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FR3095131B1 - Procede de synthese rapide d’une zeolithe de type structural afx par synthese en presence d’un structurant organique azote - Google Patents

Procede de synthese rapide d’une zeolithe de type structural afx par synthese en presence d’un structurant organique azote Download PDF

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Publication number
FR3095131B1
FR3095131B1 FR1904199A FR1904199A FR3095131B1 FR 3095131 B1 FR3095131 B1 FR 3095131B1 FR 1904199 A FR1904199 A FR 1904199A FR 1904199 A FR1904199 A FR 1904199A FR 3095131 B1 FR3095131 B1 FR 3095131B1
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France
Prior art keywords
synthesis
organic nitrogen
structural type
zeolith
structuring
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
FR1904199A
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English (en)
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FR3095131A1 (fr
Inventor
Franco Raquel Martinez
Bogdan Harbuzaru
Eric Llido
David Berthout
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IFP Energies Nouvelles IFPEN
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IFP Energies Nouvelles IFPEN
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Publication date
Application filed by IFP Energies Nouvelles IFPEN filed Critical IFP Energies Nouvelles IFPEN
Priority to FR1904199A priority Critical patent/FR3095131B1/fr
Priority to PCT/EP2020/060475 priority patent/WO2020212355A1/fr
Publication of FR3095131A1 publication Critical patent/FR3095131A1/fr
Application granted granted Critical
Publication of FR3095131B1 publication Critical patent/FR3095131B1/fr
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Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/70—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/70—Catalysts, in general, characterised by their form or physical properties characterised by their crystalline properties, e.g. semi-crystalline
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2235/00—Indexing scheme associated with group B01J35/00, related to the analysis techniques used to determine the catalysts form or properties
    • B01J2235/15—X-ray diffraction
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/30—Catalysts, in general, characterised by their form or physical properties characterised by their physical properties
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/46—Other types characterised by their X-ray diffraction pattern and their defined composition
    • C01B39/48—Other types characterised by their X-ray diffraction pattern and their defined composition using at least one organic template directing agent
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2235/00—Indexing scheme associated with group B01J35/00, related to the analysis techniques used to determine the catalysts form or properties
    • B01J2235/30—Scanning electron microscopy; Transmission electron microscopy

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Inorganic Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Silicates, Zeolites, And Molecular Sieves (AREA)

Abstract

L’invention concerne un procédé de préparation d'une zéolithe de type structural AFX comprenant au moins :i) le mélange en milieu aqueux, d'au moins une source d'au moins d’un élément tétravalent X (XO2), au moins une source d’au moins un élément trivalent Y (Y2O3), d’un composé organique azoté R, d’au moins une source d'au moins un métal alcalin et/ou alcalino-terreux M, avec la composition molaire suivante : XO2/Y2O3 compris entre 10 et 100, H2O/XO2 compris entre 5 et 60, R/XO2 compris entre 0,05 à 0,50, M2/nO/XO2 compris entre 0,05 à 0,40, bornes incluses, au moins un élément X étant le silicium, au moins un élément Y étant l’aluminium, pour obtenir un gel précurseur homogène;ii) le traitement hydrothermal dudit gel précurseur sous pression autogène à une température comprise entre 120°C et 250°C, pendant 2 à 12 heures . Figure à publier : Figure 1
FR1904199A 2019-04-19 2019-04-19 Procede de synthese rapide d’une zeolithe de type structural afx par synthese en presence d’un structurant organique azote Active FR3095131B1 (fr)

Priority Applications (2)

Application Number Priority Date Filing Date Title
FR1904199A FR3095131B1 (fr) 2019-04-19 2019-04-19 Procede de synthese rapide d’une zeolithe de type structural afx par synthese en presence d’un structurant organique azote
PCT/EP2020/060475 WO2020212355A1 (fr) 2019-04-19 2020-04-14 Procede de synthese rapide d'une zeolithe de type structural afx par synthese en presence d'un structurant organique azote

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FR1904199A FR3095131B1 (fr) 2019-04-19 2019-04-19 Procede de synthese rapide d’une zeolithe de type structural afx par synthese en presence d’un structurant organique azote
FR1904199 2019-04-19

Publications (2)

Publication Number Publication Date
FR3095131A1 FR3095131A1 (fr) 2020-10-23
FR3095131B1 true FR3095131B1 (fr) 2021-10-29

Family

ID=68072569

Family Applications (1)

Application Number Title Priority Date Filing Date
FR1904199A Active FR3095131B1 (fr) 2019-04-19 2019-04-19 Procede de synthese rapide d’une zeolithe de type structural afx par synthese en presence d’un structurant organique azote

Country Status (2)

Country Link
FR (1) FR3095131B1 (fr)
WO (1) WO2020212355A1 (fr)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112591760B (zh) * 2020-12-03 2022-06-17 金华职业技术学院 一种y分子筛转晶合成新形貌的ssz-16分子筛及其方法

Family Cites Families (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4508837A (en) 1982-09-28 1985-04-02 Chevron Research Company Zeolite SSZ-16
US5194235A (en) 1992-08-27 1993-03-16 Chevron Research And Technology Company Synthesis of SSZ-16 zeolite catalyst
RU2732126C2 (ru) 2014-11-14 2020-09-11 Джонсон Мэтти Паблик Лимитед Компани Afx цеолит
JP6430303B2 (ja) 2015-03-16 2018-11-28 国立大学法人横浜国立大学 Ａｆｘ型ゼオライトの製法
US9868643B2 (en) 2016-05-20 2018-01-16 Chevron U.S.A. Inc. Synthesis of zeolite SSZ-16
KR20190009806A (ko) 2016-05-24 2019-01-29 엑손모빌 케미칼 패턴츠 인코포레이티드 촉매 금속을 포함하는 합성 제올라이트
WO2018064318A1 (fr) 2016-09-30 2018-04-05 Johnson Matthey Public Limited Company Nouvelle synthèse de zéolite avec un métal alcalinoterreux
US10414665B2 (en) 2016-09-30 2019-09-17 Johnson Matthey Public Limited Company Synthesis of AFX zeolite
FR3064261B1 (fr) * 2017-03-24 2019-03-22 IFP Energies Nouvelles Procede de synthese de la zeolithe izm-2 en presence d'un structurant dihydroxyde de 1,6-bis(methylpiperidinium)hexane
FR3081343B1 (fr) * 2018-05-24 2023-11-10 Ifp Energies Now Procede de preparation d’une zeolithe de type structural afx par synthese en presence d’un structurant organique azote

Also Published As

Publication number Publication date
WO2020212355A1 (fr) 2020-10-22
FR3095131A1 (fr) 2020-10-23

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