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ES2109089T3 - Procedimiento para la fabricacion de cuerpos moldeados de celulosa. - Google Patents

Procedimiento para la fabricacion de cuerpos moldeados de celulosa.

Info

Publication number
ES2109089T3
ES2109089T3 ES95906834T ES95906834T ES2109089T3 ES 2109089 T3 ES2109089 T3 ES 2109089T3 ES 95906834 T ES95906834 T ES 95906834T ES 95906834 T ES95906834 T ES 95906834T ES 2109089 T3 ES2109089 T3 ES 2109089T3
Authority
ES
Spain
Prior art keywords
cellulose
solution
less
molded
aqueous
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
ES95906834T
Other languages
English (en)
Other versions
ES2109089T5 (es
Inventor
Wolfram Kalt
Heinrich Firgo
Johann Manner
Eduard Mulleder
Bruno Mangeng
Arnold Nigsch
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Lenzing AG
Original Assignee
Lenzing AG
Chemiefaser Lenzing AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=3490408&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=ES2109089(T3) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by Lenzing AG, Chemiefaser Lenzing AG filed Critical Lenzing AG
Application granted granted Critical
Publication of ES2109089T3 publication Critical patent/ES2109089T3/es
Publication of ES2109089T5 publication Critical patent/ES2109089T5/es
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C291/00—Compounds containing carbon and nitrogen and having functional groups not covered by groups C07C201/00 - C07C281/00
    • C07C291/02—Compounds containing carbon and nitrogen and having functional groups not covered by groups C07C201/00 - C07C281/00 containing nitrogen-oxide bonds
    • C07C291/04—Compounds containing carbon and nitrogen and having functional groups not covered by groups C07C201/00 - C07C281/00 containing nitrogen-oxide bonds containing amino-oxide bonds
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08B—POLYSACCHARIDES; DERIVATIVES THEREOF
    • C08B1/00—Preparatory treatment of cellulose for making derivatives thereof, e.g. pre-treatment, pre-soaking, activation
    • C08B1/003—Preparation of cellulose solutions, i.e. dopes, with different possible solvents, e.g. ionic liquids
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J3/00—Processes of treating or compounding macromolecular substances
    • C08J3/02—Making solutions, dispersions, lattices or gels by other methods than by solution, emulsion or suspension polymerisation techniques
    • C08J3/09—Making solutions, dispersions, lattices or gels by other methods than by solution, emulsion or suspension polymerisation techniques in organic liquids
    • C08J3/091—Making solutions, dispersions, lattices or gels by other methods than by solution, emulsion or suspension polymerisation techniques in organic liquids characterised by the chemical constitution of the organic liquid
    • C08J3/096—Nitrogen containing compounds
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L1/00—Compositions of cellulose, modified cellulose or cellulose derivatives
    • C08L1/02—Cellulose; Modified cellulose
    • D—TEXTILES; PAPER
    • D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
    • D01F2/00—Monocomponent artificial filaments or the like of cellulose or cellulose derivatives; Manufacture thereof
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2301/00—Characterised by the use of cellulose, modified cellulose or cellulose derivatives

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Health & Medical Sciences (AREA)
  • General Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Biochemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Dispersion Chemistry (AREA)
  • Textile Engineering (AREA)
  • Polysaccharides And Polysaccharide Derivatives (AREA)
  • Manufacture Of Macromolecular Shaped Articles (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Artificial Filaments (AREA)
  • Paper (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)
  • Treatment Of Water By Ion Exchange (AREA)
  • Confectionery (AREA)
  • Processes Of Treating Macromolecular Substances (AREA)
  • Moulding By Coating Moulds (AREA)

Abstract

LA INVENCION SE REFIERE A UN PROCESO PARA LA ELABORACION DE CUERPOS MOLDEADOS DE CELULOSA, COMPRENDIENDO EL INDICADO PROCESO LAS SIGUIENTES ETAPAS: (A) LA CELULOSA SE DISUELVE EN UNA SOLUCION ACUOSA DE UN OXIDO AMINO TERCIARIO, EN PARTICULAR NMETILMORFOLINA - N-OXIDO (NMMO), PARA FORMAR UNA SOLUCION DE CELULOSA QUE PUEDE SER MOLDEADA; (B) MOLDEADO DE LA SOLUCION DE CELULOSA Y GUIA DE LA SOLUCION DE CELULOSA MOLDEADA DENTRO DE UN BAÑO DE PRECIPITACION ACUOSA EN DONDE SE PRECIPITA LA CELULOSA, DE FORMA QUE SE OBTIENE UN CUERPO MOLDEADO Y SE UTILIZA EL BAÑO DE PRECIPITACION; (C) REGENERACION DEL BAÑO DE PRECIPITACION UTILIZADO, CON UNA SOLUCION DE OXIDO DE AMINO ACUOSO, REGENERADO, SIENDO FORMADO CON UTILIZACION EN UNA ETAPA (A) CONTRA LA CELULOSA DE DISOLUCION. LA INVENCION SE CARACTERIZA DE TAL MODO QUE EN LA ETAPA (A) SE UTILIZA UNA SOLUCION DE OXIDO AMINO ACUOSO REGENERADO QUE DISPONE DE UN PH EN LA ZONA DE LOS LIMITES SUPERIOR E INFERIOR DEFINIDOS, COMO UNA FUNCION DE CONCENTRACION DE OXIDO DE AMINO TERCIARIO, MEDIANTE LA ECUACION PH = - 0,0015 X A{SUP,2} + 0,2816 X A + F, A, SIENDO A LA CONCENTRACION DE OXIDO DE AMINO TERCIARIO EN LA SOLUCION ACUOSA, EXPRESADA EN TANTO % EN PESO DE SOLUCION ACUOSA, Y SATISFACIENDO LA CONDICION: 40 % MENOR IGUAL QUE A MENOR IGUAL QUE 86 %, Y CON PREFERENCIA MENOR IGUAL 70 % DE A MENOR IGUAL 80 %, Y TENIENDO EL VALOR 1,00 PARA EL LIMITE SUPERIOR Y -1,80 Y CON PREFERENCIA -1,00 PARA EL LIMITE INFERIOR.
ES95906834T 1994-03-01 1995-02-01 Procedimiento para la fabricacion de cuerpos moldeados de celulosa. Expired - Lifetime ES2109089T5 (es)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
AT0043094A ATA43094A (de) 1994-03-01 1994-03-01 Verfahren zur herstellung cellulosischer formkörper, lösung eines tert. aminoxids und ihre aufarbeitung
AT430/94 1994-03-01

Publications (2)

Publication Number Publication Date
ES2109089T3 true ES2109089T3 (es) 1998-01-01
ES2109089T5 ES2109089T5 (es) 2006-05-16

Family

ID=3490408

Family Applications (1)

Application Number Title Priority Date Filing Date
ES95906834T Expired - Lifetime ES2109089T5 (es) 1994-03-01 1995-02-01 Procedimiento para la fabricacion de cuerpos moldeados de celulosa.

Country Status (36)

Country Link
US (2) US5602247A (es)
EP (2) EP0696330B1 (es)
JP (2) JP2758991B2 (es)
KR (1) KR0173006B1 (es)
CN (2) CN1124044A (es)
AT (3) ATA43094A (es)
AU (2) AU680337B2 (es)
BG (1) BG62409B1 (es)
BR (2) BR9505855A (es)
CA (1) CA2160785C (es)
CZ (1) CZ290928B6 (es)
DE (5) DE59500899D1 (es)
EE (1) EE9500061A (es)
ES (1) ES2109089T5 (es)
FI (2) FI955205A7 (es)
GB (2) GB2291833B (es)
GR (1) GR3025123T3 (es)
HR (1) HRP950076B1 (es)
HU (1) HU214289B (es)
ID (1) ID917B (es)
IL (1) IL112678A (es)
LV (1) LV11331B (es)
MA (1) MA23460A1 (es)
MY (1) MY115340A (es)
NO (2) NO954351L (es)
NZ (1) NZ278816A (es)
PE (1) PE46295A1 (es)
PL (1) PL181246B1 (es)
RO (1) RO113353B1 (es)
RU (1) RU2142523C1 (es)
SI (1) SI0695324T2 (es)
SK (1) SK281026B6 (es)
TW (1) TW460479B (es)
WO (2) WO1995023885A1 (es)
YU (1) YU48932B (es)
ZA (1) ZA951333B (es)

Families Citing this family (26)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
ATA43094A (de) * 1994-03-01 1995-04-15 Chemiefaser Lenzing Ag Verfahren zur herstellung cellulosischer formkörper, lösung eines tert. aminoxids und ihre aufarbeitung
AT402643B (de) * 1995-08-18 1997-07-25 Chemiefaser Lenzing Ag Verfahren zur reinigung einer wässrigen lösung verfahren zur reinigung einer wässrigen lösung eines tertiären aminoxids eines tertiären aminoxids
US5858285A (en) * 1995-08-18 1999-01-12 Lenzing Aktiengesellschaft Process for the production of an aqueous solution of a tertiary amine-oxide
AT408547B (de) * 1995-09-26 2001-12-27 Chemiefaser Lenzing Ag Verfahren zum transportieren einer lösung von cellulose in einem wässrigen tertiären aminoxid
US6471727B2 (en) 1996-08-23 2002-10-29 Weyerhaeuser Company Lyocell fibers, and compositions for making the same
US6210801B1 (en) 1996-08-23 2001-04-03 Weyerhaeuser Company Lyocell fibers, and compositions for making same
US6331354B1 (en) 1996-08-23 2001-12-18 Weyerhaeuser Company Alkaline pulp having low average degree of polymerization values and method of producing the same
US6306334B1 (en) 1996-08-23 2001-10-23 The Weyerhaeuser Company Process for melt blowing continuous lyocell fibers
AT404846B (de) * 1997-06-16 1999-03-25 Chemiefaser Lenzing Ag Zusammensetzung enthaltend feine feststoffteilchen
US5942167A (en) * 1997-08-12 1999-08-24 Viskase Corporation Method of making a cellulose food casing including solvent recovery
CN1061106C (zh) * 1997-12-09 2001-01-24 宜宾丝丽雅集团有限公司 溶剂法纤维素纤维制造方法
US6096258A (en) * 1998-01-20 2000-08-01 Viskase Corporation Method and apparatus for forming a cellulose article including solvent recovery means
US6773648B2 (en) 1998-11-03 2004-08-10 Weyerhaeuser Company Meltblown process with mechanical attenuation
AT407997B (de) * 1999-08-10 2001-07-25 Chemiefaser Lenzing Ag Gefärbte cellulosische formkörper
DE10009471B4 (de) * 2000-02-28 2006-07-27 Thüringisches Institut für Textil- und Kunststoff-Forschung e.V. Verfahren zur Herstellung einer Lösung erhöhter thermischer Stabilität von Cellulose in wässrigem Aminoxid
AT410319B (de) * 2001-07-25 2003-03-25 Chemiefaser Lenzing Ag Celluloseschwamm und verfahren zu dessen herstellung
AT411769B (de) * 2002-07-12 2004-05-25 Chemiefaser Lenzing Ag Verfahren zur herstellung cellulosischer formkörper
FR2880619B1 (fr) * 2005-01-10 2010-03-12 Cebal Sas Emballages plastiques, en particulier tubes souples, contenant des substances reactives associees a un temoin de presence
ES2360828T3 (es) 2006-03-29 2011-06-09 Virginia Tech Intellectual Properties, Inc. Fraccionamiento de lignocelulosa a base de disolvente de celulosa con condiciones de reacción moderadas y ciclación de reactivos.
CA2718427C (en) * 2008-03-14 2015-01-27 Virginia Tech Intellectual Properties, Inc. Method and apparatus for lignocellulose pretreatment using a super-cellulose-solvent and highly volatile solvents
EP2565303A1 (de) * 2011-09-02 2013-03-06 Aurotec GmbH Extrusionsverfahren
US10809718B2 (en) 2017-07-28 2020-10-20 Loon Llc Systems and methods for controlling aerial vehicles
KR101904771B1 (ko) * 2017-09-22 2018-10-05 오영세 라이오셀 섬유 및 그 제조방법
US10890885B2 (en) 2017-12-21 2021-01-12 Loon Llc Managing power of aerial vehicles
CN110357972A (zh) * 2018-04-09 2019-10-22 株式会社大赛璐 乙酸纤维素的制造方法
CN109468688B (zh) * 2018-11-22 2021-06-08 绍兴美标纺织品检验有限公司 纤维素纤维的纺丝方法

Family Cites Families (20)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
AT185793B (de) * 1952-12-02 1956-06-11 Erwin Otto Haberfeld Lohnbeutel (-zettel) für die Lohnbuchhaltung
DE2000082A1 (de) * 1970-01-02 1971-07-15 Wolff Walsrode Ag Verfahren zur Verhinderung des Abbaus von Alkalicellulose
US4416698A (en) * 1977-07-26 1983-11-22 Akzona Incorporated Shaped cellulose article prepared from a solution containing cellulose dissolved in a tertiary amine N-oxide solvent and a process for making the article
US4324593A (en) * 1978-09-01 1982-04-13 Akzona Incorporated Shapeable tertiary amine N-oxide solution of cellulose, shaped cellulose product made therefrom and process for preparing the shapeable solution and cellulose products
DE3034685C2 (de) * 1980-09-13 1984-07-05 Akzo Gmbh, 5600 Wuppertal Cellulose-Form- und Spinnmasse mit geringen Anteilen an niedermolekularen Abbauprodukten
DD218104B5 (de) * 1983-10-17 1996-06-13 Thueringisches Inst Textil Verfahren zur Herstellung thermisch stabiler Cellulose-Aminoxidloesungen
US4577013A (en) * 1983-12-22 1986-03-18 Ciba-Geigy Corporation Ionically modified cellulose material, its preparation and its use
US4724207A (en) * 1984-02-02 1988-02-09 Cuno Incorporated Modified siliceous chromatographic supports
DD229708A1 (de) * 1984-12-13 1985-11-13 Schwarza Chemiefaser Verfahren zur herstellung von stabilen polymerloesungen
SU1427011A1 (ru) * 1985-08-19 1988-09-30 Предприятие П/Я А-3844 Способ регенерации N-метилморфолин-N-оксида из технологических растворов при производстве гидратцеллюлозных волокон
DD254199B5 (de) * 1986-12-04 1994-01-05 Thueringische Faser Ag Schwarz Verfahren zur reinigung waessriger n-methylmorpholin-n-oxyd-loesungen
EP0306261B1 (en) * 1987-08-31 1992-07-15 Sharp Kabushiki Kaisha Use of a cation exchange polyimide resin
AU3539989A (en) * 1988-04-12 1989-11-03 Peter Grandics Novel crosslinked cellulose chromatography media
AT392972B (de) * 1988-08-16 1991-07-25 Chemiefaser Lenzing Ag Verfahren zur herstellung von loesungen von cellulose sowie einrichtung zur durchfuehrung des verfahrens
AT392776B (de) * 1989-10-16 1991-06-10 Chemiefaser Lenzing Ag Verfahren zur reinigung waesseriger loesungen von n-methylmorpholin-n-oxid
AT395608B (de) * 1990-11-26 1993-02-25 Chemiefaser Lenzing Ag Verfahren zur reinigung von waesserigen n-methylmorpholin-n-oxid-loesungen
GB9125594D0 (en) * 1991-12-02 1992-01-29 Courtaulds Plc Purifying solutions
AT396930B (de) * 1992-01-23 1993-12-27 Chemiefaser Lenzing Ag Aminoxide
AT399519B (de) * 1993-09-14 1995-05-26 Chemiefaser Lenzing Ag Form- bzw. spinnmasse enthaltend cellulose und verfahren zur herstellung cellulosischer formkörper
ATA43094A (de) * 1994-03-01 1995-04-15 Chemiefaser Lenzing Ag Verfahren zur herstellung cellulosischer formkörper, lösung eines tert. aminoxids und ihre aufarbeitung

Also Published As

Publication number Publication date
EP0696330B1 (de) 1997-11-12
RU2142523C1 (ru) 1999-12-10
CZ290928B6 (cs) 2002-11-13
AU1527495A (en) 1995-09-18
EP0695324A1 (de) 1996-02-07
CA2160785C (en) 2007-01-09
FI955205A0 (fi) 1995-10-31
BG100106A (bg) 1996-11-29
CN1124033A (zh) 1996-06-05
GB9521214D0 (en) 1995-12-20
DE59500899D1 (de) 1997-12-04
WO1995023885A1 (de) 1995-09-08
NO954351L (no) 1995-11-07
AU690202B2 (en) 1998-04-23
IL112678A0 (en) 1995-05-26
FI955205L (fi) 1995-10-31
CN1085994C (zh) 2002-06-05
BR9505855A (pt) 1996-02-13
DE29508167U1 (de) 1995-09-07
YU12695A (sh) 1997-09-30
DE59500974D1 (de) 1997-12-18
CA2160785A1 (en) 1995-09-08
JPH08508785A (ja) 1996-09-17
GB2291834B (en) 1998-01-07
DE19580078D2 (de) 1996-06-27
RO113353B1 (ro) 1998-06-30
FI955204A0 (fi) 1995-10-31
LV11331B (en) 1996-10-20
AU680337B2 (en) 1997-07-24
HK1004778A1 (en) 1998-12-04
JP2758991B2 (ja) 1998-05-28
ES2109089T5 (es) 2006-05-16
HU214289B (hu) 1998-03-02
IL112678A (en) 2000-01-31
HRP950076B1 (en) 2000-04-30
GB2291834A (en) 1996-02-07
US5628941A (en) 1997-05-13
EP0695324B2 (de) 2005-11-16
GR3025123T3 (en) 1998-01-30
EE9500061A (et) 1996-02-15
NO954350D0 (no) 1995-10-30
SI0695324T1 (sl) 1998-02-28
NO308370B1 (no) 2000-09-04
MY115340A (en) 2003-05-31
PL311309A1 (en) 1996-02-05
NO954351D0 (no) 1995-10-30
FI955204A7 (fi) 1995-10-31
GB2291833B (en) 1997-11-26
SI0695324T2 (sl) 2006-04-30
EP0695324B1 (de) 1997-10-29
GB9521213D0 (en) 1995-12-20
CZ295095A3 (en) 1996-02-14
PE46295A1 (es) 1995-12-29
ATA43094A (de) 1995-04-15
MA23460A1 (fr) 1995-10-01
US5602247A (en) 1997-02-11
HRP950076A2 (en) 1997-02-28
FI955205A7 (fi) 1995-10-31
HU9503112D0 (en) 1996-01-29
NZ278816A (en) 1997-11-24
SK281026B6 (sk) 2000-11-07
ZA951333B (en) 1995-10-23
BR9505780A (pt) 1996-02-27
DE19580076D2 (de) 1996-06-27
TW460479B (en) 2001-10-21
ATE159746T1 (de) 1997-11-15
HUT74115A (en) 1996-11-28
EP0696330A1 (de) 1996-02-14
FI114220B (fi) 2004-09-15
LV11331A (lv) 1996-06-20
YU48932B (sh) 2002-12-10
GB2291833A (en) 1996-02-07
AU1527595A (en) 1995-09-18
PL181246B1 (pl) 2001-06-29
SK134095A3 (en) 1997-01-08
CN1124044A (zh) 1996-06-05
ATE160182T1 (de) 1997-11-15
BG62409B1 (bg) 1999-10-29
WO1995023827A1 (de) 1995-09-08
JPH08508784A (ja) 1996-09-17
JP2703117B2 (ja) 1998-01-26
KR0173006B1 (ko) 1999-03-30
ID917B (id) 1996-09-12
NO954350L (no) 1995-12-07

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