ES377165A1 - A procedure for the preparation of 5- (3-cyanopropyl) -hidantoin. (Machine-translation by Google Translate, not legally binding) - Google Patents
A procedure for the preparation of 5- (3-cyanopropyl) -hidantoin. (Machine-translation by Google Translate, not legally binding)Info
- Publication number
- ES377165A1 ES377165A1 ES377165A ES377165A ES377165A1 ES 377165 A1 ES377165 A1 ES 377165A1 ES 377165 A ES377165 A ES 377165A ES 377165 A ES377165 A ES 377165A ES 377165 A1 ES377165 A1 ES 377165A1
- Authority
- ES
- Spain
- Prior art keywords
- reagent
- cyanopropyl
- translation
- procedure
- preparation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 238000000034 method Methods 0.000 title abstract 2
- -1 3-cyanopropyl Chemical group 0.000 title 1
- 239000003153 chemical reaction reagent Substances 0.000 abstract 7
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 abstract 4
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 abstract 4
- FNEARBHZFXEPFD-UHFFFAOYSA-N 5-oxopentanenitrile Chemical compound O=CCCCC#N FNEARBHZFXEPFD-UHFFFAOYSA-N 0.000 abstract 2
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 abstract 2
- 239000001569 carbon dioxide Substances 0.000 abstract 2
- 229910002092 carbon dioxide Inorganic materials 0.000 abstract 2
- 238000006243 chemical reaction Methods 0.000 abstract 2
- DBKOXARNAKRIDK-UHFFFAOYSA-N 4-(2,5-dioxoimidazolidin-4-yl)butanenitrile Chemical compound O=C1NC(CCCC#N)C(=O)N1 DBKOXARNAKRIDK-UHFFFAOYSA-N 0.000 abstract 1
- VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 abstract 1
- 229910021529 ammonia Inorganic materials 0.000 abstract 1
- 239000000908 ammonium hydroxide Substances 0.000 abstract 1
- 239000007791 liquid phase Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D233/00—Heterocyclic compounds containing 1,3-diazole or hydrogenated 1,3-diazole rings, not condensed with other rings
- C07D233/54—Heterocyclic compounds containing 1,3-diazole or hydrogenated 1,3-diazole rings, not condensed with other rings having two double bonds between ring members or between ring members and non-ring members
- C07D233/66—Heterocyclic compounds containing 1,3-diazole or hydrogenated 1,3-diazole rings, not condensed with other rings having two double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D233/72—Two oxygen atoms, e.g. hydantoin
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
A procedure for the preparation of 5- (3-cyanopropyl) -hydantoin by conversion of 4-cyanobutyraldehyde, in liquid phase, by means of a cyanided reagent, an ammonium reagent and a carbon dioxide reagent, characterized in that during the reaction with the ammonium reagent, the number of moles of the ammonium reagent present, per mole of 4-cyanobutyraldehyde to be converted, is at least two more than double the number of moles of the carbon dioxide reagent present, and therefore minus 2 moles of the ammonium reagent are used in the form of ammonia and/or ammonium hydroxide. (Machine-translation by Google Translate, not legally binding)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| NL6903445.A NL160256C (en) | 1969-03-06 | 1969-03-06 | PROCESS FOR THE PREPARATION OF 5- (3-CYANOPRO-PYL) -HYDANTOIN. |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ES377165A1 true ES377165A1 (en) | 1972-05-16 |
Family
ID=19806334
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES377165A Expired ES377165A1 (en) | 1969-03-06 | 1970-03-05 | A procedure for the preparation of 5- (3-cyanopropyl) -hidantoin. (Machine-translation by Google Translate, not legally binding) |
Country Status (15)
| Country | Link |
|---|---|
| JP (1) | JPS5425030B1 (en) |
| AT (1) | AT293434B (en) |
| BE (1) | BE746941A (en) |
| BG (1) | BG19801A3 (en) |
| CH (1) | CH565158A5 (en) |
| CS (1) | CS162706B2 (en) |
| DE (1) | DE2010696A1 (en) |
| ES (1) | ES377165A1 (en) |
| FR (1) | FR2037516A5 (en) |
| GB (1) | GB1290943A (en) |
| IL (1) | IL33967A0 (en) |
| NL (1) | NL160256C (en) |
| PL (1) | PL80469B1 (en) |
| RO (1) | RO56848A (en) |
| SE (1) | SE349804B (en) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| NL166920C (en) * | 1970-12-23 | 1981-10-15 | Stamicarbon | METHOD FOR PREPARING LYSINE OR A LYSINE COMPOUND |
-
1969
- 1969-03-06 NL NL6903445.A patent/NL160256C/en not_active IP Right Cessation
-
1970
- 1970-02-23 GB GB1290943D patent/GB1290943A/en not_active Expired
- 1970-02-25 IL IL33967A patent/IL33967A0/en unknown
- 1970-02-27 BG BG014074A patent/BG19801A3/en unknown
- 1970-03-03 AT AT196270A patent/AT293434B/en not_active IP Right Cessation
- 1970-03-03 FR FR7007505A patent/FR2037516A5/fr not_active Expired
- 1970-03-04 JP JP1863470A patent/JPS5425030B1/ja active Pending
- 1970-03-05 ES ES377165A patent/ES377165A1/en not_active Expired
- 1970-03-05 PL PL1970139221A patent/PL80469B1/pl unknown
- 1970-03-05 RO RO62665A patent/RO56848A/ro unknown
- 1970-03-06 DE DE19702010696 patent/DE2010696A1/en active Pending
- 1970-03-06 CH CH336970A patent/CH565158A5/xx not_active IP Right Cessation
- 1970-03-06 BE BE746941D patent/BE746941A/en not_active IP Right Cessation
- 1970-03-06 SE SE03046/70A patent/SE349804B/xx unknown
- 1970-03-06 CS CS1528A patent/CS162706B2/cs unknown
Also Published As
| Publication number | Publication date |
|---|---|
| BE746941A (en) | 1970-09-07 |
| BG19801A3 (en) | 1975-10-10 |
| DE2010696A1 (en) | 1970-10-15 |
| PL80469B1 (en) | 1975-08-30 |
| RO56848A (en) | 1974-09-01 |
| NL6903445A (en) | 1970-09-08 |
| CS162706B2 (en) | 1975-07-15 |
| JPS5425030B1 (en) | 1979-08-24 |
| GB1290943A (en) | 1972-09-27 |
| NL160256C (en) | 1979-10-15 |
| AT293434B (en) | 1971-10-11 |
| NL160256B (en) | 1979-05-15 |
| FR2037516A5 (en) | 1970-12-31 |
| CH565158A5 (en) | 1975-08-15 |
| SE349804B (en) | 1972-10-09 |
| IL33967A0 (en) | 1970-04-20 |
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