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GB2354519B - Production of porous ceramic articles - Google Patents

Production of porous ceramic articles

Info

Publication number
GB2354519B
GB2354519B GB0100085A GB0100085A GB2354519B GB 2354519 B GB2354519 B GB 2354519B GB 0100085 A GB0100085 A GB 0100085A GB 0100085 A GB0100085 A GB 0100085A GB 2354519 B GB2354519 B GB 2354519B
Authority
GB
United Kingdom
Prior art keywords
particles
article
dispersion
remove
liquid carrier
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
GB0100085A
Other versions
GB2354519A (en
GB2354519A8 (en
GB0100085D0 (en
Inventor
Robert Terence Smith
Rodney Martin Sambrook
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Dytech Corp Ltd
Original Assignee
Dytech Corp Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Dytech Corp Ltd filed Critical Dytech Corp Ltd
Priority to GB0100085A priority Critical patent/GB2354519B/en
Publication of GB0100085D0 publication Critical patent/GB0100085D0/en
Publication of GB2354519A publication Critical patent/GB2354519A/en
Application granted granted Critical
Publication of GB2354519B publication Critical patent/GB2354519B/en
Publication of GB2354519A8 publication Critical patent/GB2354519A8/en
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B38/00Porous mortars, concrete, artificial stone or ceramic ware; Preparation thereof
    • C04B38/0038Porous mortars, concrete, artificial stone or ceramic ware; Preparation thereof by superficial sintering or bonding of particulate matter
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61LMETHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L27/00Materials for grafts or prostheses or for coating grafts or prostheses
    • A61L27/02Inorganic materials
    • A61L27/12Phosphorus-containing materials, e.g. apatite
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B38/00Porous mortars, concrete, artificial stone or ceramic ware; Preparation thereof
    • C04B38/06Porous mortars, concrete, artificial stone or ceramic ware; Preparation thereof by burning-out added substances by burning natural expanding materials or by sublimating or melting out added substances
    • C04B38/0615Porous mortars, concrete, artificial stone or ceramic ware; Preparation thereof by burning-out added substances by burning natural expanding materials or by sublimating or melting out added substances the burned-out substance being a monolitic element having approximately the same dimensions as the final article, e.g. a porous polyurethane sheet or a prepreg obtained by bonding together resin particles
    • C04B38/062Porous mortars, concrete, artificial stone or ceramic ware; Preparation thereof by burning-out added substances by burning natural expanding materials or by sublimating or melting out added substances the burned-out substance being a monolitic element having approximately the same dimensions as the final article, e.g. a porous polyurethane sheet or a prepreg obtained by bonding together resin particles the burned-out substance being formed in situ, e.g. by polymerisation of a prepolymer composition containing ceramic powder
    • C04B38/0625Porous mortars, concrete, artificial stone or ceramic ware; Preparation thereof by burning-out added substances by burning natural expanding materials or by sublimating or melting out added substances the burned-out substance being a monolitic element having approximately the same dimensions as the final article, e.g. a porous polyurethane sheet or a prepreg obtained by bonding together resin particles the burned-out substance being formed in situ, e.g. by polymerisation of a prepolymer composition containing ceramic powder involving a foaming step of the burnable material
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61FFILTERS IMPLANTABLE INTO BLOOD VESSELS; PROSTHESES; DEVICES PROVIDING PATENCY TO, OR PREVENTING COLLAPSING OF, TUBULAR STRUCTURES OF THE BODY, e.g. STENTS; ORTHOPAEDIC, NURSING OR CONTRACEPTIVE DEVICES; FOMENTATION; TREATMENT OR PROTECTION OF EYES OR EARS; BANDAGES, DRESSINGS OR ABSORBENT PADS; FIRST-AID KITS
    • A61F2310/00Prostheses classified in A61F2/28 or A61F2/30 - A61F2/44 being constructed from or coated with a particular material
    • A61F2310/00005The prosthesis being constructed from a particular material
    • A61F2310/00179Ceramics or ceramic-like structures
    • A61F2310/00293Ceramics or ceramic-like structures containing a phosphorus-containing compound, e.g. apatite
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2111/00Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
    • C04B2111/00474Uses not provided for elsewhere in C04B2111/00
    • C04B2111/00836Uses not provided for elsewhere in C04B2111/00 for medical or dental applications

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Ceramic Engineering (AREA)
  • Health & Medical Sciences (AREA)
  • Materials Engineering (AREA)
  • Structural Engineering (AREA)
  • Organic Chemistry (AREA)
  • Oral & Maxillofacial Surgery (AREA)
  • Animal Behavior & Ethology (AREA)
  • Medicinal Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Transplantation (AREA)
  • Epidemiology (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Dermatology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Materials For Medical Uses (AREA)
  • Manufacture Of Porous Articles, And Recovery And Treatment Of Waste Products (AREA)
  • Porous Artificial Stone Or Porous Ceramic Products (AREA)

Abstract

A method of making a porous article composed of bonded particles and having a controlled level of porosity, pore size and interconnectivity comprises the steps of: <SL> <LI>a) forming a dispersion comprising a liquid carrier, the particles to be bonded and a polymerisable monomeric material; <LI>b) introducing small bubbles of oxygen containing gas into the dispersion with agitation to form a foam which is allowed to caused to coalesce; <LI>c) adjusting the concentration of oxygen within the foaming gas to control the onset of polymerisation, then <LI>d) polymerising the foamed structure; <LI>e) drying the structure to remove the liquid carrier and provide a solid article having pores derived from the bubbles, and <LI>f) firing the article to remove the organic binder and provide a ceramic bond. </SL> The particles may be of hydroxyapatite, which gives a product used in bone cell culture, or for carrying drugs.
GB0100085A 1996-10-04 1996-10-04 Production of porous ceramic articles Expired - Lifetime GB2354519B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
GB0100085A GB2354519B (en) 1996-10-04 1996-10-04 Production of porous ceramic articles

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
GB0100085A GB2354519B (en) 1996-10-04 1996-10-04 Production of porous ceramic articles
GB9620752A GB2317887A (en) 1996-10-04 1996-10-04 Porous ceramic articles; bone cell growth and drug carriers

Publications (4)

Publication Number Publication Date
GB0100085D0 GB0100085D0 (en) 2001-02-14
GB2354519A GB2354519A (en) 2001-03-28
GB2354519B true GB2354519B (en) 2001-06-13
GB2354519A8 GB2354519A8 (en) 2001-07-19

Family

ID=10800966

Family Applications (3)

Application Number Title Priority Date Filing Date
GB0100085A Expired - Lifetime GB2354519B (en) 1996-10-04 1996-10-04 Production of porous ceramic articles
GB0100084A Expired - Lifetime GB2354518B (en) 1996-10-04 1996-10-04 A porous ceramic body composed of bonded particles
GB9620752A Withdrawn GB2317887A (en) 1996-10-04 1996-10-04 Porous ceramic articles; bone cell growth and drug carriers

Family Applications After (2)

Application Number Title Priority Date Filing Date
GB0100084A Expired - Lifetime GB2354518B (en) 1996-10-04 1996-10-04 A porous ceramic body composed of bonded particles
GB9620752A Withdrawn GB2317887A (en) 1996-10-04 1996-10-04 Porous ceramic articles; bone cell growth and drug carriers

Country Status (5)

Country Link
EP (1) EP0958261A1 (en)
JP (1) JP2001501902A (en)
AU (1) AU4563997A (en)
GB (3) GB2354519B (en)
WO (1) WO1998015505A1 (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109512678A (en) * 2018-11-28 2019-03-26 福建工程学院 A kind of artificial tooth film layer preparation method

Families Citing this family (25)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE19718672C1 (en) * 1997-05-02 1998-09-24 Zschimmer & Schwarz Gmbh & Co Use of a sugar
GB9821663D0 (en) 1998-10-05 1998-11-25 Abonetics Ltd Foamed ceramics
GB9825109D0 (en) * 1998-11-16 1999-01-13 Dytech Corp Ltd Porous ceramic matrices
JP3400740B2 (en) 1999-04-13 2003-04-28 東芝セラミックス株式会社 Calcium phosphate porous sintered body and method for producing the same
US6833486B1 (en) * 1999-05-12 2004-12-21 D & E Cryo Cc Ceramic wound treatment device
EP1108698B8 (en) * 1999-12-16 2006-10-04 IsoTis N.V. Porous ceramic body
AU778651B2 (en) 1999-12-16 2004-12-16 Isotis N.V. Porous ceramic body
US20020022885A1 (en) * 2000-05-19 2002-02-21 Takahiro Ochi Biomaterial
GB0019003D0 (en) * 2000-08-04 2000-09-20 Lo Wei Jen Porous synthetic bone graft and method of manufacture thereof
GB0020610D0 (en) * 2000-08-21 2000-10-11 Dytech Corp Ltd Uses of porous carriers
GB0020734D0 (en) * 2000-08-22 2000-10-11 Dytech Corp Ltd Bicontinuous composites
US6713420B2 (en) 2000-10-13 2004-03-30 Toshiba Ceramics Co., Ltd. Porous ceramics body for in vivo or in vitro use
JP4070951B2 (en) 2000-12-07 2008-04-02 ペンタックス株式会社 Method for producing porous calcium phosphate ceramic sintered body
WO2002049978A1 (en) * 2000-12-21 2002-06-27 Corning Incorporated Refractories for fused silica production furnaces
US6949251B2 (en) 2001-03-02 2005-09-27 Stryker Corporation Porous β-tricalcium phosphate granules for regeneration of bone tissue
DE10113108B4 (en) * 2001-03-15 2007-07-26 Dot Gmbh Active substance-containing calcium phosphate materials
DE60215895T2 (en) 2001-09-13 2007-05-31 Akira Myoi, Toyonaka Porous calcium phosphate ceramic for in vivo applications
AU2003256227A1 (en) * 2002-07-30 2004-02-16 Nanyang Technological University Spherical nano-composite powder and a method of preparing the same
DE10328892A1 (en) 2003-06-26 2005-05-12 Curasan Ag Bone building agent and manufacturing process
JP4215595B2 (en) * 2003-08-21 2009-01-28 安正 赤川 Implant fixing member and implant composite material
WO2007086964A2 (en) 2005-10-21 2007-08-02 University Of South Florida Method of producing interconnected volumetric porosity in materials
EP2192876B1 (en) 2007-08-09 2014-03-26 The Board of Regents of The University of Texas System Bi-layered bone-like scaffolds
US8044105B2 (en) 2008-02-04 2011-10-25 Dow Global Technologies Llc Water-based ceramic foams showing improved gel strength
DK2569342T3 (en) 2010-05-11 2022-04-19 Howmedica Osteonics Corp Multivalent Organophosphorus Metal Compounds and Interpenetrating Polymer Adhesive Network Compositions and Methods
WO2012158527A2 (en) 2011-05-13 2012-11-22 Howmedica Osteonics Organophosphorous & multivalent metal compound compositions & methods

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO1993004013A1 (en) * 1991-08-12 1993-03-04 Dytech Corporation Limited Porous articles
GB2289466A (en) * 1994-05-10 1995-11-22 Dytech Corp Ltd Porous ceramic articles

Family Cites Families (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3537947A (en) * 1967-05-18 1970-11-03 Uniroyal Inc Leather-like poromeric material and method for making the same
US4218255A (en) * 1976-08-30 1980-08-19 University Of Dayton Porous ceramic carriers for controlled release of proteins, polypeptide hormones, and other substances within human and/or other mamillian species and method
JPS56145153A (en) * 1980-03-05 1981-11-11 Toyo Tire & Rubber Co Manufacture of porous ceramic moldings
JPS56166843A (en) * 1980-05-28 1981-12-22 Mitsubishi Mining & Cement Co Filler for bone broken section and void section
DK154260C (en) * 1981-02-20 1989-05-22 Mundipharma Gmbh PROCEDURE FOR THE MANUFACTURING OF A BONE IMPLANT OF FURNISHED TRICAL CUMPHOSPHATE, SPECIFICALLY FOR FILLING OF SPACES OR FOR COMPOSITION OF BONE PARTS AFTER FRACTURE.
US4654314A (en) * 1983-07-09 1987-03-31 Sumitomo Cement Co., Ltd. Porous ceramic material and processes for preparing same
JPS6021763A (en) * 1983-07-15 1985-02-04 ティーディーケイ株式会社 Artificial bone material
US4629464A (en) * 1984-09-25 1986-12-16 Tdk Corporation Porous hydroxyapatite material for artificial bone substitute
US5011495A (en) * 1990-02-16 1991-04-30 The United States Of America As Represented By The Secretary Of The Army Unique bone regeneration tricalcium phosphate
DE4313715A1 (en) * 1993-04-27 1994-11-03 Roehm Gmbh Highly filled, foamed polymer material
GB9409258D0 (en) * 1994-05-10 1994-06-29 Dytech Corp Ltd Production of ceramic articles

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO1993004013A1 (en) * 1991-08-12 1993-03-04 Dytech Corporation Limited Porous articles
GB2289466A (en) * 1994-05-10 1995-11-22 Dytech Corp Ltd Porous ceramic articles

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109512678A (en) * 2018-11-28 2019-03-26 福建工程学院 A kind of artificial tooth film layer preparation method

Also Published As

Publication number Publication date
GB0100084D0 (en) 2001-02-14
GB2354519A (en) 2001-03-28
AU4563997A (en) 1998-05-05
JP2001501902A (en) 2001-02-13
WO1998015505A1 (en) 1998-04-16
GB2354519A8 (en) 2001-07-19
GB0100085D0 (en) 2001-02-14
GB9620752D0 (en) 1996-11-20
GB2317887A (en) 1998-04-08
GB2354518B (en) 2001-06-13
GB2354518A (en) 2001-03-28
EP0958261A1 (en) 1999-11-24

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