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EP1572335B1 - Micromelangeur lamellaire statique - Google Patents

Micromelangeur lamellaire statique Download PDF

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Publication number
EP1572335B1
EP1572335B1 EP03780105.7A EP03780105A EP1572335B1 EP 1572335 B1 EP1572335 B1 EP 1572335B1 EP 03780105 A EP03780105 A EP 03780105A EP 1572335 B1 EP1572335 B1 EP 1572335B1
Authority
EP
European Patent Office
Prior art keywords
micro
aperture
plate
slot
mixer according
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
EP03780105.7A
Other languages
German (de)
English (en)
Other versions
EP1572335A2 (fr
Inventor
Wolfgang Ehrfeld
Matthias Kroschel
Till Merkel
Frank Herbstritt
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Ehrfeld Mikrotechnik BTS GmbH
Original Assignee
Ehrfeld Mikrotechnik BTS GmbH
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Ehrfeld Mikrotechnik BTS GmbH filed Critical Ehrfeld Mikrotechnik BTS GmbH
Publication of EP1572335A2 publication Critical patent/EP1572335A2/fr
Application granted granted Critical
Publication of EP1572335B1 publication Critical patent/EP1572335B1/fr
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F25/00Flow mixers; Mixers for falling materials, e.g. solid particles
    • B01F25/40Static mixers
    • B01F25/42Static mixers in which the mixing is affected by moving the components jointly in changing directions, e.g. in tubes provided with baffles or obstructions
    • B01F25/421Static mixers in which the mixing is affected by moving the components jointly in changing directions, e.g. in tubes provided with baffles or obstructions by moving the components in a convoluted or labyrinthine path
    • B01F25/422Static mixers in which the mixing is affected by moving the components jointly in changing directions, e.g. in tubes provided with baffles or obstructions by moving the components in a convoluted or labyrinthine path between stacked plates, e.g. grooved or perforated plates
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F25/00Flow mixers; Mixers for falling materials, e.g. solid particles
    • B01F25/40Static mixers
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F25/00Flow mixers; Mixers for falling materials, e.g. solid particles
    • B01F25/20Jet mixers, i.e. mixers using high-speed fluid streams
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F33/00Other mixers; Mixing plants; Combinations of mixers
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F33/00Other mixers; Mixing plants; Combinations of mixers
    • B01F33/30Micromixers
    • B01F33/301Micromixers using specific means for arranging the streams to be mixed, e.g. channel geometries or dispositions
    • B01F33/3012Interdigital streams, e.g. lamellae
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F33/00Other mixers; Mixing plants; Combinations of mixers
    • B01F33/30Micromixers
    • B01F33/301Micromixers using specific means for arranging the streams to be mixed, e.g. channel geometries or dispositions
    • B01F33/3012Interdigital streams, e.g. lamellae
    • B01F33/30121Interdigital streams, e.g. lamellae the interdigital streams being concentric lamellae
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10STECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S366/00Agitating
    • Y10S366/03Micromixers: variable geometry from the pathway influences mixing/agitation of non-laminar fluid flow

Definitions

  • the invention relates to a micromixer for mixing, dispersing, emulsifying or suspending at least two fluid phases, which must contain at least one slot plate with slot openings and an aperture plate arranged above it with blind slots.
  • the slot openings in the slot plate (s) and diaphragm plate (s) are designed as through holes.
  • Static micromixers are key elements of microreaction technology.
  • Statistical micromixers exploit the principle of multilamination to achieve rapid mixing of fluid phases by diffusion. By a geometrical configuration of alternately arranged lamellae, it is possible to ensure a good mixing in the microscopic range.
  • Multilamination mixers of structured and periodically stacked thin plates have already been extensively described in the literature; Examples of this can be found in the German patents DE 44 16 343 . DE 195 40 292 . DE 199 17 156 A1 and the German patent application DE 199 28 123 , The German patent application DE 199 27 554 also describes a micromixer for mixing two or more educts, in contrast to the multilamination mixers consisting of structured and periodically stacked thin plates, the micromixer having mixing cells.
  • Each of these mixing cells has a feed chamber to which at least two groups of channel fingers adjoin, which engage in a comb-like manner between the channel fingers to form mixing areas.
  • Above the mixing area are outlet slots that extend perpendicular to the channel fingers and through which the product exits. Due to the parallel connection in two spatial directions, a significantly higher throughput is possible.
  • the advantages achieved by the invention are that the static lamination micro mixing can be manufactured inexpensively, is easy to clean and the fluids to be mixed are mixed together quickly and effectively.
  • the pressure loss is so low that it can also be used for large throughputs.

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Dispersion Chemistry (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)

Claims (13)

  1. Micro-mélangeur statique à stratification servant à mélanger, disperser, émulsifier ou mettre en suspension au moins deux phases fluides, et présentant :
    une partie inférieure de boîtier (10) qui présente des canaux séparés d'amenée (11a/b) ouverts sur le côté supérieur de la partie inférieure de boîtier,
    une plaque fendue (20) placée sur la partie inférieure de boîtier et dans laquelle des ouvertures en fente (22a/b) sont disposées par paires sous la forme d'ouvertures continues à bord fermé et d'une largeur d'au moins 500 micromètres,
    une plaque d'écran (30) placée sur la plaque fendue et présentant au moins une ouverture d'écran (31) continue, en forme de fente à bord fermé et dont la largeur est d'au moins 500 micromètres et
    un espace de mélange (45) situé au-dessus de la plaque d'écran,
    l'ouverture en fente de la paire d'ouvertures en fente ménagées dans la plaque fendue (20) recouvre par une de ses extrémités un des canaux d'amenée (11) de la partie inférieure de boîtier (10) tandis que l'autre ouverture en fente de la paire recouvre par une extrémité un autre canal d'amenée (11) ménagé dans la partie inférieure de boîtier (10), les deux ouvertures en fente de la paire formant avec la même ouverture (31) de l'écran ménagée dans la plaque d'écran exactement une surface de superposition.
  2. Micro-mélangeur selon la revendication 1, caractérisé en ce que la section transversale des ouvertures en fente ménagées dans la plaque a la forme d'un entonnoir ou d'un biseau.
  3. Micro-mélangeur selon les revendications 1 ou 2, caractérisé en ce que les fentes ménagées dans la plaque d'écran sont parallèles et décalées l'une par rapport à l'autre et/ou disposées l'une par rapport à l'autre selon un motif périodique.
  4. Micro-mélangeur selon les revendications 1 à 3, caractérisé en ce que les ouvertures ménagées dans la plaque fendue et les ouvertures ménagées dans la plaque d'écran sont disposées à un angle mutuel de 90°.
  5. Micro-mélangeur selon les revendications 1 à 4, caractérisé en ce que les ouvertures ménagées dans la plaque fendue et les ouvertures ménagées dans la plaque d'écran ont une largeur inférieure à 100 µm.
  6. Micro-mélangeur selon les revendications 1 à 5, caractérisé en ce que la plaque fendue et la plaque d'écran sont réalisées totalement ou en partie en métal, verre, céramique, matière synthétique ou en une combinaison de ces matériaux.
  7. Micro-mélangeur selon les revendications 1 à 6, caractérisé en ce que la plaque fendue et la plaque d'écran sont réalisées par estampage, gaufrage, fraisage, érosion, gravure, gravure au plasma, découpe au laser, enlèvement au laser ou par la technique dite LIGA, mais de préférence par découpe au laser ou par la technique LIGA.
  8. Micro-mélangeur selon les revendications 1 à 7, caractérisé en ce que la plaque fendue et la plaque d'écran sont constituées d'un empilement de minces plaques micro-structurées.
  9. Micro-mélangeur selon la revendication 8, caractérisé en ce que les minces plaques micro-structurées sont reliées les unes aux autres en correspondance de matière par brasage, soudage, soudage par diffusion, collage ou en correspondance mécanique par vissage, compression ou rivetage.
  10. Micro-mélangeur selon les revendications 1 à 9, caractérisé en ce que le micro-mélangeur est placé dans un boîtier prévu dans ce but.
  11. Micro-mélangeur selon les revendications 1 à 10, caractérisé en ce que le boîtier contient des canaux qui permettent une répartition spatiale des phases fluides.
  12. Micro-mélangeur selon les revendications 1 à 11, caractérisé en ce que les canaux de répartition des fluides sont disposés dans le boîtier en parallèle et décalage mutuel, radialement, concentriquement ou les uns derrière les autres.
  13. Procédé de mélange, de dispersion, d'émulsification ou de mise en suspension d'au moins deux phases fluides, caractérisé en ce qu'il utilise au moins un micro-mélangeur statique à stratification selon l'une des revendications 1 à 12.
EP03780105.7A 2002-12-07 2003-12-03 Micromelangeur lamellaire statique Expired - Lifetime EP1572335B1 (fr)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
DE20218972U 2002-12-07
DE20218972U DE20218972U1 (de) 2002-12-07 2002-12-07 Statischer Laminationsmikrovermischer
PCT/EP2003/013603 WO2004052518A2 (fr) 2002-12-07 2003-12-03 Micromelangeur lamellaire statique

Publications (2)

Publication Number Publication Date
EP1572335A2 EP1572335A2 (fr) 2005-09-14
EP1572335B1 true EP1572335B1 (fr) 2013-05-29

Family

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Family Applications (1)

Application Number Title Priority Date Filing Date
EP03780105.7A Expired - Lifetime EP1572335B1 (fr) 2002-12-07 2003-12-03 Micromelangeur lamellaire statique

Country Status (8)

Country Link
US (1) US7909502B2 (fr)
EP (1) EP1572335B1 (fr)
JP (2) JP4847700B2 (fr)
KR (1) KR100806401B1 (fr)
CN (1) CN100360218C (fr)
AU (1) AU2003288216A1 (fr)
DE (1) DE20218972U1 (fr)
WO (1) WO2004052518A2 (fr)

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CN100360218C (zh) 2008-01-09
JP2011183386A (ja) 2011-09-22
KR100806401B1 (ko) 2008-02-21
KR20050085326A (ko) 2005-08-29
AU2003288216A8 (en) 2004-06-30
DE20218972U1 (de) 2003-02-13
CN1780681A (zh) 2006-05-31
US20060087917A1 (en) 2006-04-27
JP4847700B2 (ja) 2011-12-28
JP2006508795A (ja) 2006-03-16
AU2003288216A1 (en) 2004-06-30
US7909502B2 (en) 2011-03-22
WO2004052518A2 (fr) 2004-06-24
WO2004052518A3 (fr) 2005-06-09
EP1572335A2 (fr) 2005-09-14

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