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GB1476511A - Process for the purification of mixtures of fatty acids or of their esters - Google Patents

Process for the purification of mixtures of fatty acids or of their esters

Info

Publication number
GB1476511A
GB1476511A GB3088474A GB3088474A GB1476511A GB 1476511 A GB1476511 A GB 1476511A GB 3088474 A GB3088474 A GB 3088474A GB 3088474 A GB3088474 A GB 3088474A GB 1476511 A GB1476511 A GB 1476511A
Authority
GB
United Kingdom
Prior art keywords
esters
fatty acids
purification
mixtures
montmorillonite
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB3088474A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Henkel AG and Co KGaA
Original Assignee
Henkel AG and Co KGaA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Henkel AG and Co KGaA filed Critical Henkel AG and Co KGaA
Publication of GB1476511A publication Critical patent/GB1476511A/en
Expired legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
    • C11C1/00—Preparation of fatty acids from fats, fatty oils, or waxes; Refining the fatty acids
    • C11C1/08—Refining
    • C11C1/10—Refining by distillation
    • C11C1/103—Refining by distillation after or with the addition of chemicals
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C07C51/487—Separation; Purification; Stabilisation; Use of additives by treatment giving rise to chemical modification
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/30—Preparation of carboxylic acid esters by modifying the acid moiety of the ester, such modification not being an introduction of an ester group
    • C07C67/333—Preparation of carboxylic acid esters by modifying the acid moiety of the ester, such modification not being an introduction of an ester group by isomerisation; by change of size of the carbon skeleton
    • C07C67/343—Preparation of carboxylic acid esters by modifying the acid moiety of the ester, such modification not being an introduction of an ester group by isomerisation; by change of size of the carbon skeleton by increase in the number of carbon atoms
    • C07C67/347—Preparation of carboxylic acid esters by modifying the acid moiety of the ester, such modification not being an introduction of an ester group by isomerisation; by change of size of the carbon skeleton by increase in the number of carbon atoms by addition to unsaturated carbon-to-carbon bonds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/48—Separation; Purification; Stabilisation; Use of additives
    • C07C67/52—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation
    • C07C67/54—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation by distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/48—Separation; Purification; Stabilisation; Use of additives
    • C07C67/60—Separation; Purification; Stabilisation; Use of additives by treatment giving rise to chemical modification
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B3/00—Refining fats or fatty oils
    • C11B3/001—Refining fats or fatty oils by a combination of two or more of the means hereafter

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Microbiology (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Fats And Perfumes (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

Abstract

1476511 Purification of unsaturated fatty acids or esters HENKEL & CIE GmbH 12 July 1974 [14 July 1973] 30884/74 Heading C2C Fatty acid acids or esters are purified from fractions with multiple unsaturation by heating in the presence of montmorillonite with a specific surface of more than 150 m.<SP>2</SP> per gram to 110‹ to 210‹ C., and then distilling to separate the mixture. Oleic acid or esters thereof or natural mixtures such as fatty acids of olive, palm and groundnut oil may be used. 2-25% by weight of montmorillonite may be used, and the process may be continuous. Examples describe the treatment of methyl esters of oleic acid and linoleic acid with minor amounts of saturated fatty acids (14-18 C).
GB3088474A 1973-07-14 1974-07-12 Process for the purification of mixtures of fatty acids or of their esters Expired GB1476511A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE19732335890 DE2335890C2 (en) 1973-07-14 1973-07-14 Process for the separation of polyunsaturated fractions from an oleic acid-rich natural fatty acid or ester mixture

Publications (1)

Publication Number Publication Date
GB1476511A true GB1476511A (en) 1977-06-16

Family

ID=5886912

Family Applications (1)

Application Number Title Priority Date Filing Date
GB3088474A Expired GB1476511A (en) 1973-07-14 1974-07-12 Process for the purification of mixtures of fatty acids or of their esters

Country Status (8)

Country Link
JP (1) JPS5040518A (en)
BE (1) BE817591A (en)
DE (1) DE2335890C2 (en)
ES (1) ES428247A1 (en)
FR (1) FR2236830B1 (en)
GB (1) GB1476511A (en)
IT (1) IT1015776B (en)
NL (1) NL7408005A (en)

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4277413A (en) * 1980-01-02 1981-07-07 The Procter & Gamble Company Fractionation of alkyl carboxylate mixtures
US4277412A (en) * 1980-01-02 1981-07-07 The Proctor & Gamble Company Fractionation of triglyceride mixtures
US4282164A (en) * 1980-01-02 1981-08-04 The Procter & Gamble Company Fractionation of alkylcarboxylate mixtures
US4284580A (en) * 1980-01-02 1981-08-18 The Procter & Gamble Company Fractionation of triglyceride mixture
US4948811A (en) * 1988-01-26 1990-08-14 The Procter & Gamble Company Salad/cooking oil balanced for health benefits

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE2926635A1 (en) * 1979-07-02 1981-01-15 Henkel Kgaa METHOD FOR PURIFYING FATTY ACID OR FATTY ACID ESTER MIXTURES
DE4124517A1 (en) * 1991-07-24 1993-01-28 Battelle Institut E V Sepn. of reactive fatty acids or ester(s) from their mixts. - by fractional distn. under vacuum of mixt. obtd. by saponification or transesterification of natural oil

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2482760A (en) * 1946-06-20 1949-09-27 Emery Industries Inc Purification of oleic acid
BE543588A (en) * 1954-12-13
NL285293A (en) * 1962-06-25

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4277413A (en) * 1980-01-02 1981-07-07 The Procter & Gamble Company Fractionation of alkyl carboxylate mixtures
US4277412A (en) * 1980-01-02 1981-07-07 The Proctor & Gamble Company Fractionation of triglyceride mixtures
US4282164A (en) * 1980-01-02 1981-08-04 The Procter & Gamble Company Fractionation of alkylcarboxylate mixtures
US4284580A (en) * 1980-01-02 1981-08-18 The Procter & Gamble Company Fractionation of triglyceride mixture
US4948811A (en) * 1988-01-26 1990-08-14 The Procter & Gamble Company Salad/cooking oil balanced for health benefits

Also Published As

Publication number Publication date
DE2335890A1 (en) 1975-02-06
FR2236830B1 (en) 1978-02-10
FR2236830A1 (en) 1975-02-07
ES428247A1 (en) 1976-07-16
DE2335890C2 (en) 1982-10-28
IT1015776B (en) 1977-05-20
NL7408005A (en) 1975-01-16
JPS5040518A (en) 1975-04-14
BE817591A (en) 1975-01-13

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Legal Events

Date Code Title Description
PS Patent sealed
PCNP Patent ceased through non-payment of renewal fee