DE15736193T1 - Fluorfreie wasserabstossende zusammensetzung - Google Patents
Fluorfreie wasserabstossende zusammensetzung Download PDFInfo
- Publication number
- DE15736193T1 DE15736193T1 DE15736193.2T DE15736193T DE15736193T1 DE 15736193 T1 DE15736193 T1 DE 15736193T1 DE 15736193 T DE15736193 T DE 15736193T DE 15736193 T1 DE15736193 T1 DE 15736193T1
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- 239000000203 mixture Substances 0.000 title claims abstract 22
- -1 polysiloxane Polymers 0.000 claims abstract 23
- 239000000178 monomer Substances 0.000 claims abstract 11
- 125000004432 carbon atom Chemical group C* 0.000 claims abstract 9
- 125000003158 alcohol group Chemical group 0.000 claims abstract 4
- 239000003960 organic solvent Substances 0.000 claims abstract 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract 4
- 229920000877 Melamine resin Polymers 0.000 claims abstract 2
- 239000004640 Melamine resin Substances 0.000 claims abstract 2
- 125000006297 carbonyl amino group Chemical group [H]N([*:2])C([*:1])=O 0.000 claims abstract 2
- 125000003055 glycidyl group Chemical group C(C1CO1)* 0.000 claims abstract 2
- 239000012948 isocyanate Substances 0.000 claims abstract 2
- 150000002513 isocyanates Chemical class 0.000 claims abstract 2
- 229920000058 polyacrylate Polymers 0.000 claims abstract 2
- 229920001296 polysiloxane Polymers 0.000 claims abstract 2
- 239000000758 substrate Substances 0.000 claims 8
- 230000015572 biosynthetic process Effects 0.000 claims 7
- 238000000034 method Methods 0.000 claims 5
- 239000001993 wax Substances 0.000 claims 5
- 125000004122 cyclic group Chemical group 0.000 claims 2
- 238000006116 polymerization reaction Methods 0.000 claims 2
- 239000004753 textile Substances 0.000 claims 2
- 150000001491 aromatic compounds Chemical class 0.000 claims 1
- 125000002511 behenyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 claims 1
- 125000003901 ceryl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 claims 1
- 125000001309 chloro group Chemical group Cl* 0.000 claims 1
- 150000001875 compounds Chemical class 0.000 claims 1
- 125000001995 cyclobutyl group Chemical group [H]C1([H])C([H])([H])C([H])(*)C1([H])[H] 0.000 claims 1
- 125000000113 cyclohexyl group Chemical group [H]C1([H])C([H])([H])C([H])([H])C([H])(*)C([H])([H])C1([H])[H] 0.000 claims 1
- 125000001511 cyclopentyl group Chemical group [H]C1([H])C([H])([H])C([H])([H])C([H])(*)C1([H])[H] 0.000 claims 1
- 125000001559 cyclopropyl group Chemical group [H]C1([H])C([H])([H])C1([H])* 0.000 claims 1
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 claims 1
- 239000004744 fabric Substances 0.000 claims 1
- 239000000835 fiber Substances 0.000 claims 1
- 125000000959 isobutyl group Chemical group [H]C([H])([H])C([H])(C([H])([H])[H])C([H])([H])* 0.000 claims 1
- 125000001449 isopropyl group Chemical group [H]C([H])([H])C([H])(*)C([H])([H])[H] 0.000 claims 1
- 239000010985 leather Substances 0.000 claims 1
- 238000002844 melting Methods 0.000 claims 1
- 230000008018 melting Effects 0.000 claims 1
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 claims 1
- 125000001802 myricyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 claims 1
- 125000001280 n-hexyl group Chemical group C(CCCCC)* 0.000 claims 1
- 125000000740 n-pentyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 claims 1
- 125000000913 palmityl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 claims 1
- 239000000123 paper Substances 0.000 claims 1
- 239000012188 paraffin wax Substances 0.000 claims 1
- 230000000379 polymerizing effect Effects 0.000 claims 1
- 125000002914 sec-butyl group Chemical group [H]C([H])([H])C([H])([H])C([H])(*)C([H])([H])[H] 0.000 claims 1
- 125000000999 tert-butyl group Chemical group [H]C([H])([H])C(*)(C([H])([H])[H])C([H])([H])[H] 0.000 claims 1
Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/02—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with hydrocarbons
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- C08F220/10—Esters
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- C08F220/18—Esters of monohydric alcohols or phenols of phenols or of alcohols containing two or more carbon atoms with acrylic or methacrylic acids
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- C08F220/18—Esters of monohydric alcohols or phenols of phenols or of alcohols containing two or more carbon atoms with acrylic or methacrylic acids
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Abstract
Zusammensetzung, aufweisend mindestens die Komponenten (A) und (B) und gegebenenfalls mindestens eine der Komponenten (C) bis (E): (A) Polyacrylat erhalten durch Polymerisation der Monomeren (M1) CH2=CR3COO-R1 mit (M2) CH2=CR3COO-R2 und gegebenenfalls (M3) CH2=CR3-X-R4; (B) Wachs; (C) inaktiviertes Isocyanat; (D) organisches Polysiloxan; (E) Melaminharz; wobei R1 der Alkoholrest in Monomer (M1) enthaltend von 1 bis 8 Kohlenstoffatomen ist; R2 der Alkoholrest in Monomer (M2) enthaltend von 9 bis 40 Kohlenstoffatomen ist; R3 H, CH3 oder C2H5 ist; X COO oder CONH ist; R4 Glycidyl oder CH2(CH2)n-OR5 ist, wobei n eine ganze Zahl im Bereich von 1–10 ist und R5 H oder ein Rest enthaltend von 1 bis 6 Kohlenstoffatomen ist; und wobei die Zusammensetzung auf Wasser und/oder einem organischen Lösungsmittel basiert und fluorfrei ist.
Claims (15)
- Zusammensetzung, aufweisend mindestens die Komponenten (A) und (B) und gegebenenfalls mindestens eine der Komponenten (C) bis (E): (A) Polyacrylat erhalten durch Polymerisation der Monomeren (M1) CH2=CR3COO-R1 mit (M2) CH2=CR3COO-R2 und gegebenenfalls (M3) CH2=CR3-X-R4; (B) Wachs; (C) inaktiviertes Isocyanat; (D) organisches Polysiloxan; (E) Melaminharz; wobei R1 der Alkoholrest in Monomer (M1) enthaltend von 1 bis 8 Kohlenstoffatomen ist; R2 der Alkoholrest in Monomer (M2) enthaltend von 9 bis 40 Kohlenstoffatomen ist; R3 H, CH3 oder C2H5 ist; X COO oder CONH ist; R4 Glycidyl oder CH2(CH2)n-OR5 ist, wobei n eine ganze Zahl im Bereich von 1–10 ist und R5 H oder ein Rest enthaltend von 1 bis 6 Kohlenstoffatomen ist; und wobei die Zusammensetzung auf Wasser und/oder einem organischen Lösungsmittel basiert und fluorfrei ist.
- Zusammensetzung nach Anspruch 1, wobei R1 von 1 bis 6 Kohlenstoffatome enthält und R2 von 12 bis 40 Kohlenstoffatome enthält.
- Zusammensetzung nach Anspruch 1 oder 2, wobei R1 verzweigtes oder unverzweigtes oder zyklisches C1-C6-Alkyl ist und R2 verzweigtes oder unverzweigtes oder zyklisches C12-C40-Alkyl ist.
- Zusammensetzung nach einem der vorhergehenden Ansprüche, wobei R1 ausgewählt ist aus einer oder mehreren der Gruppe bestehend aus Methyl, Ethyl, n-Propyl, iso-Propyl, n-Butyl, iso-Butyl, sek.-Butyl, tert.-Butyl, n-Pentyl und Isomere davon, n-Hexyl und Isomere davon, Cyclopropyl, Cyclobutyl, Cyclopentyl, Cyclohexyl; und R2 ausgewählt ist aus einer oder mehreren der Gruppe bestehend aus n-Dodecyl (lauryl) und Isomeren davon, n-Tridecyl und Isomeren davon, n-Tetradecyl (myristyl) und Isomere davon, n-Pentadecyl und Isomere davon, N-Hexadecyl (Cetyl) und Isomere davon, n-Heptadecyl und Isomere davon, n-Octadecyl (stearyl) und Isomere davon, n-Nonadecyl und Isomere davon, n-Eicosyl und Isomere davon, n-Heneicosyl und Isomere davon, n-Docosyl (Behenyl) und Isomere davon, n-Tricosyl und Isomere davon, n-Tetracosyl und Isomere davon, n-Pentacosyl und Isomere davon, n-Hexacosyl (ceryl) und Isomere davon, n-Heptacosyl und Isomere davon, n-Octacosyl und Isomere davon, n-Nonacosyl und Isomere davon, n-Triacontyl (Myricyl) und Isomere davon.
- Zusammensetzung nach einem der vorhergehenden Ansprüche, wobei (A) bei der Polymerisation von 5 bis 45 Gew.-% Monomer (M1) mit 55 bis 95 Gew.-% Monomer (M2) bezogen auf die Gesamtmenge von (A) (= 100 Gew.-%); oder 5 bis 44 Gew.-% Monomer (M1) mit 55 bis 94 Gew.-% Monomer (M2) und 0,1 bis 20 Gew.-% (M3) bezogen auf die Gesamtmenge an (A) (= 100 Gew.-%) erhalten wird.
- Zusammensetzung nach einem der vorhergehenden Ansprüche, wobei das Wachs einen Schmelzpunkt im Bereich von 50 bis 130°C oder 60 bis 90°C aufweist.
- Zusammensetzung nach einem der vorhergehenden Ansprüche, wobei das Wachs ein Paraffinwachs ist.
- Zusammensetzung nach einem der vorhergehenden Ansprüche, wobei die Zusammensetzung von 5–90 Gew.-% (A); 5–90 Gew.-% (B); 0–40 Gew.-% (C); 0–40 Gew.-% (D); 0–40 Gew.-% (E); 0,1–90 Gew.-% Wasser und/oder ein organisches Lösungsmittel; bezogen auf die Gesamtmenge der Zusammensetzung (= 100 Gew.-%) aufgeweist.
- Zusammensetzung nach einem der vorhergehenden Ansprüche, wobei die Zusammensetzung keine Verbindungen enthält, die N-Methylolgruppen oder Chlorgruppen aufweisen.
- Verfahren zur Herstellung einer Zusammensetzung nach einem der vorhergehenden Ansprüche, aufweisend mindestens die Schritte (C1) bis (C2): (C1) Homogenisieren einer Mischung aus mindestens Monomeren (M1) und (M2) und einer Komponente (B) und Wasser und/oder einem organischen Lösungsmittel; (C2) Polymerisieren der in Schritt (C1) erhaltenen Mischung.
- Verfahren zur Behandlung eines Substrats, aufweisend mindestens Schritt (S1): (S1) Kontaktieren eines Substrats mit der in einem der Ansprüche 1 bis 9 definierten Zusammensetzung oder Kontaktieren eines Substrats mit der Zusammensetzung, die gemäß dem Verfahren nach Anspruch 10 hergestellt wurde.
- Substrat, aufweisend mindestens die Komponenten (A) und (B) wie in Anspruch 1 definiert.
- Substrat nach Anspruch 12, behandelt nach dem Verfahren gemäß Anspruch 11.
- Substrat nach Anspruch 12 oder 13 oder erhalten nach dem Verfahren nach Anspruch 11, wobei das Substrat in Form einer linearen Formation wie Faden und Garn, in Form einer ebenen Formation wie Gewebe, gestricktem Gewebe, geknotetem Gewebe, Vliesstoff, Filz oder in Form einer räumlichen Formation wie einem Schlauch und Outwear für Frauen, Männer und Kinder vorliegt; oder wobei das Substrat ein Textil, eine Faser, Gewebe, Papier, Vlies, Leder oder eine Kombination von zwei oder mehreren davon ist.
- Verwendung einer Zusammensetzung nach einem der Ansprüche 1 bis 9 oder Verwendung eines Wachses, das n-Paraffine in einer Menge von 75 bis 95 Gew.-% und Isoparaffine und/oder Cycloparaffine und/oder aromatische Verbindungen in einer Menge von 5 bis 25 Gew.-%, bezogen auf die Gesamtmenge des Wachses aufweist oder daraus besteht, wobei die n-Paraffine 20 bis 60 Kohlenstoffatome aufweisen, und wobei vorzugsweise die n-Paraffine ein Molekulargewicht von 300 bis 600 aufweisen; in oder als Veredelung für jegliches Textil in Form einer linearen Formation wie Faden und Garn, in Form einer ebenen Formation wie Gewebe, gestricktem Gewebe, geknotetem Gewebe, Vliesstoff, Filz oder in Form von einer räumliche Formation wie einem Schlauch und Outwear für Frauen, Männer und Kinder.
Applications Claiming Priority (4)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP14002305 | 2014-07-04 | ||
| EP14002305 | 2014-07-04 | ||
| PCT/EP2015/001372 WO2016000830A1 (en) | 2014-07-04 | 2015-07-03 | Fluorine-free water-repellent composition |
| EP15736193.2A EP3164427B1 (de) | 2014-07-04 | 2015-07-03 | Fluorfreie wasserabstossende zusammensetzung |
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| Publication Number | Publication Date |
|---|---|
| DE15736193T1 true DE15736193T1 (de) | 2017-08-17 |
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| Application Number | Title | Priority Date | Filing Date |
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| DE15734300.5T Pending DE15734300T1 (de) | 2014-07-04 | 2015-07-03 | Zusammensetzung mit mischungen von polyacrylaten mit fluorhaltigen polyacrylaten |
| DE15736193.2T Pending DE15736193T1 (de) | 2014-07-04 | 2015-07-03 | Fluorfreie wasserabstossende zusammensetzung |
| DE15734579.4T Pending DE15734579T1 (de) | 2014-07-04 | 2015-07-03 | Fluorhaltige wasserabstossende zusammensetzung |
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| Application Number | Title | Priority Date | Filing Date |
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| DE15734300.5T Pending DE15734300T1 (de) | 2014-07-04 | 2015-07-03 | Zusammensetzung mit mischungen von polyacrylaten mit fluorhaltigen polyacrylaten |
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| Application Number | Title | Priority Date | Filing Date |
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| DE15734579.4T Pending DE15734579T1 (de) | 2014-07-04 | 2015-07-03 | Fluorhaltige wasserabstossende zusammensetzung |
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| Country | Link |
|---|---|
| US (3) | US11072885B2 (de) |
| EP (3) | EP3164427B1 (de) |
| JP (3) | JP6693892B2 (de) |
| KR (3) | KR102508998B1 (de) |
| CN (3) | CN106536622B (de) |
| DE (3) | DE15734300T1 (de) |
| ES (3) | ES2714281T3 (de) |
| MX (1) | MX2016016714A (de) |
| PL (1) | PL3164425T3 (de) |
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| JP6741442B2 (ja) * | 2016-02-29 | 2020-08-19 | 日華化学株式会社 | 撥水助剤、非フッ素系撥水剤組成物、及び撥水性繊維製品の製造方法 |
| KR102092158B1 (ko) * | 2016-03-11 | 2020-03-23 | 다이킨 고교 가부시키가이샤 | 수지 조성물 및 성형체 |
| DE102016212443A1 (de) * | 2016-07-07 | 2018-01-11 | Rudolf Gmbh | Zubereitungen als Hydrophobierungsmittel |
| PT3516105T (pt) * | 2016-09-23 | 2021-06-11 | Huntsman Textile Effects Germany Gmbh | Dispersões aquosas isentas flúor para o acabamento de tecidos têxteis |
| EP3498910A1 (de) | 2017-12-14 | 2019-06-19 | Henkel IP & Holding GmbH | Superhydrophobe beschichtungen zur behandlung von textilien |
| CN108124206A (zh) * | 2017-12-19 | 2018-06-05 | 东莞市爱高音响有限公司 | 一种抗水音箱面网及其制作方法 |
| EP3732221B1 (de) * | 2017-12-26 | 2022-02-23 | Akzo Nobel Coatings International B.V. | Fluorinat-polyacrylat-beschichtungszusammensetzung, herstellungsverfahren dafür und verwendung davon |
| CN109988264B (zh) * | 2017-12-29 | 2022-03-04 | 乳源东阳光氟有限公司 | 一种无氟防水剂及其制备方法和应用 |
| JPWO2019163570A1 (ja) * | 2018-02-20 | 2020-12-17 | ダイキン工業株式会社 | 表面処理剤 |
| DE102018117071A1 (de) | 2018-07-13 | 2020-01-16 | Mitsubishi Hitec Paper Europe Gmbh | Heißsiegelfähiges Barrierepapier |
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