ES408273A1 - Process for the preparation of 4-chloro-2,5-dimethoxyaniline - Google Patents
Process for the preparation of 4-chloro-2,5-dimethoxyanilineInfo
- Publication number
- ES408273A1 ES408273A1 ES408273A ES408273A ES408273A1 ES 408273 A1 ES408273 A1 ES 408273A1 ES 408273 A ES408273 A ES 408273A ES 408273 A ES408273 A ES 408273A ES 408273 A1 ES408273 A1 ES 408273A1
- Authority
- ES
- Spain
- Prior art keywords
- chloro
- preparation
- reduction
- dimethoxyaniline
- catalytic
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- YGUFQYGSBVXPMC-UHFFFAOYSA-N 4-chloro-2,5-dimethoxyaniline Chemical compound COC1=CC(Cl)=C(OC)C=C1N YGUFQYGSBVXPMC-UHFFFAOYSA-N 0.000 title abstract 2
- 238000000034 method Methods 0.000 title abstract 2
- BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 abstract 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 abstract 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 abstract 1
- 239000007864 aqueous solution Substances 0.000 abstract 1
- 229910052799 carbon Inorganic materials 0.000 abstract 1
- 239000003054 catalyst Substances 0.000 abstract 1
- 230000003197 catalytic effect Effects 0.000 abstract 1
- 238000010531 catalytic reduction reaction Methods 0.000 abstract 1
- 150000001875 compounds Chemical class 0.000 abstract 1
- 229910052739 hydrogen Inorganic materials 0.000 abstract 1
- 239000001257 hydrogen Substances 0.000 abstract 1
- 239000007791 liquid phase Substances 0.000 abstract 1
- 229910052697 platinum Inorganic materials 0.000 abstract 1
- 238000006722 reduction reaction Methods 0.000 abstract 1
- 239000000126 substance Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C213/00—Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton
- C07C213/02—Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton by reactions involving the formation of amino groups from compounds containing hydroxy groups or etherified or esterified hydroxy groups
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
- B01J23/38—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals
- B01J23/40—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals of the platinum group metals
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
- B01J23/38—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals
- B01J23/40—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals of the platinum group metals
- B01J23/42—Platinum
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
- B01J21/18—Carbon
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
- B01J37/20—Sulfiding
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Catalysts (AREA)
Abstract
Procedure for the preparation of 4-chloro-2,5-dimethoxy-aniline by catalytic reduction with hydrogen of the nitrated compound in liquid phase at elevated temperature and pressure, characterized in that the reduction is carried out in the presence of a platinum catalyst on sulphided or sulphited carbon with the addition of catalytic amounts of buffer substances, which in aqueous solution give rise to a pH value of 8 to 10. (Machine-translation by Google Translate, not legally binding)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE2156051A DE2156051C3 (en) | 1971-11-11 | 1971-11-11 | Process for the preparation of 4-chloro-2,5-dimethoxy-aniline |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ES408273A1 true ES408273A1 (en) | 1975-11-16 |
Family
ID=5824830
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES408273A Expired ES408273A1 (en) | 1971-11-11 | 1972-11-04 | Process for the preparation of 4-chloro-2,5-dimethoxyaniline |
Country Status (20)
| Country | Link |
|---|---|
| JP (1) | JPS5644060B2 (en) |
| AT (1) | AT331210B (en) |
| AU (1) | AU474209B2 (en) |
| BE (1) | BE791300A (en) |
| CA (1) | CA995248A (en) |
| CH (1) | CH575377A5 (en) |
| CS (1) | CS173610B2 (en) |
| DD (1) | DD99356A5 (en) |
| DE (1) | DE2156051C3 (en) |
| ES (1) | ES408273A1 (en) |
| FR (1) | FR2160166A5 (en) |
| GB (1) | GB1393428A (en) |
| HU (1) | HU165205B (en) |
| IL (1) | IL40777A (en) |
| IT (1) | IT970356B (en) |
| NL (1) | NL7214964A (en) |
| PL (1) | PL85137B1 (en) |
| RO (1) | RO62342A (en) |
| SU (1) | SU474135A3 (en) |
| ZA (1) | ZA727738B (en) |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2455704C3 (en) * | 1974-11-25 | 1978-06-08 | Hoechst Ag, 6000 Frankfurt | Process for the preparation of 4-chloro-23-dimethoxy aniline |
| CA1148562A (en) * | 1979-02-22 | 1983-06-21 | Alfred J. Bird | Catalyst for the hydrogenation of halogen substituted aromatic nitro compounds |
| JPS58159957U (en) * | 1982-04-19 | 1983-10-25 | 日本発条株式会社 | Headrest upper and lower adjustment mechanism |
| DE3821013A1 (en) * | 1988-06-22 | 1989-12-28 | Hoechst Ag | METHOD FOR PRODUCING 4-CHLORINE-2,5-DIMETHOXYANILINE |
-
0
- BE BE791300D patent/BE791300A/en not_active IP Right Cessation
-
1971
- 1971-11-11 DE DE2156051A patent/DE2156051C3/en not_active Expired
-
1972
- 1972-10-18 DD DD166310A patent/DD99356A5/xx unknown
- 1972-11-01 ZA ZA727738A patent/ZA727738B/en unknown
- 1972-11-02 RO RO72709A patent/RO62342A/ro unknown
- 1972-11-04 ES ES408273A patent/ES408273A1/en not_active Expired
- 1972-11-06 NL NL7214964A patent/NL7214964A/xx not_active Application Discontinuation
- 1972-11-07 CS CS7507A patent/CS173610B2/cs unknown
- 1972-11-07 AU AU48583/72A patent/AU474209B2/en not_active Expired
- 1972-11-08 GB GB5151772A patent/GB1393428A/en not_active Expired
- 1972-11-08 IL IL40777A patent/IL40777A/en unknown
- 1972-11-09 CH CH1630472A patent/CH575377A5/xx not_active IP Right Cessation
- 1972-11-09 IT IT31481/72A patent/IT970356B/en active
- 1972-11-09 HU HUHO1523A patent/HU165205B/hu unknown
- 1972-11-09 AT AT952372A patent/AT331210B/en not_active IP Right Cessation
- 1972-11-09 SU SU1843993A patent/SU474135A3/en active
- 1972-11-10 FR FR7239905A patent/FR2160166A5/fr not_active Expired
- 1972-11-10 CA CA156,152A patent/CA995248A/en not_active Expired
- 1972-11-10 JP JP11219772A patent/JPS5644060B2/ja not_active Expired
- 1972-11-10 PL PL1972158797A patent/PL85137B1/pl unknown
Also Published As
| Publication number | Publication date |
|---|---|
| DE2156051B2 (en) | 1974-03-28 |
| PL85137B1 (en) | 1976-04-30 |
| CA995248A (en) | 1976-08-17 |
| CH575377A5 (en) | 1976-05-14 |
| ZA727738B (en) | 1973-09-26 |
| CS173610B2 (en) | 1977-02-28 |
| AU4858372A (en) | 1974-05-09 |
| AT331210B (en) | 1976-08-10 |
| GB1393428A (en) | 1975-05-07 |
| ATA952372A (en) | 1975-11-15 |
| DE2156051C3 (en) | 1974-10-31 |
| BE791300A (en) | 1973-05-14 |
| IL40777A0 (en) | 1973-01-30 |
| FR2160166A5 (en) | 1973-06-22 |
| AU474209B2 (en) | 1976-07-15 |
| JPS4857938A (en) | 1973-08-14 |
| NL7214964A (en) | 1973-05-15 |
| DE2156051A1 (en) | 1973-05-17 |
| RO62342A (en) | 1977-08-15 |
| HU165205B (en) | 1974-07-27 |
| DD99356A5 (en) | 1973-08-05 |
| SU474135A3 (en) | 1975-06-14 |
| IT970356B (en) | 1974-04-10 |
| IL40777A (en) | 1976-04-30 |
| JPS5644060B2 (en) | 1981-10-16 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| ES413925A1 (en) | Hydrocarbon isomerization process | |
| GB1226469A (en) | ||
| ES408273A1 (en) | Process for the preparation of 4-chloro-2,5-dimethoxyaniline | |
| ES386504A1 (en) | Process for preparing 3-pentene nitrile | |
| ES400237A2 (en) | Method of activating silver catalysts | |
| ES394885A1 (en) | ' -methylfluorene-2-acetic acid | |
| GB1323188A (en) | Process for the preparation of o-aminobenzonitrile | |
| ES425412A1 (en) | Procedure for obtaining epsilon-aminocaprnamide. (Machine-translation by Google Translate, not legally binding) | |
| GB907154A (en) | Improved process for the catalytic reduction of dinitrotoluenes | |
| ES383050A1 (en) | Production of alcohols | |
| ES447827A1 (en) | 2,5-dimethoxy-4-chloroaniline | |
| ES402244A1 (en) | Process for the production of dichloroacetoxypropane | |
| GB1025813A (en) | Production of mannitol/sorbitol | |
| ES277847A1 (en) | Procedure for the obtaining of hydrocyanic acid and acetic acid from oxyaminoacetone (Machine-translation by Google Translate, not legally binding) | |
| ES296448A1 (en) | Procedure for the preparation of cycloexilamine from ciloxane (Machine-translation by Google Translate, not legally binding) | |
| ES309014A1 (en) | Procedure for the preparation of medicamentos amtihelminticos. (Machine-translation by Google Translate, not legally binding) | |
| KR850004094A (en) | Method for preparing aminobenzylamine | |
| ES388746A1 (en) | Catalytic composite of platinum group metal nickel and group iva metal with carrier material and use thereof | |
| ES257994A1 (en) | Procedure for the preparation of pharmaceutical products with local anesthetic activity (Machine-translation by Google Translate, not legally binding) | |
| ES377165A1 (en) | A procedure for the preparation of 5- (3-cyanopropyl) -hidantoin. (Machine-translation by Google Translate, not legally binding) | |
| ES411613A1 (en) | A procedure for the obtaining of N-isopropil-alpha-chloroacetanilida pura. (Machine-translation by Google Translate, not legally binding) | |
| ES398319A1 (en) | Procedure for the obtaining of benzene derivatives of heterociclic character. (Machine-translation by Google Translate, not legally binding) | |
| ES276763A1 (en) | Procedure for the preparation of 8-hydroxypenylic acid (Machine-translation by Google Translate, not legally binding) | |
| ES381369A1 (en) | Hydrocarbon conversion process and catalyst therefore | |
| ES311770A1 (en) | Procedure for the production of cycloexanone. (Machine-translation by Google Translate, not legally binding) |