DE1087585B - Process for the production of a gel-like product which contains lower alcohols and water - Google Patents
Process for the production of a gel-like product which contains lower alcohols and waterInfo
- Publication number
- DE1087585B DE1087585B DEK24983A DEK0024983A DE1087585B DE 1087585 B DE1087585 B DE 1087585B DE K24983 A DEK24983 A DE K24983A DE K0024983 A DEK0024983 A DE K0024983A DE 1087585 B DE1087585 B DE 1087585B
- Authority
- DE
- Germany
- Prior art keywords
- product
- gel
- water
- lower alcohols
- production
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 150000001298 alcohols Chemical class 0.000 title claims description 7
- 238000000034 method Methods 0.000 title claims description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 title claims description 3
- 238000004519 manufacturing process Methods 0.000 title claims 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 8
- 241000283153 Cetacea Species 0.000 claims description 4
- 150000002148 esters Chemical class 0.000 claims description 4
- 125000004432 carbon atom Chemical group C* 0.000 claims description 3
- 235000014113 dietary fatty acids Nutrition 0.000 claims description 2
- 229930195729 fatty acid Natural products 0.000 claims description 2
- 239000000194 fatty acid Substances 0.000 claims description 2
- 150000004665 fatty acids Chemical class 0.000 claims description 2
- 239000000203 mixture Substances 0.000 claims description 2
- 239000004094 surface-active agent Substances 0.000 claims description 2
- 235000019441 ethanol Nutrition 0.000 description 10
- 229920000151 polyglycol Polymers 0.000 description 3
- 239000010695 polyglycol Substances 0.000 description 3
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
- 230000001476 alcoholic effect Effects 0.000 description 2
- 125000000217 alkyl group Chemical group 0.000 description 2
- 125000003118 aryl group Chemical group 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- 150000002170 ethers Chemical class 0.000 description 2
- MVLVMROFTAUDAG-UHFFFAOYSA-N ethyl octadecanoate Chemical compound CCCCCCCCCCCCCCCCCC(=O)OCC MVLVMROFTAUDAG-UHFFFAOYSA-N 0.000 description 2
- JUCOQIYAKWHGSZ-UHFFFAOYSA-N icosyl acetate Chemical compound CCCCCCCCCCCCCCCCCCCCOC(C)=O JUCOQIYAKWHGSZ-UHFFFAOYSA-N 0.000 description 2
- GLDOVTGHNKAZLK-UHFFFAOYSA-N octadecan-1-ol Chemical compound CCCCCCCCCCCCCCCCCCO GLDOVTGHNKAZLK-UHFFFAOYSA-N 0.000 description 2
- PNGBYKXZVCIZRN-UHFFFAOYSA-M sodium;hexadecane-1-sulfonate Chemical compound [Na+].CCCCCCCCCCCCCCCCS([O-])(=O)=O PNGBYKXZVCIZRN-UHFFFAOYSA-M 0.000 description 2
- 239000013543 active substance Substances 0.000 description 1
- -1 arachyl alcohol Chemical compound 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000002537 cosmetic Substances 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 235000015110 jellies Nutrition 0.000 description 1
- 239000008274 jelly Substances 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- GOQYKNQRPGWPLP-UHFFFAOYSA-N n-heptadecyl alcohol Natural products CCCCCCCCCCCCCCCCCO GOQYKNQRPGWPLP-UHFFFAOYSA-N 0.000 description 1
- 239000003883 ointment base Substances 0.000 description 1
- 239000000825 pharmaceutical preparation Substances 0.000 description 1
- 229940127557 pharmaceutical product Drugs 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- BDHFUVZGWQCTTF-UHFFFAOYSA-M sulfonate Chemical compound [O-]S(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-M 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/06—Solidifying liquids
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Preparation (AREA)
Description
Verfahren zur Herstellung eines gelartigen Produkts, welches niedere Alkohole und Wasser enthält Es ist bekannt, daß man niedere Alkohole, z. B. Process for the preparation of a gel-like product, which lower Contains alcohols and water. It is known that one can use lower alcohols, e.g. B.
Äthyl alkohol verschiedener Konzentration zu gallertartigen Massen verfestigen kann, wenn man in ihnen einen bestimmten Prozentsatz höherer Alkohole von der Art des Stearylalkohols zusammen mit einem geeigneten Prozentsatz eines oberflächenaktiven Stoffes (z. B. Sulfonat, Poly- und Alkyl- wie Arylpolyglykoläther u. a.) auflöst und erkalten läßt, wobei ein Zustand von höheren Estern sich oft vorteilhaft auf die Konsistenz des entstehenden Produktes auswirkt.Ethyl alcohol of various concentrations to form gelatinous masses Can solidify if you have a certain percentage of higher alcohols in them of the type of stearyl alcohol along with an appropriate percentage of one surfactant (e.g. sulfonate, poly and alkyl such as aryl polyglycol ethers inter alia) dissolves and lets it cool, whereby a state of higher esters is often has a beneficial effect on the consistency of the resulting product.
Es wurde nun gefunden, daß die höheren Alkohole in solchen alkoholischen Gallertansätzen entbehrlich werden, wenn man an ihre Stelle eine größere Menge eines höheren Esters, bei welchem entweder der Alkohol oder die Fettsäure 16 Kohlenstoffatome oder mehr besitzt von der Art des Arachylacetates, Athylstearats, oder natürlich vorkommende Produkte, welche diese enthalten, wie Walrat oder deren Gemische, zusetzt. It has now been found that the higher alcohols in such alcoholic Gelatinous deposits can be dispensed with if a larger amount of one is used in their place higher ester in which either the alcohol or the fatty acid has 16 carbon atoms or more of the type of arachyl acetate, ethyl stearate, or natural occurring products that contain them, such as whale rat or mixtures thereof, added.
Dabei werden außerdem noch oberflächenaktive Substanzen, wie Natriumcetylsulfonat oder Alkyl-bzw. Arylpolyglykoläther in geringer Menge, d. h. etwa 1 O/o, zugesetzt. Surface-active substances such as sodium cetyl sulfonate are also used or alkyl or. Aryl polyglycol ethers in a small amount, d. H. about 10% added.
Beispiel I 0,8 g Arachylacetat, 0,2 g Walrat und 0,1 g Natriumcetylsulfonat werden in 8,2 ccm 700/oigem Äthylalkohol unter Erwärmen gelöst. Beim Abkühlen mit oder ohne Rühren bildet die Lösung ein gallertartiges Produkt. Example I 0.8 g arachyl acetate, 0.2 g whale rat and 0.1 g sodium cetyl sulfonate are dissolved in 8.2 cc of 700 / o strength ethyl alcohol with heating. When cooling down with or without stirring, the solution forms a gelatinous product.
Beispiel II 0,8 g Arachylalkohol, 0,2 g Walrat und 0,1 g Polyglykoläther werden mit 700/oigem Äthylalkohol, wie im Beispiel 1 beschrieben, behandelt. Beim Abkühlen erstarrt die alkoholische Lösung zu einer Gallerte. Example II 0.8 g of arachyl alcohol, 0.2 g of whale rat and 0.1 g of polyglycol ether are treated with 700% ethyl alcohol as described in Example 1. At the Cooling down, the alcoholic solution solidifies into a jelly.
In entsprechender Abwandlung ist das Verfahren auch auf andere niedere Alkohole anwendbar. In a corresponding modification, the procedure is also applicable to other lower ones Alcohols applicable.
Die so erhaltenen Produkte können als Salbengrundlage für kosmetische oder pharmazeutische Produkte Verwendung finden. The products thus obtained can be used as an ointment base for cosmetic or pharmaceutical products are used.
Claims (2)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DEK24983A DE1087585B (en) | 1955-02-22 | 1955-02-22 | Process for the production of a gel-like product which contains lower alcohols and water |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DEK24983A DE1087585B (en) | 1955-02-22 | 1955-02-22 | Process for the production of a gel-like product which contains lower alcohols and water |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE1087585B true DE1087585B (en) | 1960-08-25 |
Family
ID=7217176
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DEK24983A Pending DE1087585B (en) | 1955-02-22 | 1955-02-22 | Process for the production of a gel-like product which contains lower alcohols and water |
Country Status (1)
| Country | Link |
|---|---|
| DE (1) | DE1087585B (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1280218B (en) * | 1960-11-09 | 1968-10-17 | Dow Chemical Co | Thickening of non-polar organic solvents |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE907769C (en) * | 1950-01-06 | 1954-03-29 | Dr Walter Kinttof | Process for the preparation of a gel-like product from lower alcohols |
-
1955
- 1955-02-22 DE DEK24983A patent/DE1087585B/en active Pending
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE907769C (en) * | 1950-01-06 | 1954-03-29 | Dr Walter Kinttof | Process for the preparation of a gel-like product from lower alcohols |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1280218B (en) * | 1960-11-09 | 1968-10-17 | Dow Chemical Co | Thickening of non-polar organic solvents |
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