ES483153A1 - Procedimiento para la purificacion de mezclas que contienen una cicloalcanona con 5-12 atomos de carbono - Google Patents
Procedimiento para la purificacion de mezclas que contienen una cicloalcanona con 5-12 atomos de carbonoInfo
- Publication number
- ES483153A1 ES483153A1 ES483153A ES483153A ES483153A1 ES 483153 A1 ES483153 A1 ES 483153A1 ES 483153 A ES483153 A ES 483153A ES 483153 A ES483153 A ES 483153A ES 483153 A1 ES483153 A1 ES 483153A1
- Authority
- ES
- Spain
- Prior art keywords
- cycloalkanone
- purification
- oxidation
- aldol condensation
- acid
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
- C07C45/78—Separation; Purification; Stabilisation; Use of additives
- C07C45/85—Separation; Purification; Stabilisation; Use of additives by treatment giving rise to a chemical modification
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Abstract
Procedimiento para la purificación de mezclas que contienen una cicloalcanona con 5-12 átomos de carbono en el anillo y han sido obtenidas en la oxidación del correspondiente cicloalcano en fase líquida por medio de un gas que contiene oxígeno molecular, caracterizado porque la mezcla que contiene la cicloalcanona es sometida a una reacción de condensación aldólica en que está convertido por lo menos 80% de los aldehidos presentes, pero se deja saponificar como máximo 20% de los ésteres cicloalcohílicos derivados de ácidos carboxílicos con al menos 4 átomos de carbono por molécula.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| NL7808416A NL7808416A (nl) | 1978-08-12 | 1978-08-12 | Werkwijze voor het verwijderen van aldehyden uit cyclo- alkanon bevattende mengsels verkregen bij oxidatie van cycloalkanen. |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ES483153A1 true ES483153A1 (es) | 1980-03-01 |
Family
ID=19831369
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES483153A Expired ES483153A1 (es) | 1978-08-12 | 1979-08-06 | Procedimiento para la purificacion de mezclas que contienen una cicloalcanona con 5-12 atomos de carbono |
Country Status (17)
| Country | Link |
|---|---|
| JP (1) | JPS5527192A (es) |
| AR (1) | AR223010A1 (es) |
| BE (1) | BE878200A (es) |
| BR (1) | BR7905172A (es) |
| CA (1) | CA1123457A (es) |
| CS (1) | CS209931B2 (es) |
| DD (1) | DD145529A5 (es) |
| DE (1) | DE2932361A1 (es) |
| ES (1) | ES483153A1 (es) |
| FR (1) | FR2433012A1 (es) |
| GB (1) | GB2028329B (es) |
| IN (1) | IN152254B (es) |
| IT (1) | IT1120507B (es) |
| MX (1) | MX5997E (es) |
| MY (1) | MY8500894A (es) |
| NL (1) | NL7808416A (es) |
| PL (1) | PL117395B1 (es) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP1433774A1 (en) * | 2002-12-27 | 2004-06-30 | Koninklijke DSM N.V. | Process for reducing the aldehyde concentration in a mixture comprising cyclohexanone and one or more aldehydes |
| US20060189829A1 (en) * | 2005-02-18 | 2006-08-24 | Basf Corporation | Method of minimizing aldehyde based impurities in a process stream |
Family Cites Families (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1085529B (de) * | 1952-07-03 | 1960-07-21 | American Home Prod | Verfahren zur Herstellung von 4-Aryl-4-carbalkoxy-N-alkyl-azacycloalkanen und deren Salzen |
| DE1046610B (de) * | 1955-06-15 | 1958-12-18 | Basf Ag | Verfahren zur Herstellung von Cyclohexanol und Cyclohexanon durch Oxydation von Cyclohexan |
| DE1085520B (de) * | 1958-01-25 | 1960-07-21 | Basf Ag | Verfahren zur Herstellung von Alkylen-bis-cycloalkanonen |
| DE1155121B (de) * | 1960-05-06 | 1963-10-03 | Basf Ag | Verfahren zur Herstellung von Cyclohexanol und Cyclohexanon durch Oxydation von Cyclohexan |
| DE1518255B1 (de) * | 1965-01-30 | 1969-12-11 | Vickers Zimmer Ag | Verfahren zur Aufarbeitung des Reaktionsgemisches der Oxydation von Cyclohexan mit sauerstoffhaltigen Gasen in fluessiger Phase |
| DE2246103A1 (de) * | 1972-09-20 | 1974-03-28 | Bayer Sa Nv | Verfahren zur reinigung von cyclohexanon |
| JPS4969634A (es) * | 1973-09-20 | 1974-07-05 | ||
| US3987100A (en) * | 1974-04-11 | 1976-10-19 | E. I. Du Pont De Nemours And Company | Cyclohexane oxidation in the presence of binary catalysts |
| DE2650892C3 (de) * | 1976-11-06 | 1980-05-29 | Basf Ag, 6700 Ludwigshafen | Verfahren zur Aufarbeitung von Cyclohexanol und Cyclohexanon enthaltenden Reaktionsgemischen |
-
1978
- 1978-08-12 NL NL7808416A patent/NL7808416A/nl not_active Application Discontinuation
-
1979
- 1979-07-25 CA CA332,513A patent/CA1123457A/en not_active Expired
- 1979-08-06 ES ES483153A patent/ES483153A1/es not_active Expired
- 1979-08-08 CS CS795441A patent/CS209931B2/cs unknown
- 1979-08-09 DE DE19792932361 patent/DE2932361A1/de not_active Ceased
- 1979-08-09 JP JP10177679A patent/JPS5527192A/ja active Pending
- 1979-08-09 AR AR277658A patent/AR223010A1/es active
- 1979-08-10 DD DD79214917A patent/DD145529A5/de unknown
- 1979-08-10 MX MX798311U patent/MX5997E/es unknown
- 1979-08-10 IN IN830/CAL/79A patent/IN152254B/en unknown
- 1979-08-10 BR BR7905172A patent/BR7905172A/pt unknown
- 1979-08-10 FR FR7920505A patent/FR2433012A1/fr active Granted
- 1979-08-10 BE BE0/196697A patent/BE878200A/nl not_active IP Right Cessation
- 1979-08-10 IT IT50026/79A patent/IT1120507B/it active
- 1979-08-11 PL PL1979217702A patent/PL117395B1/pl unknown
- 1979-08-13 GB GB7928080A patent/GB2028329B/en not_active Expired
-
1985
- 1985-12-30 MY MY894/85A patent/MY8500894A/xx unknown
Also Published As
| Publication number | Publication date |
|---|---|
| FR2433012A1 (fr) | 1980-03-07 |
| IN152254B (es) | 1983-11-26 |
| PL117395B1 (en) | 1981-07-31 |
| CA1123457A (en) | 1982-05-11 |
| FR2433012B1 (es) | 1982-12-10 |
| CS209931B2 (en) | 1981-12-31 |
| NL7808416A (nl) | 1980-02-14 |
| GB2028329B (en) | 1982-09-15 |
| MY8500894A (en) | 1985-12-31 |
| DD145529A5 (de) | 1980-12-17 |
| AR223010A1 (es) | 1981-07-15 |
| JPS5527192A (en) | 1980-02-27 |
| BR7905172A (pt) | 1980-05-06 |
| GB2028329A (en) | 1980-03-05 |
| IT7950026A0 (it) | 1979-08-10 |
| DE2932361A1 (de) | 1980-02-28 |
| PL217702A1 (es) | 1980-04-08 |
| MX5997E (es) | 1984-09-18 |
| BE878200A (nl) | 1980-02-11 |
| IT1120507B (it) | 1986-03-26 |
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