_active Application Discontinuation
-
1989
- 1989-01-13 SG SG30/89A patent/SG3089G/en unknown
- 1989-06-29 HK HK514/89A patent/HK51489A/en not_active IP Right Cessation
-
1990
- 1990-02-28 JP JP2049174A patent/JPH02262533A/ja active Granted
- 1990-02-28 JP JP2049173A patent/JPH02270840A/ja active Pending
- 1990-02-28 JP JP2049175A patent/JPH02262532A/ja active Pending
-
1992
- 1992-05-13 CA CA000616341A patent/CA1338433C/en not_active Expired - Fee Related
Also Published As
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