GB678807A - Process for the production of titanium metal - Google Patents
Process for the production of titanium metalInfo
- Publication number
- GB678807A GB678807A GB11126/51A GB1112651A GB678807A GB 678807 A GB678807 A GB 678807A GB 11126/51 A GB11126/51 A GB 11126/51A GB 1112651 A GB1112651 A GB 1112651A GB 678807 A GB678807 A GB 678807A
- Authority
- GB
- United Kingdom
- Prior art keywords
- electrolyte
- cathode
- titanium
- fused
- production
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 title abstract 3
- 238000000034 method Methods 0.000 title abstract 3
- 239000010936 titanium Substances 0.000 title abstract 3
- 229910052719 titanium Inorganic materials 0.000 title abstract 3
- 229910052751 metal Inorganic materials 0.000 title 1
- 239000002184 metal Substances 0.000 title 1
- 239000003792 electrolyte Substances 0.000 abstract 4
- XJDNKRIXUMDJCW-UHFFFAOYSA-J titanium tetrachloride Chemical compound Cl[Ti](Cl)(Cl)Cl XJDNKRIXUMDJCW-UHFFFAOYSA-J 0.000 abstract 2
- KPZGRMZPZLOPBS-UHFFFAOYSA-N 1,3-dichloro-2,2-bis(chloromethyl)propane Chemical compound ClCC(CCl)(CCl)CCl KPZGRMZPZLOPBS-UHFFFAOYSA-N 0.000 abstract 1
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 abstract 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 abstract 1
- TWRXJAOTZQYOKJ-UHFFFAOYSA-L Magnesium chloride Chemical class [Mg+2].[Cl-].[Cl-] TWRXJAOTZQYOKJ-UHFFFAOYSA-L 0.000 abstract 1
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 abstract 1
- 239000011575 calcium Substances 0.000 abstract 1
- 229910052791 calcium Inorganic materials 0.000 abstract 1
- 235000011148 calcium chloride Nutrition 0.000 abstract 1
- 150000001805 chlorine compounds Chemical class 0.000 abstract 1
- 230000005611 electricity Effects 0.000 abstract 1
- 238000005868 electrolysis reaction Methods 0.000 abstract 1
- 239000011876 fused mixture Substances 0.000 abstract 1
- 235000011147 magnesium chloride Nutrition 0.000 abstract 1
- 239000011591 potassium Substances 0.000 abstract 1
- 229910052700 potassium Inorganic materials 0.000 abstract 1
- 235000011164 potassium chloride Nutrition 0.000 abstract 1
- 239000011734 sodium Substances 0.000 abstract 1
- 229910052708 sodium Inorganic materials 0.000 abstract 1
- 235000002639 sodium chloride Nutrition 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25C—PROCESSES FOR THE ELECTROLYTIC PRODUCTION, RECOVERY OR REFINING OF METALS; APPARATUS THEREFOR
- C25C7/00—Constructional parts, or assemblies thereof, of cells; Servicing or operating of cells
- C25C7/005—Constructional parts, or assemblies thereof, of cells; Servicing or operating of cells of cells for the electrolysis of melts
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25C—PROCESSES FOR THE ELECTROLYTIC PRODUCTION, RECOVERY OR REFINING OF METALS; APPARATUS THEREFOR
- C25C3/00—Electrolytic production, recovery or refining of metals by electrolysis of melts
- C25C3/26—Electrolytic production, recovery or refining of metals by electrolysis of melts of titanium, zirconium, hafnium, tantalum or vanadium
- C25C3/28—Electrolytic production, recovery or refining of metals by electrolysis of melts of titanium, zirconium, hafnium, tantalum or vanadium of titanium
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Electrochemistry (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Electrolytic Production Of Metals (AREA)
Abstract
678,807. Electrolytic production of titanium. SHAWINIGAN WATER & POWER CO. May 11, 1951 [May 12, 1950], No. 11126/51. Class 41. A process for the production of metallic titanium comprises electrolysing a fused mixture containing one or more chlorides of the group consisting of sodium, potassium, calcium, and magnesium chlorides, together with titanium tetrachloride in an amount less than the electrochemical equivalent of the amount of electricity used, while maintaining the titanium tetrachloride and the cathodic electrolysis products isolated from the atmosphere. The process may be carried out in the apparatus shown which comprises a circular cell with a refractory lining 1, an annular anode 2, a circular cathode 3, a fused electrolyte 4, a metallic bell 5 electrically insulated from the cathode, a metallic screen 6 between the anode and cathode, and means 7 for introducing tetrachloride to the space above the cathode electrolyte. The electrolyte may be fused by alternating current the electrodes being immersed in the electrolyte.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US678807XA | 1950-05-12 | 1950-05-12 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB678807A true GB678807A (en) | 1952-09-10 |
Family
ID=22079025
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB11126/51A Expired GB678807A (en) | 1950-05-12 | 1951-05-11 | Process for the production of titanium metal |
Country Status (1)
| Country | Link |
|---|---|
| GB (1) | GB678807A (en) |
Cited By (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2731404A (en) * | 1952-10-29 | 1956-01-17 | Horizons Titanium Corp | Production of titanium metal |
| US2789943A (en) * | 1955-05-05 | 1957-04-23 | New Jersey Zinc Co | Production of titanium |
| DE1016452B (en) * | 1952-09-29 | 1957-09-26 | Bayer Ag | Process for the production of titanium |
| US2936269A (en) * | 1956-10-18 | 1960-05-10 | Nat Lead Co | Method for electrolytic production of refractory metal |
| DE1086051B (en) * | 1956-12-17 | 1960-07-28 | New Jersey Zinc Co | Process and device for the extraction of titanium of high purity |
| DE1096617B (en) * | 1954-07-06 | 1961-01-05 | New Jersey Zinc Co | Process for the electrolytic production of titanium |
| DE1108923B (en) * | 1954-11-10 | 1961-06-15 | Norton Ges M B H Deutsche | Process and device for the production of titanium by fused-salt electrolysis |
| DE1128990B (en) * | 1955-11-29 | 1962-05-03 | New Jersey Zinc Co | Device and electrolytic cell for the production of titanium by fused-salt electrolysis |
| DE1202989B (en) * | 1959-07-31 | 1965-10-14 | Lonza Ag | Process for the production of titanium by fused-salt electrolysis |
| US4116801A (en) * | 1974-10-24 | 1978-09-26 | The Dow Chemical Company | Apparatus for electrowinning multivalent metals |
| US4118291A (en) * | 1974-10-24 | 1978-10-03 | The Dow Chemical Company | Method of electrowinning titanium |
| US4165262A (en) * | 1976-09-13 | 1979-08-21 | The Dow Chemical Company | Method of electrowinning titanium |
| DE2819964A1 (en) * | 1974-10-24 | 1979-11-15 | Dow Chemical Co | DEVICE AND METHOD FOR ELECTROLYTIC EXTRACTION OF VALUED METALS |
| EP2870277A4 (en) * | 2012-07-03 | 2016-01-13 | Ceramatec Inc | APPARATUS AND METHOD FOR PRODUCING METAL IN A NASICON ELECTROLYTIC CELL |
-
1951
- 1951-05-11 GB GB11126/51A patent/GB678807A/en not_active Expired
Cited By (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1016452B (en) * | 1952-09-29 | 1957-09-26 | Bayer Ag | Process for the production of titanium |
| US2731404A (en) * | 1952-10-29 | 1956-01-17 | Horizons Titanium Corp | Production of titanium metal |
| DE1096617B (en) * | 1954-07-06 | 1961-01-05 | New Jersey Zinc Co | Process for the electrolytic production of titanium |
| DE1108923B (en) * | 1954-11-10 | 1961-06-15 | Norton Ges M B H Deutsche | Process and device for the production of titanium by fused-salt electrolysis |
| US2789943A (en) * | 1955-05-05 | 1957-04-23 | New Jersey Zinc Co | Production of titanium |
| DE1128990B (en) * | 1955-11-29 | 1962-05-03 | New Jersey Zinc Co | Device and electrolytic cell for the production of titanium by fused-salt electrolysis |
| US2936269A (en) * | 1956-10-18 | 1960-05-10 | Nat Lead Co | Method for electrolytic production of refractory metal |
| DE1086051B (en) * | 1956-12-17 | 1960-07-28 | New Jersey Zinc Co | Process and device for the extraction of titanium of high purity |
| DE1202989B (en) * | 1959-07-31 | 1965-10-14 | Lonza Ag | Process for the production of titanium by fused-salt electrolysis |
| US4116801A (en) * | 1974-10-24 | 1978-09-26 | The Dow Chemical Company | Apparatus for electrowinning multivalent metals |
| US4118291A (en) * | 1974-10-24 | 1978-10-03 | The Dow Chemical Company | Method of electrowinning titanium |
| DE2819964A1 (en) * | 1974-10-24 | 1979-11-15 | Dow Chemical Co | DEVICE AND METHOD FOR ELECTROLYTIC EXTRACTION OF VALUED METALS |
| US4165262A (en) * | 1976-09-13 | 1979-08-21 | The Dow Chemical Company | Method of electrowinning titanium |
| EP2870277A4 (en) * | 2012-07-03 | 2016-01-13 | Ceramatec Inc | APPARATUS AND METHOD FOR PRODUCING METAL IN A NASICON ELECTROLYTIC CELL |
| US9856569B2 (en) | 2012-07-03 | 2018-01-02 | Field Upgrading Limited | Apparatus and method of producing metal in a nasicon electrolytic cell |
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