GB1526885A - Process for the preparation of polycarbonates containing aliphatically bound hydroxyl end groups - Google Patents
Process for the preparation of polycarbonates containing aliphatically bound hydroxyl end groupsInfo
- Publication number
- GB1526885A GB1526885A GB2161476A GB2161476A GB1526885A GB 1526885 A GB1526885 A GB 1526885A GB 2161476 A GB2161476 A GB 2161476A GB 2161476 A GB2161476 A GB 2161476A GB 1526885 A GB1526885 A GB 1526885A
- Authority
- GB
- United Kingdom
- Prior art keywords
- ethylene glycol
- polycarbonates
- preparation
- aliphatically bound
- end groups
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 229920000515 polycarbonate Polymers 0.000 title abstract 5
- 239000004417 polycarbonate Substances 0.000 title abstract 5
- 125000002887 hydroxy group Chemical group [H]O* 0.000 title abstract 2
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 abstract 6
- 239000004814 polyurethane Substances 0.000 abstract 2
- 229920002635 polyurethane Polymers 0.000 abstract 2
- 238000005809 transesterification reaction Methods 0.000 abstract 2
- KMTRUDSVKNLOMY-UHFFFAOYSA-N Ethylene carbonate Chemical compound O=C1OCCO1 KMTRUDSVKNLOMY-UHFFFAOYSA-N 0.000 abstract 1
- 239000003054 catalyst Substances 0.000 abstract 1
- 239000003795 chemical substances by application Substances 0.000 abstract 1
- 150000001875 compounds Chemical class 0.000 abstract 1
- 238000004508 fractional distillation Methods 0.000 abstract 1
- 239000012442 inert solvent Substances 0.000 abstract 1
- 239000000203 mixture Substances 0.000 abstract 1
- 239000005056 polyisocyanate Substances 0.000 abstract 1
- 229920001228 polyisocyanate Polymers 0.000 abstract 1
- 239000011541 reaction mixture Substances 0.000 abstract 1
- 239000002904 solvent Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G64/00—Macromolecular compounds obtained by reactions forming a carbonic ester link in the main chain of the macromolecule
- C08G64/16—Aliphatic-aromatic or araliphatic polycarbonates
- C08G64/1608—Aliphatic-aromatic or araliphatic polycarbonates saturated
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G64/00—Macromolecular compounds obtained by reactions forming a carbonic ester link in the main chain of the macromolecule
- C08G64/02—Aliphatic polycarbonates
- C08G64/0208—Aliphatic polycarbonates saturated
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G64/00—Macromolecular compounds obtained by reactions forming a carbonic ester link in the main chain of the macromolecule
- C08G64/20—General preparatory processes
- C08G64/30—General preparatory processes using carbonates
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Polyesters Or Polycarbonates (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Polyurethanes Or Polyureas (AREA)
Abstract
1526885 Polycarbonates; polyurethanes BAYER AG 25 May 1976 [27 May 1975] 21614/76 Heading C3R A polycarbonate containing aliphaticallybound OH end-groups is made by transesterifying a dihydroxyl compound (D) having aliphatically bound OH groups with ethylene glycol carbonate (C), ethylene glycol being simultaneously removed from the reaction mixture by fractional distillation, as an azeotropic mixture with an inert solvent (S) in which ethylene glycol is insoluble. Suitable solvents are listed 10-30% mol excess of (C) may be used. A transesterification catalyst may be present, many being listed. High MW polycarbonates are obtained if, after removal of (S) and any unreacted (C), some (F) still remains to be distilled off under transesterification conditions. A polyurethane may be formed by reacting a polyisocyanate with the polycarbonate.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19752523352 DE2523352A1 (en) | 1975-05-27 | 1975-05-27 | METHOD FOR PRODUCING ALIPHATIC POLYCARBONATES |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB1526885A true GB1526885A (en) | 1978-10-04 |
Family
ID=5947486
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB2161476A Expired GB1526885A (en) | 1975-05-27 | 1976-05-25 | Process for the preparation of polycarbonates containing aliphatically bound hydroxyl end groups |
Country Status (9)
| Country | Link |
|---|---|
| JP (1) | JPS51144492A (en) |
| AT (1) | AT355310B (en) |
| BE (1) | BE842196A (en) |
| BR (1) | BR7603333A (en) |
| DE (1) | DE2523352A1 (en) |
| ES (1) | ES448262A1 (en) |
| FR (1) | FR2312521A1 (en) |
| GB (1) | GB1526885A (en) |
| IT (1) | IT1061310B (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP3298065A4 (en) * | 2015-05-21 | 2019-02-27 | Basf Se | PREPARATION OF HYPERBRANCHED POLYCARBONATE POLYCARBONATE AND USE THEREOF |
Families Citing this family (24)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4131731A (en) * | 1976-11-08 | 1978-12-26 | Beatrice Foods Company | Process for preparing polycarbonates |
| JPS5556124A (en) * | 1978-10-19 | 1980-04-24 | Beatrice Foods Co | Manufacture of polycarbonate |
| JPS5564535A (en) * | 1978-11-10 | 1980-05-15 | Nisso Yuka Kogyo Kk | Separation of mixture of ethylene glycol and ethylene carbonate |
| WO1987000185A1 (en) * | 1985-07-01 | 1987-01-15 | The Dow Chemical Company | A process for increasing the molecular weight of poly(alkylene carbonate) polyols |
| JP2623550B2 (en) * | 1987-01-27 | 1997-06-25 | 東亞合成株式会社 | Method for producing polycarbonate diol |
| JPS6466236A (en) * | 1987-09-08 | 1989-03-13 | Mitsubishi Gas Chemical Co | Aliphatic polycarbonate and production thereof |
| JP2554775B2 (en) * | 1990-11-29 | 1996-11-13 | 出光石油化学株式会社 | Method for producing polycarbonate |
| EP0754714B1 (en) * | 1994-04-08 | 1999-11-03 | Asahi Kasei Kogyo Kabushiki Kaisha | Process for producing hydroxyl-terminated polycarbonate |
| EP0781792B1 (en) | 1995-12-28 | 2002-02-06 | Asahi Glass Company Ltd. | Cross-linked polyurethane resin sheet and laminated product employing it |
| WO2013076099A1 (en) | 2011-11-24 | 2013-05-30 | Bayer Intellectual Property Gmbh | Production and use of high-molecular-weight aliphatic polycarbonates |
| TWI761404B (en) | 2016-12-19 | 2022-04-21 | 德商科思創德意志股份有限公司 | Process for producing (cyclo) aliphatic polycarbonate polyols having low reactivity |
| EP3783045A1 (en) | 2019-08-19 | 2021-02-24 | Covestro Deutschland AG | Process for preparing polyether carbonate polyols |
| EP3783046A1 (en) | 2019-08-19 | 2021-02-24 | Covestro Deutschland AG | Process for preparing polyether carbonate polyols |
| EP4017900A1 (en) | 2019-08-19 | 2022-06-29 | Covestro Deutschland AG | Method for preparing polyether carbonate alcohols |
| EP4017899A1 (en) | 2019-08-19 | 2022-06-29 | Covestro Intellectual Property GmbH & Co. KG | Process for preparing polyether carbonate alcohols |
| EP3783044A1 (en) | 2019-08-19 | 2021-02-24 | Covestro Deutschland AG | Process for preparing polyether carbonate polyols |
| WO2021032555A1 (en) | 2019-08-19 | 2021-02-25 | Covestro Deutschland Ag | Process for preparing polyether carbonate alcohols |
| EP3862377A1 (en) | 2020-02-04 | 2021-08-11 | Covestro Deutschland AG | Process for producing polyether carbonate polyols |
| EP4039727A1 (en) | 2021-02-05 | 2022-08-10 | Covestro Deutschland AG | Method for the preparation of polyether carbonate alcohols |
| EP4180474A1 (en) | 2021-11-12 | 2023-05-17 | Covestro Deutschland AG | Method for the preparation of polyether carbonate alcohols |
| US20250066547A1 (en) | 2022-01-18 | 2025-02-27 | Asahi Kasei Kabushiki Kaisha | Method for producing polycarbonate diol, polycarbonate diol and transesterification catalyst |
| EP4293065B8 (en) | 2022-06-14 | 2025-11-26 | Technische Universität Berlin | Polymers containing a polyether carbonate-containing block, preparation method thereof and use of the polymers as a tenside |
| EP4378972A1 (en) | 2022-11-30 | 2024-06-05 | Covestro Deutschland AG | (cyclo)aliphatic polycarbonate polyol composition |
| DE102023000396A1 (en) | 2023-02-09 | 2024-08-14 | Covestro Deutschland Ag | Process for the preparation of polyether carbonate alcohols |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2001091A1 (en) * | 1970-01-12 | 1971-07-22 | Huels Chemische Werke Ag | Carboxylic acid alcoholysis catalysts forpro |
-
1975
- 1975-05-27 DE DE19752523352 patent/DE2523352A1/en not_active Withdrawn
-
1976
- 1976-05-25 GB GB2161476A patent/GB1526885A/en not_active Expired
- 1976-05-25 IT IT4963776A patent/IT1061310B/en active
- 1976-05-25 BE BE167310A patent/BE842196A/en unknown
- 1976-05-25 AT AT381876A patent/AT355310B/en not_active IP Right Cessation
- 1976-05-26 BR BR7603333A patent/BR7603333A/en unknown
- 1976-05-26 FR FR7616063A patent/FR2312521A1/en active Granted
- 1976-05-26 ES ES448262A patent/ES448262A1/en not_active Expired
- 1976-05-27 JP JP51060714A patent/JPS51144492A/en active Pending
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP3298065A4 (en) * | 2015-05-21 | 2019-02-27 | Basf Se | PREPARATION OF HYPERBRANCHED POLYCARBONATE POLYCARBONATE AND USE THEREOF |
Also Published As
| Publication number | Publication date |
|---|---|
| FR2312521B1 (en) | 1982-09-10 |
| FR2312521A1 (en) | 1976-12-24 |
| AT355310B (en) | 1980-02-25 |
| BR7603333A (en) | 1976-12-07 |
| IT1061310B (en) | 1983-02-28 |
| DE2523352A1 (en) | 1976-12-09 |
| BE842196A (en) | 1976-11-25 |
| ES448262A1 (en) | 1977-12-01 |
| JPS51144492A (en) | 1976-12-11 |
| ATA381876A (en) | 1979-07-15 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PS | Patent sealed | ||
| PCNP | Patent ceased through non-payment of renewal fee |