GB800160A - Process of producing anhydrous zirconium salts of organic monocarboxylic acids - Google Patents
Process of producing anhydrous zirconium salts of organic monocarboxylic acidsInfo
- Publication number
- GB800160A GB800160A GB20775/56A GB2077556A GB800160A GB 800160 A GB800160 A GB 800160A GB 20775/56 A GB20775/56 A GB 20775/56A GB 2077556 A GB2077556 A GB 2077556A GB 800160 A GB800160 A GB 800160A
- Authority
- GB
- United Kingdom
- Prior art keywords
- acetic acid
- zirconium
- acetate
- excess
- tetrachloride
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/41—Preparation of salts of carboxylic acids
- C07C51/412—Preparation of salts of carboxylic acids by conversion of the acids, their salts, esters or anhydrides with the same carboxylic acid part
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
- C07F7/003—Compounds containing elements of Groups 4 or 14 of the Periodic Table without C-Metal linkages
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
Abstract
Anhydrous zirconium salts of acetic acid and of fatty acids containing at least 4 carbon atoms in the hydrocarbon group are obtained by heating zirconium tetrachloride with an excess of acetic acid or with the equivalent quantity of fatty acid dissolved in an organic solvent, and distilling off the hydrogen chloride together with the excess of acetic acid or the solvent. The removal of hydrogen chloride may be accelerated by the passage of an inert gas such as carbon dioxide, nitrogen or dry air. Specified solvents are benzene, carbon tetrachloride and petroleum ether. When preparing zirconium acetate it is advisable to react no more tetrachloride with excess of acetic acid than will ensure that the zirconium tetra-acetate remains in solution in the boiling glacial acetic acid. On cooling the acetate precipitates. It may be dried by the passage of nitrogen or dry air at 110-130 DEG C. When preparing zirconium salts of the higher acids, the solvent is completely removed. Examples describe the preparation of anhydrous zirconium acetate and stearate.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE800160X | 1955-08-20 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB800160A true GB800160A (en) | 1958-08-20 |
Family
ID=6712198
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB20775/56A Expired GB800160A (en) | 1955-08-20 | 1956-07-04 | Process of producing anhydrous zirconium salts of organic monocarboxylic acids |
Country Status (1)
| Country | Link |
|---|---|
| GB (1) | GB800160A (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3076831A (en) * | 1960-01-29 | 1963-02-05 | Goldschmidt Ag Th | Manufacture of crystalline zirconium tetraacetate |
| US3104248A (en) * | 1960-12-30 | 1963-09-17 | Nat Lead Co | Acetatozirconyl halides |
| CN108752189A (en) * | 2018-06-20 | 2018-11-06 | 乐山沃耐稀电子材料有限公司 | A kind of preparation method of acetic acid zirconium |
| CN116651499A (en) * | 2023-05-12 | 2023-08-29 | 国家能源集团宁夏煤业有限责任公司 | Method for producing Fischer-Tropsch wax oxidation reaction catalyst and its application |
-
1956
- 1956-07-04 GB GB20775/56A patent/GB800160A/en not_active Expired
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3076831A (en) * | 1960-01-29 | 1963-02-05 | Goldschmidt Ag Th | Manufacture of crystalline zirconium tetraacetate |
| US3104248A (en) * | 1960-12-30 | 1963-09-17 | Nat Lead Co | Acetatozirconyl halides |
| CN108752189A (en) * | 2018-06-20 | 2018-11-06 | 乐山沃耐稀电子材料有限公司 | A kind of preparation method of acetic acid zirconium |
| CN116651499A (en) * | 2023-05-12 | 2023-08-29 | 国家能源集团宁夏煤业有限责任公司 | Method for producing Fischer-Tropsch wax oxidation reaction catalyst and its application |
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