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ES339439A1 - Process for producing beta-Methylmercaptopropionaldehyde - Google Patents

Process for producing beta-Methylmercaptopropionaldehyde

Info

Publication number
ES339439A1
ES339439A1 ES339439A ES339439A ES339439A1 ES 339439 A1 ES339439 A1 ES 339439A1 ES 339439 A ES339439 A ES 339439A ES 339439 A ES339439 A ES 339439A ES 339439 A1 ES339439 A1 ES 339439A1
Authority
ES
Spain
Prior art keywords
methylmercaptopropionaldehyde
less
producing beta
acrolein
condensing
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
ES339439A
Other languages
Spanish (es)
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Sumitomo Chemical Co Ltd
Original Assignee
Sumitomo Chemical Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Sumitomo Chemical Co Ltd filed Critical Sumitomo Chemical Co Ltd
Publication of ES339439A1 publication Critical patent/ES339439A1/en
Expired legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C323/00—Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

Abstract

A process for the production of #-methylmercaptopropionaldehyde comprises (1) reacting methyl mercaptan with acrolein in a molar ratio of 1 : 1À001-1 1À20 and in the presence of a catalyst, (2) removing from the product of step (1) impurities having a lower boiling point than #-methylmercaptopropionaldehyde by rectification under a pressure of less than 200 mm. Hg. with a retention time of less than 60 minutes, while keeping the temperature of the #-methylmercaptopropionaldehyde below 125 degrees and (3) condensing the vapour distilled in step (2) by contacting it with a previously condensed and cooled distillate from step (2).
ES339439A 1966-04-18 1967-04-18 Process for producing beta-Methylmercaptopropionaldehyde Expired ES339439A1 (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP2486866 1966-04-18

Publications (1)

Publication Number Publication Date
ES339439A1 true ES339439A1 (en) 1968-05-01

Family

ID=12150171

Family Applications (1)

Application Number Title Priority Date Filing Date
ES339439A Expired ES339439A1 (en) 1966-04-18 1967-04-18 Process for producing beta-Methylmercaptopropionaldehyde

Country Status (5)

Country Link
BE (1) BE697178A (en)
DE (1) DE1618879B1 (en)
ES (1) ES339439A1 (en)
GB (1) GB1173174A (en)
NL (1) NL6705426A (en)

Families Citing this family (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5352837A (en) * 1993-06-08 1994-10-04 Novus International, Inc. Process for the preparation of 3-(methylthio)propanal
US5925794A (en) * 1993-06-08 1999-07-20 Novus International, Inc. Process for the preparation of 3-(methylthio)propanal
US5905171A (en) 1995-06-22 1999-05-18 Novus International, Inc. Process for the preparation of 3-(methylthio)propanal
US5637766A (en) * 1993-06-08 1997-06-10 Novus International, Inc. Process for the preparation of 3-(methylthio) propanal
US5663409A (en) * 1995-06-07 1997-09-02 Novus International, Inc. Process for the preparation of 3-(methylthio) propanal and 2-hydroxy-4-(methylthio) butanenitrile
DE102010064250A1 (en) * 2010-12-28 2012-06-28 Evonik Degussa Gmbh Process for the preparation of methylmercaptopropionaldehyde
EP3205643A1 (en) 2016-02-15 2017-08-16 Evonik Degussa GmbH Method for the preparation of 3-methylthiopropionaldehyde
EP3339290B1 (en) 2016-12-22 2019-06-19 Evonik Degussa GmbH Storage of 3-methylthiopropionaldehyde and methyl mercaptan
EP3656760A1 (en) 2018-11-21 2020-05-27 Evonik Operations GmbH Storage stable form of 3-methylthiopropionaldehyde

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CH253951A (en) * 1945-10-25 1948-04-15 Merck & Co Inc Process for the preparation of B-methylmercapto-propionaldehyde.
GB687483A (en) * 1949-07-04 1953-02-18 Dow Chemical Co Improved method for the production of beta-methylmercapto-propionaldehyde
US2676190A (en) * 1951-10-23 1954-04-20 Du Pont Process for the manufacture of beta-methylmercapto-propionaldehyde
US2776996A (en) * 1955-12-22 1957-01-08 Du Pont Manufacture of beta-methylmercaptopropionaldehyde

Also Published As

Publication number Publication date
NL6705426A (en) 1967-10-19
BE697178A (en) 1967-10-02
GB1173174A (en) 1969-12-03
DE1618879B1 (en) 1971-12-16

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