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GB916318A - Improvements in and relating to the production of regenerated cellulose filaments from viscose - Google Patents

Improvements in and relating to the production of regenerated cellulose filaments from viscose

Info

Publication number
GB916318A
GB916318A GB30795/60A GB3079560A GB916318A GB 916318 A GB916318 A GB 916318A GB 30795/60 A GB30795/60 A GB 30795/60A GB 3079560 A GB3079560 A GB 3079560A GB 916318 A GB916318 A GB 916318A
Authority
GB
United Kingdom
Prior art keywords
filaments
viscose
holes
cellulose
bath
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB30795/60A
Inventor
Peter Lewis
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Akzo Nobel UK PLC
Original Assignee
Courtaulds PLC
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Courtaulds PLC filed Critical Courtaulds PLC
Priority to GB30795/60A priority Critical patent/GB916318A/en
Priority to US136580A priority patent/US3097914A/en
Priority to BE607955A priority patent/BE607955A/en
Priority to FR872628A priority patent/FR1302067A/en
Priority to NL269028A priority patent/NL269028A/en
Priority to SE893161A priority patent/SE219624C1/en
Publication of GB916318A publication Critical patent/GB916318A/en
Expired legal-status Critical Current

Links

Classifications

    • DTEXTILES; PAPER
    • D01NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01FCHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
    • D01F2/00Monocomponent artificial filaments or the like of cellulose or cellulose derivatives; Manufacture thereof
    • D01F2/06Monocomponent artificial filaments or the like of cellulose or cellulose derivatives; Manufacture thereof from viscose
    • D01F2/08Composition of the spinning solution or the bath

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Artificial Filaments (AREA)

Abstract

Ribbon filaments of regenerated cellulose are made by extruding viscose having a cellulose to caustic soda ratio of at least 1 and at a salt point of 4-6 through a multihole jet, the holes of which have no re-entrant sector in their cross-sections, into a coagulating bath held at 40 DEG -60 DEG C. and containing at least 24% Na2SO4, 9-12% H2SO4 and not more than 0,02% ZnSO4 as an impurity, drawing the incompletely regenerated filaments from the bath and subsequently completely regenerating the filaments. Preferably the jet holes are of circular cross-section. The cellulose to caustic soda ratio of the viscose may be at least 1,4 with a salt point of 4-6, or may be between 1 and 1,25, when the salt point is desirably 4-4,5. In an example a viscose is extruded through holes of 0,005 inch diameter and the filaments pass through the bath for 24 inches before being lapped on a godet. They are then stretched 30% in passing to a second godet of higher peripheral speed, collected in a centrifugal box and the cake washed successively with dilute acid and water. Such filaments have an elongated cross-section, their width being in general five times their thickness.
GB30795/60A 1960-09-07 1960-09-07 Improvements in and relating to the production of regenerated cellulose filaments from viscose Expired GB916318A (en)

Priority Applications (6)

Application Number Priority Date Filing Date Title
GB30795/60A GB916318A (en) 1960-09-07 1960-09-07 Improvements in and relating to the production of regenerated cellulose filaments from viscose
US136580A US3097914A (en) 1960-09-07 1961-09-07 Process for the production of a ribbon filament yarn of regenerated cellulose
BE607955A BE607955A (en) 1960-09-07 1961-09-07 Improvements relating to the production of regenerated cellulose filaments from viscose
FR872628A FR1302067A (en) 1960-09-07 1961-09-07 Improvements in the production of regenerated cellulose filaments
NL269028A NL269028A (en) 1960-09-07 1961-09-07 Method for manufacturing a ribbon filament thread from regenerated cellulose
SE893161A SE219624C1 (en) 1960-09-07 1961-09-07 Method for producing a fiber bundle of regenerated cellulose whose fibers have an elongated cross-section

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
GB30795/60A GB916318A (en) 1960-09-07 1960-09-07 Improvements in and relating to the production of regenerated cellulose filaments from viscose

Publications (1)

Publication Number Publication Date
GB916318A true GB916318A (en) 1963-01-23

Family

ID=10313245

Family Applications (1)

Application Number Title Priority Date Filing Date
GB30795/60A Expired GB916318A (en) 1960-09-07 1960-09-07 Improvements in and relating to the production of regenerated cellulose filaments from viscose

Country Status (6)

Country Link
US (1) US3097914A (en)
BE (1) BE607955A (en)
FR (1) FR1302067A (en)
GB (1) GB916318A (en)
NL (1) NL269028A (en)
SE (1) SE219624C1 (en)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4405549A (en) * 1981-07-13 1983-09-20 International Telephone And Telegraph Corporation Zinc-free preparation of rayon fibers
US4402899A (en) * 1981-07-13 1983-09-06 International Telephone And Telegraph Corporation Zinc-free preparation of rayon fibers
EP0574762A1 (en) * 1992-06-13 1993-12-22 Hoechst Aktiengesellschaft Process for the production of viscose rayon fibers with ribbon-like cross-section

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US1366166A (en) * 1919-02-04 1921-01-18 Courtaulds Ltd Squirting-nozzle for use in the manufacture of strips and the like from viscose and analogous matter and for similar purposes
US1964659A (en) * 1933-02-09 1934-06-26 Delaware Rayon Company Spinnerette
BE423040A (en) * 1936-08-08
US2327516A (en) * 1939-07-22 1943-08-24 Fink Heinrich Manufacture of artificial filaments and fibers from viscose
FR961352A (en) * 1947-04-26 1950-05-11

Also Published As

Publication number Publication date
FR1302067A (en) 1962-08-24
BE607955A (en) 1962-01-02
US3097914A (en) 1963-07-16
SE219624C1 (en) 1968-03-19
NL269028A (en) 1964-06-25

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