GB915932A - Process for the production of bis-benzthiazolyl-disulphide - Google Patents
Process for the production of bis-benzthiazolyl-disulphideInfo
- Publication number
- GB915932A GB915932A GB2497461A GB2497461A GB915932A GB 915932 A GB915932 A GB 915932A GB 2497461 A GB2497461 A GB 2497461A GB 2497461 A GB2497461 A GB 2497461A GB 915932 A GB915932 A GB 915932A
- Authority
- GB
- United Kingdom
- Prior art keywords
- mercaptobenzthiazole
- nitrosyl chloride
- nitric oxide
- benzthiazolyl
- disulphide
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- AFZSMODLJJCVPP-UHFFFAOYSA-N dibenzothiazol-2-yl disulfide Chemical compound C1=CC=C2SC(SSC=3SC4=CC=CC=C4N=3)=NC2=C1 AFZSMODLJJCVPP-UHFFFAOYSA-N 0.000 title abstract 3
- MWUXSHHQAYIFBG-UHFFFAOYSA-N Nitric oxide Chemical compound O=[N] MWUXSHHQAYIFBG-UHFFFAOYSA-N 0.000 abstract 8
- YXIWHUQXZSMYRE-UHFFFAOYSA-N 1,3-benzothiazole-2-thiol Chemical compound C1=CC=C2SC(S)=NC2=C1 YXIWHUQXZSMYRE-UHFFFAOYSA-N 0.000 abstract 5
- 239000004157 Nitrosyl chloride Substances 0.000 abstract 5
- VPCDQGACGWYTMC-UHFFFAOYSA-N nitrosyl chloride Chemical compound ClN=O VPCDQGACGWYTMC-UHFFFAOYSA-N 0.000 abstract 5
- 235000019392 nitrosyl chloride Nutrition 0.000 abstract 5
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 abstract 3
- 239000000460 chlorine Substances 0.000 abstract 3
- 229910052801 chlorine Inorganic materials 0.000 abstract 3
- 239000007900 aqueous suspension Substances 0.000 abstract 2
- 239000000203 mixture Substances 0.000 abstract 2
- -1 Ammonium ions Chemical class 0.000 abstract 1
- 239000007864 aqueous solution Substances 0.000 abstract 1
- 159000000007 calcium salts Chemical class 0.000 abstract 1
- 239000002245 particle Substances 0.000 abstract 1
- 150000003839 salts Chemical class 0.000 abstract 1
- 239000000725 suspension Substances 0.000 abstract 1
Landscapes
- Thiazole And Isothizaole Compounds (AREA)
Abstract
Bis-benzthiazolyl-disulphide is obtained by reacting an aqueous suspension of mercaptobenzthiazole, or an aqueous solution of a salt of mercaptobenzthiazole, with nitrosyl chloride, or with a mixture of nitric oxide and nitrosyl chloride or nitric oxide, nitrosyl chloride and chlorine. The nitrosyl chloride is obtained by reacting nitric oxide with chlorine, and the nitric oxide formed by reacting nitrosyl chloride with mercaptobenzthiazole, is reacted with further chlorine and recycled. The reaction is carried out at 0 DEG to 50 DEG C. by passing the gas mixture into an aqueous suspension containing 1 to 15% by weight of mercaptobenzthiazole. Ammonium ions may be present in the suspension to reduce the particle size of the product. In examples bis-benzthiazolyl-disulphide is obtained from mercaptobenzthiazole and from its calcium salt.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DEF31627A DE1135909B (en) | 1960-07-09 | 1960-07-09 | Process for the preparation of dibenzthiazolydisulfide |
| DEF32779A DE1143203B (en) | 1960-12-16 | 1960-12-16 | Process for the preparation of dibenzthiazolyl disulfide |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB915932A true GB915932A (en) | 1963-01-16 |
Family
ID=25974720
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB2497461A Expired GB915932A (en) | 1960-07-09 | 1961-07-10 | Process for the production of bis-benzthiazolyl-disulphide |
Country Status (1)
| Country | Link |
|---|---|
| GB (1) | GB915932A (en) |
-
1961
- 1961-07-10 GB GB2497461A patent/GB915932A/en not_active Expired
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