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PE20081328A1 - Reactor y proceso para preparar sulfuro de hidrogeno - Google Patents

Reactor y proceso para preparar sulfuro de hidrogeno

Info

Publication number
PE20081328A1
PE20081328A1 PE2008000143A PE2008000143A PE20081328A1 PE 20081328 A1 PE20081328 A1 PE 20081328A1 PE 2008000143 A PE2008000143 A PE 2008000143A PE 2008000143 A PE2008000143 A PE 2008000143A PE 20081328 A1 PE20081328 A1 PE 20081328A1
Authority
PE
Peru
Prior art keywords
reactor
plate
hydrogen
gaseous
edge
Prior art date
Application number
PE2008000143A
Other languages
English (en)
Inventor
Andreas Wolfert
Harald Jachow
Heinz Driess
Original Assignee
Basf Ag
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Basf Ag filed Critical Basf Ag
Publication of PE20081328A1 publication Critical patent/PE20081328A1/es

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B17/00Sulfur; Compounds thereof
    • C01B17/16Hydrogen sulfides
    • C01B17/161Preparation from elemental sulfur
    • C01B17/162Preparation from elemental sulfur from elemental sulfur and hydrogen
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J10/00Chemical processes in general for reacting liquid with gaseous media other than in the presence of solid particles, or apparatus specially adapted therefor
    • B01J10/005Chemical processes in general for reacting liquid with gaseous media other than in the presence of solid particles, or apparatus specially adapted therefor carried out at high temperatures in the presence of a molten material
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24Stationary reactors without moving elements inside
    • B01J19/2415Tubular reactors
    • B01J19/242Tubular reactors in series
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/008Details of the reactor or of the particulate material; Processes to increase or to retard the rate of reaction
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/06Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds in tube reactors; the solid particles being arranged in tubes
    • B01J8/065Feeding reactive fluids
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/06Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds in tube reactors; the solid particles being arranged in tubes
    • B01J8/067Heating or cooling the reactor

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)
  • Manufacture And Refinement Of Metals (AREA)
  • Hydrogen, Water And Hydrids (AREA)

Abstract

DONDE EL REACTOR INCLUYE: a) UN DISPOSITIVO DE DISTRIBUCION, COLOCADO EN UNA FUNDICION DE AZUFRE, QUE COMPRENDE UNA PLACA DE DISTRIBUCION COLOCADA EN EL REACTOR Y POSEE UN BORDE QUE SE EXTIENDE HACIA ABAJO CON UNA REGION DEL BORDE DENTADO; b) UN DISPOSITIVO DE ALIMENTACION PARA INTRODUCIR EL HIDROGENO GASEOSO EN EL REACTOR, QUE COMPRENDE UN TUBO ABIERTO COLOCADO DE MANERA VERTICAL EN EL REACTOR Y A TRAVES DEL CUAL EL HIDROGENO GASEOSO PUEDE PASAR HACIA LA FUNDICION; Y, c) UN TUBO DE CONTACTO CONECTADO A LA PLACA DE DISTRIBUCION DE (a). EL PROCESO COMPRENDE PASAR Y DISTRIBUIR HIDROGENO GASEOSO EN UNA FUNDICION DE AZUFRE PRESENTE AL MENOS EN LA PARTE INFERIOR DEL REACTOR, A TRAVES DE (a), DONDE EL HIDROGENO SE DISTRIBUYE EN LA FUNDICION A PARTIR DE UNA BURBUJA DE HIDROGENO QUE SE FORMA DEBAJO DE LA PLACA A TRAVES DE LA REGION DEL BORDE (BRECHA ENTRE EL BORDE Y UNA CAMISA DEL REACTOR). LA PLACA TIENE ORIFICIOS DE PASO (CIRCULARES CON UN DIAMETRO DE 0,2 A 3 cm CADA UNO, O CON FORMA DE RANURA DE LA PLACA CON UN ANCHO DE RANURA DE 0,2 A 3 cm) A TRAVES DE LOS CUALES EL HIDROGENO DE LA BURBUJA SE DISTRIBUYE EN LA FUNDICION, SIENDO EL AREA TOTAL DE LOS ORIFICIOS, BASADA EN EL AREA DE LA PLACA, DE 0,001% A 5%
PE2008000143A 2007-01-16 2008-01-16 Reactor y proceso para preparar sulfuro de hidrogeno PE20081328A1 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
EP07100588 2007-01-16

Publications (1)

Publication Number Publication Date
PE20081328A1 true PE20081328A1 (es) 2008-11-12

Family

ID=39429990

Family Applications (2)

Application Number Title Priority Date Filing Date
PE2012000176A PE20121273A1 (es) 2007-01-16 2008-01-16 Reactor y proceso para preparar sulfuro de hidrogeno
PE2008000143A PE20081328A1 (es) 2007-01-16 2008-01-16 Reactor y proceso para preparar sulfuro de hidrogeno

Family Applications Before (1)

Application Number Title Priority Date Filing Date
PE2012000176A PE20121273A1 (es) 2007-01-16 2008-01-16 Reactor y proceso para preparar sulfuro de hidrogeno

Country Status (10)

Country Link
US (2) US7871594B2 (es)
EP (1) EP2125611B1 (es)
JP (1) JP5558830B2 (es)
CN (1) CN101610976B (es)
CA (1) CA2674276C (es)
CL (1) CL2008000131A1 (es)
ES (1) ES2612956T3 (es)
PE (2) PE20121273A1 (es)
PL (1) PL2125611T3 (es)
WO (1) WO2008087086A1 (es)

Families Citing this family (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
PL2125611T3 (pl) * 2007-01-16 2017-04-28 Basf Se Reaktor i sposób wytwarzania siarkowodoru
CN102177216A (zh) * 2008-09-05 2011-09-07 弗拉格赛欧股份有限公司 改进的、低粘度硫作为导热和储热液体的应用
JP5774025B2 (ja) * 2010-01-05 2015-09-02 ビーエーエスエフ ソシエタス・ヨーロピアBasf Se ポリスルフィドベースの極高温のための伝熱流体および蓄熱流体
WO2013027431A1 (ja) * 2011-08-23 2013-02-28 日揮株式会社 硫化水素合成反応器、硫化水素製造装置、硫化水素ナトリウム製造装置、及びそれらの方法
CN105169936A (zh) * 2015-09-30 2015-12-23 苏州韵蓝环保科技有限公司 一种气液洗涤塔
US10577314B2 (en) 2016-05-31 2020-03-03 Novus International, Inc. Process for producing methyl mercaptan from dimethyl sulfide

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US1623942A (en) * 1925-11-09 1927-04-05 Raymond M Garey Method for the prepartion of hydrogen sulphide
NL26828C (es) * 1927-01-19
US1700578A (en) * 1927-05-05 1929-01-29 Raymond F Bacon Production of hydrogen sulphide
DE558432C (de) 1930-09-27 1932-09-07 I G Farbenindustrie Akt Ges Verfahren zur Herstellung von Schwefelwasserstoff
US2214859A (en) * 1938-12-17 1940-09-17 Hooker Electrochemical Co Process for production of hydrogen sulphide
GB598885A (en) 1939-05-11 1948-03-01 Pingris & Mollet Fontaine Reun Chemical reaction furnace with high thermal efficiency
US2474066A (en) * 1946-01-04 1949-06-21 Barium Reduction Corp Method of making hydrogen sulfide
US2687948A (en) * 1949-02-11 1954-08-31 Gregory Paul Methods of and means for thermal operations
DE869198C (de) 1950-05-21 1953-03-05 Basf Ag Verfahren zur Reinigung von Rohbenzol
US2965455A (en) 1953-04-24 1960-12-20 Hooker Chemical Corp Apparatus for producing hydrogen sulfide
US2863725A (en) * 1953-04-24 1958-12-09 Hooker Chemical Corp Process for making sulfur free hydrogen sulfide
US2876070A (en) * 1955-03-28 1959-03-03 Chemetron Corp Method for producing hydrogen sulfide by synthesis
US2876071A (en) * 1955-05-31 1959-03-03 Chemetron Corp Method for producing hydrogen sulfide by synthesis
DE1113446B (de) 1960-06-09 1961-09-07 Basf Ag Verfahren zur Herstellung von Schwefelwasserstoff
FR1593276A (es) * 1967-12-19 1970-05-25
US3672847A (en) * 1970-03-05 1972-06-27 Selas Corp Of America Reformer furnace
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DE10245164B4 (de) * 2002-09-26 2014-11-13 Evonik Degussa Gmbh Verfahren zur Umwandlung von Polysulfanen
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PL2125611T3 (pl) * 2007-01-16 2017-04-28 Basf Se Reaktor i sposób wytwarzania siarkowodoru

Also Published As

Publication number Publication date
CN101610976A (zh) 2009-12-23
US20110081278A1 (en) 2011-04-07
CN101610976B (zh) 2012-12-05
CL2008000131A1 (es) 2009-01-23
US20100015036A1 (en) 2010-01-21
EP2125611B1 (de) 2016-11-02
CA2674276A1 (en) 2008-07-24
WO2008087086A1 (de) 2008-07-24
US8580208B2 (en) 2013-11-12
JP2010515657A (ja) 2010-05-13
US7871594B2 (en) 2011-01-18
ES2612956T3 (es) 2017-05-19
JP5558830B2 (ja) 2014-07-23
PE20121273A1 (es) 2012-10-22
PL2125611T3 (pl) 2017-04-28
EP2125611A1 (de) 2009-12-02
CA2674276C (en) 2016-07-19

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Legal Events

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FG Grant, registration
FD Application declared void or lapsed