DE2007743C - Reaction beaker - Google Patents

Description

1 sheet of drawings

Claims (1)

ι 2 The invention relates to an advantage for rotation because it is completely constant Normally only with suitable reaction beaker for rotational speed around its longitudinal axis the chemical conversion and suction can be achieved at a very high cost. In "a · - Thin film, with a removal groove in the upper individual, a speed-independent keu can be from Part of the inner surface of the cup. 5 Determine 1400 rpm upwards. Through the publication of P. Edman and these properties of G. Begg according to the invention in the journal "European Journal of Reaction Beakers also have an extensive biochemistry", March 1967, pp. 80 to 90, one is referred to as independence from temperature changes to the "Sequenator" Analyzer to the sequence. Finally, one can also become familiar with the complicated conduct of reactions on thin-film films as well as those provided in known devices for adding the agents to a rotating reaction beaker. The purpose of the device is to save complex ventilation devices for sequences in proteins and peptides for the structure of the storage vessels of the agents,
Enlightenment to a suitable degradation process but the most important advantage arises in throwing. This degradation process takes place in an inert context with the solution of the Erfin nitrogen atmosphere provided in the rotating training task, since a quantitative reaction of the thin-film film forming the reaction beaker with the added agents of the substance to be examined. As a result of the effect, the centrifugal forces sucked into the beaker rises completely without any interference without any reaction from the centrifugal forces. The obligatory high-height cup is used to create a thin film delimitation of the thin-layer film and the addition of various, film-shaped constrictions prevents any uncontrolled covering agents of the desired reaction from bare entrainment of the thin-layer films. Subjected thereby. The film liquid rises further, the wetting of the thin film is also achieved and the added agents collect in a reproducible manner on the upper edge of the beaker 35, which is provided for removal groove, which is sunk into the inner surface, a basic condition for carrying out one of the reaction cups and a deep quantitative reaction represents
of about 1 mm. The depth of the removal groove is preferably greater than the thickness of the thin-film film by means of a liquid immersed in the same. This causes the hose to be sucked out. 30 at the upper edge of the step-shaped constriction. With such an arrangement, the complete tearing of the liquid film and a disadvantage that the suction tube dipping into the extraction groove from the extraction groove causes turbulence in the on the thin film in the lower part of the cup Groove-filling liquid causes, whereby inner surface is excluded,
This turbulence retrospectively affects the thinness. an iuialer section of a layered film on the inner surface of the reaction beaker transferring an exemplary embodiment of the reac according to the invention and disrupting the course of the reaction. The erions cup is shown, the turbulence mentioned in more detail will also call changes. The lower part of the cylindrical inner cup film protrudes from the height and uniformity of the thin film, whereby a quantitative conversion 40 walled on which the thin film, not shown, can be negatively influenced. film forms is denoted by L in the figure. In the present invention, therefore, the upper part of the inner surface of the cup is based on a dispensing device, the difficulties mentioned are provided on groove 2, into which a removal hose, not shown, dips easily and with little effort. lateral- This object is achieved according to the invention 45 Between the removal groove 2 and the lower through a step-shaped narrowing between the part 1 of the cup inner surface, a step-shaped removal groove and the lower part of the cup inner Veiengung3 is provided, which in the area shown. Embodiment at the upper edge directly into the through this step-shaped narrowing, which merges in front of removal groove 2. In this embodiment, the stepped constriction 3 has the shape of the thin-layer film on the entire lower part of a cylindrical ring. What is important here is the part of the inner surface of the cup, both in terms of its step-like transition from the lower part 1 of the height and in terms of its thickness exactly and reproducibly.
bar, whereby a quantitative reaction of the _D ...
added agents with the substances of the thin patent claims:
layer film is guaranteed. 1. Bringing this stepped constriction more appropriately to the rotation around its longitudinal axis, surprisingly, there are still further advantages for the chemical reaction, and suction of a thin film with a removal groove in the upper part of the Cup inner weight fall. As a result of the constant area achieved, characterized by an area of the thin-layer film, there is a largely continuous constriction (3) between the dependence of the reaction on the viscosity, acceptance groove (2) and the lower part (1) of the surface tension and Volume dosing of the added cup inner surface. benen agents achieved, In addition, the reaction 2. Reaction beaker according to claim I, characterized also characterized by the speed of rotation of the reaction 65 that the constriction (3) is immediate bechcr-v independently, which passes an extraordinary cash into the removal groove (2).