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GB2118193A - Polycarbonate-based thermoplastic polymer blends - Google Patents

Polycarbonate-based thermoplastic polymer blends Download PDF

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Publication number
GB2118193A
GB2118193A GB08306970A GB8306970A GB2118193A GB 2118193 A GB2118193 A GB 2118193A GB 08306970 A GB08306970 A GB 08306970A GB 8306970 A GB8306970 A GB 8306970A GB 2118193 A GB2118193 A GB 2118193A
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United Kingdom
Prior art keywords
polycarbonate
thermoplastic polymer
polymer blend
polymer blends
component
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GB08306970A
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GB2118193B (en
GB8306970D0 (en
Inventor
Aldo Brancaccio
Angelo Rovella
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Publication of GB2118193B publication Critical patent/GB2118193B/en
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    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L69/00Compositions of polycarbonates; Compositions of derivatives of polycarbonates

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  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Compositions Of Macromolecular Compounds (AREA)

Abstract

Thermoplastic polymer blends are prepared by mixing together an aromatic polycarbonate, one or more polyterephthalates derived from the condensation of terephthalic acid with a glycol of formula HO-(CH2)n-OH where n is from 2 to 10, and an olefin elastomer. The materials thus obtained have a high impact strength even at low temperature, a good solvent resistance, and a better processability than polycarbonate.

Description

SPECIFICATION Polycarbonate-based thermoplastic polymer blends Polycarbonate is a resin known to possess exceptional mechanical characteristics, particularly in terms of impact strength, but it has certain defects which prevent its use in many large-consumption applications, the main defects being a substantial brittling beyond a certain critical thickness, a very low resistance to many organic solvents, and a poor impact strength at low temperature.
These defects have greatly limited the use of polycarbonate in one field, namely the automobile field, which requires materials of outstanding mechanical properties and of excellent resistance to those agents (petrol, lubricants, detergents, etc.) which habitually or accidentally come into contact with the polycarbonate during its operational iife.
The prior art describes examples of blends prepared by mixing a polycarbonate with a polyester (AU-55998, US-41 88314, US-3494885), or by mixing together a polycarbonate, a polyolefin and a third component such as an acrylic polymer (US-4245058), a hydrogenated block copolymer (US-41 22131), or an epoxidisable polydiene (G8-1 149695). The prior art also describes a thermoplastic polymer blend (GB1007724) comprising at least 50% by weight of polycarbonate and not more than 50% of an olefin polymer which can be partially substituted by a polyester resin, such that the weight ratio of the olefin polymer to the polyester is always greater than unity.However, because of the substantial plasticising effect which polyolefins have on polycarbonate, this blend has a rather low load distortion temperature, this being a limiting characteristic for many applications, including the automobile field.
We have now surprisingly found, in accordance with the present invention, that it is possible to prepare materials with improved thermal properties by suitably mixing together an aromatic polycarbonate such as bisphenol A polycarbonate, one or more thermoplastic polyesters prepared by condensing terephthalic acid with a glycol such as one of general formula HO(CH2)nOH wherein n is from 2 to 10, and an olefin elastomer in such quantities that the weight ratio of the olefin elastomer to the thermoplastic polyester is less than or equal to 1.
Although the materials obtained have an impact strength which is very close to that of polycarbonate, compared with the latter they have an excellent solvent resistance, a low sensitivity with respect to thickness, and an improved impact strength at low temperature, and are easier to mould.
These polymer blends and the products obtained from them demonstrate physical, chemical and electrical characteristics which overall are better than those of polycarbonate when used either as such or in mixtures as described in the aforesaid patents.
The present invention includes a thermoplastic polymer blend, and a material obtained from it, comprising at least one compound chosen from the following classes: (a) a bisphenol A polycarbonate; (b) one or more polyalkyleneterephthalates whose alkylene radical has from 2 to 10 carbon atoms; and (c) a modifier which modifies the impact energy absorption mechanism, which is selected from (i) a C2 or C3 polyolefin, (ii) a C2-C3 olefin copolymer (preferably of ethylene-propylene rubber type or of ethylene-propylene-diene monomer terpolymer type), (iii) a mixture of (i) and (ii), (iv) a mixture of (i) and a copolymer of polyethylenevinylacetate type, and (v) a mixture of (i) and (ii) with a copolymer of polyethylenevinylacetate type.
The quantity of component (a) is preferably from 5 to 95% by weight, the quantity of components (b) and (c) is preferably from 5 to 95% by weight, and the weight ratio of component (c) to component (b) is less than or equal to 1.
The polycarbonate used is preferably one having an intrinsic viscosity in methylene chloride at 200C of from 0.46 to 1.2 dl/g, The modifier used can be either a simple polyethylene or polypropylene, or a copolymer of two or more olefins such as an ethylene-propylene copolymer or an ethylene-propylene-diene copolymer, or a mixture of these with a copolymer of polyethylenevinylacetate type.
Although not essential, best results are obtained by carrying out one or more premixing operations on the components, then reducing the resulting blend to granules, and then moulding the blend. The apparatus used for mixing is of no special importance. Thus single screw extruders, double screw extruders, Banbury mixers and all machinery normally used in industrial practice are suitable for this purpose.
The thermoplastic polymer blend of the present invention can be-in various forms such as in the form of powder, granules, spheres, discoids or other forms, prepared for example either by extrusion or by injection.
The blend can contain various additives such as stabilisers, dyes, flame retarders, lubricants, and fillers (e.g. glass fibre, carbon fibre, asbestos fibre and glass wool).
The invention will now be illustrated by the following Examples.
EXAMPLES 1-77 Polymer blends 1 to 77, whose compositions are given in the following Tables 1 to 10, were prepared. The component granules of each blend were dried and mixed, and extruded in a single screw extruder at a temperature of 2750 C. The polymer blend obtained in this manner was then granulated and injection-moulded at a temperature of from 260 to 2800C, depending upon the composition, the mould temperature being 600 C. The following tests were carried out on the products obtained; (a) Izod notched bar impact test (ASTM D 256-61); (b) Vicat softening point at 5 kg (ASTM D 1525-72); (c) Modulus of elasticity in bending (ASTM D 790-70);; (d) Stress cracking test, i.e. at test wherein tension is applied in accordance with ASTM D 638 to samples which had been previously subjected to 0.7% tensile deformation and immersed for 2 hours in a1 :1 (volumetric) mixture of toluene and isooctane to which 15% of methyl alcohol had been added, the percentage retention of the ultimate tensile stress of the non-immersed sample then being measured.
The results obtained are given in the following Tables 1 to 10.
TABLE 1 Composition 1 2 3 4 5 6 7 8 9 PC 100 90 75 60 60 60 50 50 50 PET - 5 15 35 30 20 45 40 25 EPR - 5 10 5 10 20 5 10 25 Degrees Vicat 155 147 135 137 123 105 125 112 94 5 kg ( C) IZOD Impact, Notched 90 59 63 67 78 81 51 54 62 (kg cm/cm) Mod. Elasticity 23000 21700 19700 22300 20000 15300 22800 20300 13300 In Bending (kg/cm) % Ult. Tensile Stress - 63 78 92 94 91 90 91 89 Retention After 120 min.
Immersion TABLE 2 Composition 10 11 12 13 14 15 16 17 18 PC 100 75 75 60 60 60 50 50 50 PET - 20 15 35 30 20 45 40 25 EPDM - 5 10 5 10 20 5 10 25 Degrees Vicat 155 146 133 133 121 105 121 109 90 5 kg ( C) IZOD Impact, Notched 90 70 75 82 91 98 58 63 75 (kg cm/cm) Mod. Elasticity 23000 21800 19500 22500 20100 15100 23000 20500 13200 In Bending (kg/cm) % Ult. Tensile Stress - 65 79 90 96 93 93 94 87 Retention After 120 min.
Immersion TABLE 3 Composition 19 20 21 22 23 24 25 26 27 28 29 30 PC 100 75 75 60 60 60 50 50 50 40 40 40 PBT - 20 25 35 30 20 45 40 25 55 50 30 EPDM - 5 10 5 10 20 5 10 25 10 10 30 Degrees Vicat 155 135 121 133 124 115 131 122 108 138 127 107 5 kg( C) IZOD Impact, Notched 90 58 72 29 87 95 76 82 91 47 53 62 (kg cm/cm) Mod. Elasticity 23000 22900 20200 24000 21300 15700 24300 21700 13600 24200 21800 11300 In Bending (kg/cm) % Ulit. Tensile Stress - 75 78 80 83 77 82 84 79 87 90 88 Retention After 120 min.
Immersion TABLE 4 Composition 31 32 33 34 35 36 37 38 39 40 41 42 PC 100 75 75 60 60 60 50 50 50 40 40 40 PBT - 20 15 35 30 20 45 40 25 55 50 30 EPR - 5 10 5 10 20 5 10 25 5 10 30 Degrees Vicat 155 136 123 134 126 114 135 121 135 135 127 109 5 kg( C) IZOD Impact, Notched 90 52 65 73 78 81 71 79 84 40 45 61 (kg cm/cm) Mod. Elasticity 23000 22700 20100 24100 21300 16000 23900 21500 13700 23100 21500 11700 In Bending (kg/cm) % Ult. Tensile Stress - 73 77 81 82 79 80 86 82 85 88 84 Retention After 120 min.
Immersion TABLE 5 Composition 43 44 45 46 PC 100 75 60 50 PET - 20 35 40 PP - 5 5 10 DegreesVicat 155 143 140 115 5 kg( C) IZOD Impact, Notched 90 68 63 51 (kg cm/cm) Mod. Elasticity 23000 22100 21500 20600 In Bending (kg/cm2) % Ult. Tensile Stress - 75 85 89 Retention After 120 min.
Immersion TABLE 6 Composition 47 48 49 PC 100 60 50 PET - 35 40 PE - 5 10 DegreesVicat 155 141 114 5 kg( C) IZOD Impact, Notched 90 .67 53 (kg cm/cm) Mod. Elasticity 23000 22000 20200 In Bending (kg/cm2) % Ult. Tensile Stress - 87 91 Retention After 120 min.
Immersion TABLE 7 Composition 50 51 52 PC 100 60 50 PBT - 35 40 PP - 5 10 DegreesVicat 155 138 124 5 kg( C) IZOD Impact, Notched 90 72 70 (kg cm/cm) Mod. Elasticity 23000 23700 21900 In Bending (kg/cm2) % Ult. Tensile Stress - 84 85 Retention After 120 min.
Immersion TABLE 8 Composition 53 54 55 PC 100 60 50 PBT - 35 40 PE - 5 10 Degrees Vicat 155 135 123 5 kg( C) IZOD Impact, Notched 90 76 71 (kg cm/cm) Mod. Elasticity 23000 23500 21500 In Bending (kg/cm2) % Ult. Tensile Stress - 87 89 Retention After 120 min.
Immersion TABLE 9 Composition 56 57 58 59 60 61 62 63 64 65 66 PC 80 50 80 50 80 50 80 50 50 50 60 PBT 10 40 10 10 40 40 PET 10 40 10 40 30 EPDM 5 5 5 5 5 5 5 5 EPR PE 5 5 5 5 5 5 PP 5 5 5 5 5 EVA 5 5 5 Degrees Vicat 135 130 132 118 133 131 130 120 132 130 133 5 kg( C) IZOD Impact, Notched 63 71 54 59 60 65 53 58 62 58 66 (kg cm/cm) Mod. Elasticity 21500 20100 21200 20300 22000 21300 21400 20700 20500 20700 19800 In Bending (kg/cm) % Ult. Tensile Stress 70 83 76 90 68 81 75 93 86 83 88 Retention After 120 min.
Immersion TABLE 10 Composition 67 68 69 70 71 72 73 74 75 76 77 PC 60 50 50 50 60 60 60 50 50 50 60 PBT 40 40 40 40 40 PET 30 30 30 30 30 30 EPDM 2.5 2.5 2.5 2.5 EPR 5 5 5 5 5 5 2.5 2.5 2.5 2.5 PE 5 5 2.5 2.5 PP 5 5 5 2.5 2.5 EVA 5 5 5 2.5 2.5 2.5 2.5 Degrees Vicat 131 128 129 126 126 127 124 130 129 127 128 5 kg( C) IZOD Impact, Notched 57 67 65 56 66 61 57 69 66 71 73 (kg cm/cm) Mod. Elasticity 20100 20400 20600 19900 20200 20300 19600 20700 20600 20200 20400 In Bending (kg/cm) % Ult. Tensile Stress 91 83 80 83 93 91 89 86 84 93 93 Retention After 120 min.
Immersion ABBREVIATIONS PC polycarbonate PET polyethyleneterephthalate EPR ethylene-propylene rubber EPDM ethylene-propylene-diene monomer terpolymer PBT polybutyleneterephthalate PP polypropylene PE polyethylene EVA ethylene-vinylacetate copolymer

Claims (4)

1. A thermoplastic polymer blend comprising (a) a bisphenol A polycarbonate; (b) one or more polyalkyleneterephthalates whose alkylene radical contains from 2 to 10 carbon atoms; (c) an impact energy absorption modifier selected from (i) a C2 or C3 polyolefin, (ii) a C2-C3 olefin copolymer, (iii) a mixture of (i) and (ii), and (iv) a mixture of (i) and/or (ii) with a copolymer of polyethylenevinylacetate type; the weight ratio of component (c) to component (b) being less than or equal to 1.
2. A thermoplastic polymer blend as claimed in claim 1, wherein the quantity of component (a) present is from 5 to 95% by weight.
3. A thermoplastic polymer blend as claimed in claim 1 or 2, wherein the quantity of components (b) and (c) present is from 5 to 95% by weight.
4. A thermoplastic polymer blend, substantially as described in any of the foregoing Examples 2 to 9,11 to 18,20to30,32to42,44to46,48and49,51 and 52, and 54to 77.
GB08306970A 1982-03-26 1983-03-14 Polycarbonate-based thermoplastic polymer blends Expired GB2118193B (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
IT20406/82A IT1199982B (en) 1982-03-26 1982-03-26 POLYCARBONATE-BASED THERMOPLASTIC POLYMERIC ALLOY

Publications (3)

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GB8306970D0 GB8306970D0 (en) 1983-04-20
GB2118193A true GB2118193A (en) 1983-10-26
GB2118193B GB2118193B (en) 1986-01-15

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GB08306970A Expired GB2118193B (en) 1982-03-26 1983-03-14 Polycarbonate-based thermoplastic polymer blends

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JP (1) JPS58176241A (en)
AT (1) AT381113B (en)
BE (1) BE896271A (en)
CA (1) CA1196136A (en)
CH (1) CH653045A5 (en)
DE (1) DE3310754A1 (en)
DK (1) DK132383A (en)
ES (1) ES8405051A1 (en)
FR (1) FR2523990B1 (en)
GB (1) GB2118193B (en)
IE (1) IE54381B1 (en)
IT (1) IT1199982B (en)
NL (1) NL185672C (en)
NO (1) NO166044C (en)
SE (1) SE461736B (en)
ZA (1) ZA831660B (en)

Cited By (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0115015A1 (en) * 1983-01-03 1984-08-08 General Electric Company Linear low density polyethylene impact modifier for thermoplastic polyesters
EP0166889A1 (en) * 1984-05-04 1986-01-08 Bayer Ag Polycarbonate and polyalkylene terephthalate moulding materials
EP0187992A1 (en) * 1985-01-02 1986-07-23 General Electric Company Polycarbonate composition
US4764556A (en) * 1986-05-21 1988-08-16 Basf Aktiengesellschaft Thermoplastic molding materials of polyester and polycarbonate
US4791158A (en) * 1986-08-09 1988-12-13 Basf Aktiengesellschaft Thermoplastic molding materials containing a polyester and a polycarbonate
EP0272857A3 (en) * 1986-12-23 1989-10-18 Advanced Elastomer Systems, L.P. Polycarbonate compositions
EP0308179A3 (en) * 1987-09-17 1990-05-09 Tonen Sekiyukagaku K.K. Thermoplastic resin composition
EP0369734A3 (en) * 1988-11-14 1992-01-22 Amoco Corporation Improving the thermal properties of a polyalkyleneterephthalate without significant loss of physical and low temperature properties
US5302429A (en) * 1989-08-04 1994-04-12 Rohm And Haas Company Thermoplastic polymer compositions containing high molecular weight poly(vinyl aromatic) melt-rheology modifiers

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4587295A (en) * 1985-01-02 1986-05-06 General Electric Company Polycarbonate composition
US4895899A (en) * 1987-12-23 1990-01-23 Uniroyal Chemical Company, Inc. Impact resistant polyethylene terephthalate/polycarbonate/polyethylene graft copolymer blends

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB1007724A (en) * 1962-07-04 1965-10-22 Teijin Ltd Novel moulding material and the moulded articles obtained therefrom
GB1375670A (en) * 1971-06-21 1974-11-27
GB1375669A (en) * 1971-06-21 1974-11-27
GB1558874A (en) * 1975-12-08 1980-01-09 Gen Electric Foamed thermoplastic compositions of a linear polyester and an ionically crosslinked copolymer
GB1565959A (en) * 1975-12-08 1980-04-23 Gen Electric Thermoplastic compositions of poly(1,4-butylone)terphthalate resin and ionically crosslinked copolymers

Family Cites Families (7)

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Publication number Priority date Publication date Assignee Title
FR1368369A (en) * 1962-07-04 1964-07-31 Teijin Ltd New polymeric molding composition and molded articles obtained therefrom
JPS5726303B2 (en) * 1974-04-04 1982-06-03
JPS5139749A (en) * 1974-10-02 1976-04-02 Mitsubishi Gas Chemical Co JUGOTAISOSE IBUTSU
JPS5813588B2 (en) * 1975-02-04 1983-03-14 帝人株式会社 thermoplastic resin composition
US4226950A (en) * 1978-07-06 1980-10-07 General Electric Company Plasticized, impact modified polycarbonates
JPS5726303A (en) * 1980-07-23 1982-02-12 Mitsubishi Heavy Ind Ltd Fire furnace wall
DE3118697A1 (en) * 1981-05-12 1982-12-02 Bayer Ag, 5090 Leverkusen "THERMOPLASTIC MOLDS BASED ON POLYCARBONATE, POLYALKYLENE TEREPHTHALATE AND, IF NECESSARY, ONE OR MORE POLYMERISATES"

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB1007724A (en) * 1962-07-04 1965-10-22 Teijin Ltd Novel moulding material and the moulded articles obtained therefrom
GB1375670A (en) * 1971-06-21 1974-11-27
GB1375669A (en) * 1971-06-21 1974-11-27
GB1558874A (en) * 1975-12-08 1980-01-09 Gen Electric Foamed thermoplastic compositions of a linear polyester and an ionically crosslinked copolymer
GB1565959A (en) * 1975-12-08 1980-04-23 Gen Electric Thermoplastic compositions of poly(1,4-butylone)terphthalate resin and ionically crosslinked copolymers

Cited By (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0115015A1 (en) * 1983-01-03 1984-08-08 General Electric Company Linear low density polyethylene impact modifier for thermoplastic polyesters
EP0166889A1 (en) * 1984-05-04 1986-01-08 Bayer Ag Polycarbonate and polyalkylene terephthalate moulding materials
EP0187992A1 (en) * 1985-01-02 1986-07-23 General Electric Company Polycarbonate composition
US4764556A (en) * 1986-05-21 1988-08-16 Basf Aktiengesellschaft Thermoplastic molding materials of polyester and polycarbonate
US4791158A (en) * 1986-08-09 1988-12-13 Basf Aktiengesellschaft Thermoplastic molding materials containing a polyester and a polycarbonate
EP0272857A3 (en) * 1986-12-23 1989-10-18 Advanced Elastomer Systems, L.P. Polycarbonate compositions
US4883840A (en) * 1986-12-23 1989-11-28 Exxon Chemical Patents Inc. Elastomer modified polycarbonate compositions of improved impact strength
EP0308179A3 (en) * 1987-09-17 1990-05-09 Tonen Sekiyukagaku K.K. Thermoplastic resin composition
EP0545902A3 (en) * 1987-09-17 1993-08-18 Tonen Sekiyukagaku K.K. Thermoplastic resin composition
EP0369734A3 (en) * 1988-11-14 1992-01-22 Amoco Corporation Improving the thermal properties of a polyalkyleneterephthalate without significant loss of physical and low temperature properties
US5302429A (en) * 1989-08-04 1994-04-12 Rohm And Haas Company Thermoplastic polymer compositions containing high molecular weight poly(vinyl aromatic) melt-rheology modifiers

Also Published As

Publication number Publication date
NL8301055A (en) 1983-10-17
JPS58176241A (en) 1983-10-15
NL185672C (en) 1990-06-18
SE8301493L (en) 1983-09-27
IT8220406A0 (en) 1982-03-26
IE830675L (en) 1983-09-26
DK132383A (en) 1983-09-27
GB2118193B (en) 1986-01-15
AT381113B (en) 1986-08-25
IE54381B1 (en) 1989-09-13
NO166044B (en) 1991-02-11
CA1196136A (en) 1985-10-29
NO831023L (en) 1983-09-27
GB8306970D0 (en) 1983-04-20
DE3310754A1 (en) 1983-09-29
NL185672B (en) 1990-01-16
ES521356A0 (en) 1984-05-16
BE896271A (en) 1983-09-26
CH653045A5 (en) 1985-12-13
ZA831660B (en) 1983-12-28
SE461736B (en) 1990-03-19
DK132383D0 (en) 1983-03-23
ES8405051A1 (en) 1984-05-16
FR2523990B1 (en) 1986-10-10
IT1199982B (en) 1989-01-05
FR2523990A1 (en) 1983-09-30
NO166044C (en) 1991-05-22
SE8301493D0 (en) 1983-03-18
ATA106483A (en) 1986-01-15

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Legal Events

Date Code Title Description
732 Registration of transactions, instruments or events in the register (sect. 32/1977)
PCNP Patent ceased through non-payment of renewal fee

Effective date: 19950314