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GB984806A - Process for the production of substituted borazoles - Google Patents

Process for the production of substituted borazoles

Info

Publication number
GB984806A
GB984806A GB1656862A GB1656862A GB984806A GB 984806 A GB984806 A GB 984806A GB 1656862 A GB1656862 A GB 1656862A GB 1656862 A GB1656862 A GB 1656862A GB 984806 A GB984806 A GB 984806A
Authority
GB
United Kingdom
Prior art keywords
hydrocarbon radical
borazole
trihydrogen
chlorophenyl
tri
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB1656862A
Inventor
Elmar-Manfred Horn
Konrad Lang
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Bayer AG
Original Assignee
Bayer AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Bayer AG filed Critical Bayer AG
Priority to GB1656862A priority Critical patent/GB984806A/en
Publication of GB984806A publication Critical patent/GB984806A/en
Expired legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F5/00—Compounds containing elements of Groups 3 or 13 of the Periodic Table
    • C07F5/02—Boron compounds
    • C07F5/022—Boron compounds without C-boron linkages
    • C—CHEMISTRY; METALLURGY
    • C06—EXPLOSIVES; MATCHES
    • C06B—EXPLOSIVES OR THERMIC COMPOSITIONS; MANUFACTURE THEREOF; USE OF SINGLE SUBSTANCES AS EXPLOSIVES
    • C06B47/00—Compositions in which the components are separately stored until the moment of burning or explosion, e.g. "Sprengel"-type explosives; Suspensions of solid component in a normally non-explosive liquid phase, including a thickened aqueous phase
    • C06B47/02—Compositions in which the components are separately stored until the moment of burning or explosion, e.g. "Sprengel"-type explosives; Suspensions of solid component in a normally non-explosive liquid phase, including a thickened aqueous phase the components comprising a binary propellant
    • C06B47/10—Compositions in which the components are separately stored until the moment of burning or explosion, e.g. "Sprengel"-type explosives; Suspensions of solid component in a normally non-explosive liquid phase, including a thickened aqueous phase the components comprising a binary propellant a component containing free boron, an organic borane or a binary compound of boron, except with oxygen

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)

Abstract

N-Substituted borazoles of the formula <FORM:0984806/C2/1> where R represents an aliphatic hydrocarbon radical, a cycloaliphatic hydrocarbon radical, an aromatic hydrocarbon radical, a substituted aromatic hydrocarbon radical or an aralkyl hydrocarbon radical, are made by reacting an amine-borane represented by the formula R13N:BH3 wherein R1 represents an aliphati hydrocarbon radical, a cycloaliphatic hydrocarbon radical, or an aromatic hydrocarbon radical with a primary amine RNH2 under anhydrous conditions, in an inert medium at a molar ratio of about 1:1 of the reactants and at a temperature at which 2 mols. of hydrogen are split off per mol. amine, preferably in a temperature range from 40 DEG -130 DEG C., and isolating a borazole from the resulting mass. The amineborane can be made in situ by reaction of a tertiary amine, borohydride and boron halide as described in Specification 877,863. Suitable starting materials are specified. Detailed examples describe the preparation of (1) N,N1,N11 - tricyclohexyl - B,B1,B11 - trihydrogen barazole; (2) N,N1,N11 - tridodecyl - B,B1,B11 - trihydrogen borazole; (3) N,N1,N11 - tri (2 - chlorophenyl), (4) N,N1,N11 - tri (3 - chlorophenyl) - and (5) N,N1,N11 - (tri - 4 - chlorophenyl) - B,B1,B11 - trihydrogen borazole; (6) N,N1,N11 - tribenzyl - B,B1,B11 - trihydrogen borazole.
GB1656862A 1962-05-01 1962-05-01 Process for the production of substituted borazoles Expired GB984806A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
GB1656862A GB984806A (en) 1962-05-01 1962-05-01 Process for the production of substituted borazoles

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
GB1656862A GB984806A (en) 1962-05-01 1962-05-01 Process for the production of substituted borazoles

Publications (1)

Publication Number Publication Date
GB984806A true GB984806A (en) 1965-03-03

Family

ID=10079658

Family Applications (1)

Application Number Title Priority Date Filing Date
GB1656862A Expired GB984806A (en) 1962-05-01 1962-05-01 Process for the production of substituted borazoles

Country Status (1)

Country Link
GB (1) GB984806A (en)

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2014057885A1 (en) * 2012-10-12 2014-04-17 Ｊｘ日鉱日石エネルギー株式会社 Lubricant additive and lubricating oil composition
JP2014080459A (en) * 2012-10-12 2014-05-08 Jx Nippon Oil & Energy Corp Lubricant additive and lubricating oil composition
JP2014080460A (en) * 2012-10-12 2014-05-08 Jx Nippon Oil & Energy Corp Lubricating oil composition
WO2015156393A1 (en) * 2014-04-11 2015-10-15 Ｊｘ日鉱日石エネルギー株式会社 Lubricant composition
WO2015156392A1 (en) * 2014-04-11 2015-10-15 Ｊｘ日鉱日石エネルギー株式会社 Lubricant composition for internal combustion engine

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2014057885A1 (en) * 2012-10-12 2014-04-17 Ｊｘ日鉱日石エネルギー株式会社 Lubricant additive and lubricating oil composition
JP2014080459A (en) * 2012-10-12 2014-05-08 Jx Nippon Oil & Energy Corp Lubricant additive and lubricating oil composition
JP2014080460A (en) * 2012-10-12 2014-05-08 Jx Nippon Oil & Energy Corp Lubricating oil composition
WO2015156393A1 (en) * 2014-04-11 2015-10-15 Ｊｘ日鉱日石エネルギー株式会社 Lubricant composition
WO2015156392A1 (en) * 2014-04-11 2015-10-15 Ｊｘ日鉱日石エネルギー株式会社 Lubricant composition for internal combustion engine

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