GB1394454A - Process for the production of high-purity phenol - Google Patents
Process for the production of high-purity phenolInfo
- Publication number
- GB1394454A GB1394454A GB2559872A GB2559872A GB1394454A GB 1394454 A GB1394454 A GB 1394454A GB 2559872 A GB2559872 A GB 2559872A GB 2559872 A GB2559872 A GB 2559872A GB 1394454 A GB1394454 A GB 1394454A
- Authority
- GB
- United Kingdom
- Prior art keywords
- impurities
- phenol
- boiling
- water
- colour
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 title abstract 5
- 238000000034 method Methods 0.000 title abstract 2
- 239000012535 impurity Substances 0.000 abstract 5
- 238000009835 boiling Methods 0.000 abstract 4
- 238000000354 decomposition reaction Methods 0.000 abstract 3
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 abstract 2
- 238000003776 cleavage reaction Methods 0.000 abstract 2
- RWGFKTVRMDUZSP-UHFFFAOYSA-N cumene Chemical compound CC(C)C1=CC=CC=C1 RWGFKTVRMDUZSP-UHFFFAOYSA-N 0.000 abstract 2
- 238000004821 distillation Methods 0.000 abstract 2
- 230000007017 scission Effects 0.000 abstract 2
- OZXIZRZFGJZWBF-UHFFFAOYSA-N 1,3,5-trimethyl-2-(2,4,6-trimethylphenoxy)benzene Chemical compound CC1=CC(C)=CC(C)=C1OC1=C(C)C=C(C)C=C1C OZXIZRZFGJZWBF-UHFFFAOYSA-N 0.000 abstract 1
- FRIBMENBGGCKPD-UHFFFAOYSA-N 3-(2,3-dimethoxyphenyl)prop-2-enal Chemical compound COC1=CC=CC(C=CC=O)=C1OC FRIBMENBGGCKPD-UHFFFAOYSA-N 0.000 abstract 1
- JLBJTVDPSNHSKJ-UHFFFAOYSA-N 4-Methylstyrene Chemical compound CC1=CC=C(C=C)C=C1 JLBJTVDPSNHSKJ-UHFFFAOYSA-N 0.000 abstract 1
- UQRONKZLYKUEMO-UHFFFAOYSA-N 4-methyl-1-(2,4,6-trimethylphenyl)pent-4-en-2-one Chemical group CC(=C)CC(=O)Cc1c(C)cc(C)cc1C UQRONKZLYKUEMO-UHFFFAOYSA-N 0.000 abstract 1
- 239000002253 acid Substances 0.000 abstract 1
- 239000012141 concentrate Substances 0.000 abstract 1
- SHOJXDKTYKFBRD-UHFFFAOYSA-N mesityl oxide Natural products CC(C)=CC(C)=O SHOJXDKTYKFBRD-UHFFFAOYSA-N 0.000 abstract 1
- 150000002989 phenols Chemical class 0.000 abstract 1
- 238000000746 purification Methods 0.000 abstract 1
- 239000000126 substance Substances 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C37/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring
- C07C37/68—Purification; separation; Use of additives, e.g. for stabilisation
- C07C37/70—Purification; separation; Use of additives, e.g. for stabilisation by physical treatment
- C07C37/74—Purification; separation; Use of additives, e.g. for stabilisation by physical treatment by distillation
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
1394454 Phenol BP CHEMICALS INTERNATIONAL Ltd 4 May 1973 [1 June 1972] 25598/72 Heading C2C A process for the purification of phenol obtained from the acid cleavage of cumene hydroperoxide and containing water-soluble colour-forming impurities boiling from 152‹ to 182‹ C. comprises subjecting the phenol which has been freed from acetone, water, mesityl oxide, cumene and methyl styrene to a distillation in which the water-soluble colourforming impurities are maintained within a substantially anhydrous part of the column under distillation conditions for a period so as to concentrate the impurities and at least partially to decompose them to mesityl oxidecontaining decomposition products, removing a base product comprising phenols free from watersoluble colour-forming impurities boiling from 152‹ to 182‹ C. and an overhead fraction containing lower-boiling decomposition products in the presence or absence of the said impurities and thereafter separating the phenol from the higher boiling decomposition and cleavage products. An example is furnished.
Priority Applications (14)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB2559872A GB1394454A (en) | 1972-06-01 | 1972-06-01 | Process for the production of high-purity phenol |
| SE7307543A SE401919B (en) | 1972-06-01 | 1973-05-28 | SEE THAT PURE PHENOL RECEIVED THROUGH ACID SPLINING OF CUMUMENHYDROPEROXIDE AND CONTAINING WATER-SOLUBLE, COLOR-FORMING COMPOUNDS WITH BOILING INTERVALS 152-182Ÿ0C |
| DE2327216A DE2327216A1 (en) | 1972-06-01 | 1973-05-28 | METHOD FOR CLEANING UP PHENOL |
| NL7307442A NL7307442A (en) | 1972-06-01 | 1973-05-29 | |
| ES415422A ES415422A1 (en) | 1972-06-01 | 1973-05-30 | Process for the production of high-purity phenol |
| FR7319630A FR2186455B1 (en) | 1972-06-01 | 1973-05-30 | |
| NO2259/73A NO141646C (en) | 1972-06-01 | 1973-05-30 | PROCEDURE FOR PHENOL CLEANING. |
| AR248287A AR197813A1 (en) | 1972-06-01 | 1973-05-30 | PROCEDURE FOR THE PRODUCTION OF HIGH PURITY PHENOL |
| IT24857/73A IT988825B (en) | 1972-06-01 | 1973-05-30 | PROCESS FOR THE PRODUCTION OF HIGH PURITY PHENOL |
| BE131786A BE800342A (en) | 1972-06-01 | 1973-05-30 | PROCESS FOR PRODUCING HIGH PURE PHENOL, |
| CA172,826A CA989766A (en) | 1972-06-01 | 1973-05-31 | Process for the production of high-purity phenol |
| JP48060407A JPS582931B2 (en) | 1972-06-01 | 1973-05-31 | Phenol no seiseihouhou |
| BR4135/73A BR7304135D0 (en) | 1972-06-01 | 1973-06-01 | PHENOL PURIFICATION PROCESS |
| US468147A US3896006A (en) | 1972-06-01 | 1974-05-08 | Mesityl oxide removal from high-purity phenol |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB2559872A GB1394454A (en) | 1972-06-01 | 1972-06-01 | Process for the production of high-purity phenol |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB1394454A true GB1394454A (en) | 1975-05-14 |
Family
ID=10230290
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB2559872A Expired GB1394454A (en) | 1972-06-01 | 1972-06-01 | Process for the production of high-purity phenol |
Country Status (13)
| Country | Link |
|---|---|
| JP (1) | JPS582931B2 (en) |
| AR (1) | AR197813A1 (en) |
| BE (1) | BE800342A (en) |
| BR (1) | BR7304135D0 (en) |
| CA (1) | CA989766A (en) |
| DE (1) | DE2327216A1 (en) |
| ES (1) | ES415422A1 (en) |
| FR (1) | FR2186455B1 (en) |
| GB (1) | GB1394454A (en) |
| IT (1) | IT988825B (en) |
| NL (1) | NL7307442A (en) |
| NO (1) | NO141646C (en) |
| SE (1) | SE401919B (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4832796A (en) * | 1987-07-16 | 1989-05-23 | General Electric Company | Process for purifying phenol |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2015178476A (en) * | 2014-03-19 | 2015-10-08 | 三菱化学株式会社 | Method for producing phenol |
-
1972
- 1972-06-01 GB GB2559872A patent/GB1394454A/en not_active Expired
-
1973
- 1973-05-28 SE SE7307543A patent/SE401919B/en unknown
- 1973-05-28 DE DE2327216A patent/DE2327216A1/en not_active Withdrawn
- 1973-05-29 NL NL7307442A patent/NL7307442A/xx not_active Application Discontinuation
- 1973-05-30 IT IT24857/73A patent/IT988825B/en active
- 1973-05-30 ES ES415422A patent/ES415422A1/en not_active Expired
- 1973-05-30 FR FR7319630A patent/FR2186455B1/fr not_active Expired
- 1973-05-30 NO NO2259/73A patent/NO141646C/en unknown
- 1973-05-30 AR AR248287A patent/AR197813A1/en active
- 1973-05-30 BE BE131786A patent/BE800342A/en unknown
- 1973-05-31 CA CA172,826A patent/CA989766A/en not_active Expired
- 1973-05-31 JP JP48060407A patent/JPS582931B2/en not_active Expired
- 1973-06-01 BR BR4135/73A patent/BR7304135D0/en unknown
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4832796A (en) * | 1987-07-16 | 1989-05-23 | General Electric Company | Process for purifying phenol |
Also Published As
| Publication number | Publication date |
|---|---|
| DE2327216A1 (en) | 1973-12-20 |
| FR2186455A1 (en) | 1974-01-11 |
| NO141646C (en) | 1980-04-16 |
| JPS582931B2 (en) | 1983-01-19 |
| ES415422A1 (en) | 1976-02-16 |
| NO141646B (en) | 1980-01-07 |
| BE800342A (en) | 1973-11-30 |
| CA989766A (en) | 1976-05-25 |
| JPS4948628A (en) | 1974-05-11 |
| AR197813A1 (en) | 1974-05-10 |
| FR2186455B1 (en) | 1977-04-29 |
| BR7304135D0 (en) | 1974-07-18 |
| NL7307442A (en) | 1973-12-04 |
| IT988825B (en) | 1975-04-30 |
| SE401919B (en) | 1978-06-05 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PS | Patent sealed | ||
| PCNP | Patent ceased through non-payment of renewal fee |