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GB1152983A - Perfluoro Carboxylic Acid Fluorides and their preparation - Google Patents

Perfluoro Carboxylic Acid Fluorides and their preparation

Info

Publication number
GB1152983A
GB1152983A GB19585/66A GB1958566A GB1152983A GB 1152983 A GB1152983 A GB 1152983A GB 19585/66 A GB19585/66 A GB 19585/66A GB 1958566 A GB1958566 A GB 1958566A GB 1152983 A GB1152983 A GB 1152983A
Authority
GB
United Kingdom
Prior art keywords
acid
tertiary amino
hcl
amino group
carboxylic acid
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB19585/66A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
3M Co
Original Assignee
Minnesota Mining and Manufacturing Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Minnesota Mining and Manufacturing Co filed Critical Minnesota Mining and Manufacturing Co
Publication of GB1152983A publication Critical patent/GB1152983A/en
Expired legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C25ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25BELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
    • C25B3/00Electrolytic production of organic compounds
    • C25B3/20Processes
    • C25B3/27Halogenation
    • C25B3/28Fluorination
    • CCHEMISTRY; METALLURGY
    • C25ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25BELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
    • C25B3/00Electrolytic production of organic compounds
    • C25B3/01Products
    • C25B3/05Heterocyclic compounds
    • CCHEMISTRY; METALLURGY
    • C25ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25BELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
    • C25B3/00Electrolytic production of organic compounds
    • C25B3/01Products
    • C25B3/07Oxygen containing compounds
    • CCHEMISTRY; METALLURGY
    • C25ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25BELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
    • C25B3/00Electrolytic production of organic compounds
    • C25B3/01Products
    • C25B3/09Nitrogen containing compounds
    • CCHEMISTRY; METALLURGY
    • C25ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25BELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
    • C25B3/00Electrolytic production of organic compounds
    • C25B3/01Products
    • C25B3/11Halogen containing compounds
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10STECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S516/00Colloid systems and wetting agents; subcombinations thereof; processes of
    • Y10S516/01Wetting, emulsifying, dispersing, or stabilizing agents

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Electrochemistry (AREA)
  • Materials Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

1,152,983. Perfluoro-aminocarboxylic acids and derivatives thereof. MINNESOTA MINING & MFG. CO. 3 May, 1966 [3 May, 1965], No. 19585/66. Heading C2C. [Also in Division C7] The invention comprises perfluorocarboxylic acid fluorides substituted by a tertiary amino group and having only a perfluoroalkylene group between the acid fluoride radical and the nitrogen atom of the tertiary amino group. The compounds are prepared by electrofluorination of a tertiary amino-substituted carboxylic acid halide having only an alkylene group between the acid halide radical and the nitrogen atom of the tertiary amino group. The acid fluorides may be converted to the corresponding acids, salts and esters by conventional methods. Ethyliminodipropionyl chloride hydrochloride is prepared by reacting ethylamine with ethyl acrylate to give diethyl ethyliminodipropionate, C 2 H 5 N(CH 2 CH 2 COOC 2 H 5 ) 2 , which is then hydrolysed with HCl to give ethyliminodipropionic acid hydrochloride, C 2 H 5 N(CH 2 CH 2 COOH) 2 .HCl, which is converted by reaction with PCl 5 to the desired acid chloride, C 2 H 5 N(CH 2 CH 2 COCl) 2 .HCl.
GB19585/66A 1965-05-03 1966-05-03 Perfluoro Carboxylic Acid Fluorides and their preparation Expired GB1152983A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US45284565A 1965-05-03 1965-05-03

Publications (1)

Publication Number Publication Date
GB1152983A true GB1152983A (en) 1969-05-21

Family

ID=23798183

Family Applications (1)

Application Number Title Priority Date Filing Date
GB19585/66A Expired GB1152983A (en) 1965-05-03 1966-05-03 Perfluoro Carboxylic Acid Fluorides and their preparation

Country Status (3)

Country Link
US (1) US3471484A (en)
DE (1) DE1595998C3 (en)
GB (1) GB1152983A (en)

Families Citing this family (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
USRE29255E (en) * 1968-10-16 1977-06-07 E. I. Du Pont De Nemours And Company Photographic layers containing perfluoro compounds and coating thereof
US4985556A (en) * 1987-09-10 1991-01-15 Agency Of Industrial Science & Technology Perfluoro(dialkylaminopropene) derivatives
JP3409316B2 (en) 2000-06-26 2003-05-26 独立行政法人産業技術総合研究所 Novel perfluoro {1,4-bis [2- (fluorocarbonyl) -n-propyl] piperazine} and process for producing the same
WO2016017754A1 (en) 2014-07-30 2016-02-04 三菱マテリアル株式会社 Filter medium, method for producing filter medium, water treatment module, and water treatment device
JP5909604B1 (en) 2014-07-30 2016-04-26 三菱マテリアル株式会社 Surface coating material, coating film and hydrophilic oil-repellent material
US10208210B2 (en) 2014-07-30 2019-02-19 Mitsubishi Materials Corporation Hydrophilic oil repellent and production method of same, surface coating material, coating film, resin composition, oil-water separation filter material, and porous body
JP6461573B2 (en) 2014-07-30 2019-01-30 三菱マテリアル株式会社 Oil / water separator / collector

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2500388A (en) * 1948-07-21 1950-03-14 Minnesota Mining & Mfg Fluorocarbon ethers
US2519983A (en) * 1948-11-29 1950-08-22 Minnesota Mining & Mfg Electrochemical process of making fluorine-containing carbon compounds
US2567011A (en) * 1949-01-10 1951-09-04 Minnesota Mining & Mfg Fluorocarbon acids and derivatives
US2616927A (en) * 1950-05-12 1952-11-04 Minnesota Mining & Mfg Fluorocarbon tertiary amines
GB763673A (en) * 1953-12-21 1956-12-12 Minnesota Mining & Mfg Improvements in and relating to fluorocarbon acids and derivatives
US2950317A (en) * 1957-10-21 1960-08-23 Minnesota Mining & Mfg Process for preparation of perfluoroalkyl sulfonyl chlorides

Also Published As

Publication number Publication date
DE1595998C3 (en) 1980-11-20
DE1595998B2 (en) 1980-03-20
US3471484A (en) 1969-10-07
DE1595998A1 (en) 1970-03-19

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Legal Events

Date Code Title Description
PS Patent sealed [section 19, patents act 1949]
PE Patent expired