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DE1063530B - Fluid bed dryer - Google Patents

Fluid bed dryer

Info

Publication number
DE1063530B
DE1063530B DEF17366A DEF0017366A DE1063530B DE 1063530 B DE1063530 B DE 1063530B DE F17366 A DEF17366 A DE F17366A DE F0017366 A DEF0017366 A DE F0017366A DE 1063530 B DE1063530 B DE 1063530B
Authority
DE
Germany
Prior art keywords
shaft
stirrer
bed dryer
fluid bed
sieve
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
DEF17366A
Other languages
German (de)
Inventor
Dr Heinrich Freudenberger
Dipl-Ing Dr Lutz Ziegler
Josef Westenberger
Dr-Ing Paul Dietrich
Dipl-Ing Gerhard Schloemann
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Hoechst AG
Original Assignee
Hoechst AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Hoechst AG filed Critical Hoechst AG
Priority to DEF17366A priority Critical patent/DE1063530B/en
Publication of DE1063530B publication Critical patent/DE1063530B/en
Pending legal-status Critical Current

Links

Classifications

    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F26DRYING
    • F26BDRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
    • F26B3/00Drying solid materials or objects by processes involving the application of heat
    • F26B3/02Drying solid materials or objects by processes involving the application of heat by convection, i.e. heat being conveyed from a heat source to the materials or objects to be dried by a gas or vapour, e.g. air
    • F26B3/06Drying solid materials or objects by processes involving the application of heat by convection, i.e. heat being conveyed from a heat source to the materials or objects to be dried by a gas or vapour, e.g. air the gas or vapour flowing through the materials or objects to be dried
    • F26B3/08Drying solid materials or objects by processes involving the application of heat by convection, i.e. heat being conveyed from a heat source to the materials or objects to be dried by a gas or vapour, e.g. air the gas or vapour flowing through the materials or objects to be dried so as to loosen them, e.g. to form a fluidised bed
    • F26B3/092Drying solid materials or objects by processes involving the application of heat by convection, i.e. heat being conveyed from a heat source to the materials or objects to be dried by a gas or vapour, e.g. air the gas or vapour flowing through the materials or objects to be dried so as to loosen them, e.g. to form a fluidised bed agitating the fluidised bed, e.g. by vibrating or pulsating
    • F26B3/0923Drying solid materials or objects by processes involving the application of heat by convection, i.e. heat being conveyed from a heat source to the materials or objects to be dried by a gas or vapour, e.g. air the gas or vapour flowing through the materials or objects to be dried so as to loosen them, e.g. to form a fluidised bed agitating the fluidised bed, e.g. by vibrating or pulsating by mechanical means, e.g. vibrated plate, stirrer

Landscapes

  • Engineering & Computer Science (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Microbiology (AREA)
  • Mechanical Engineering (AREA)
  • General Engineering & Computer Science (AREA)
  • Drying Of Solid Materials (AREA)

Description

Wirbelbetttrockner Gegenstand der Erfindung ist ein Wirbelbetttrockner für in feuchtem Zustand klebende und nicht rieselfähige Pulver insbesondere thermoplastischer Kunststoffe, z. B. Perlpolymerisat. Dieses ist in diesem Zustand nicht rieselfähig, läßt sich wie Schnee leicht zusammenballen und klebt bereits bei schwacher Erwärmung zu Klumpen.Fluidized bed dryer The invention relates to a fluidized bed dryer for powders that stick and do not flow freely when wet, especially thermoplastic Plastics, e.g. B. pearl polymer. This is not free-flowing in this state, can be easily balled up like snow and sticks even if the temperature is low to lump.

Es ist bekannt, Kunststoffpulver in Trocknungsschränken auf Horden zu trocknen. Die meisten Kunststoffpulver kleben, backen oder fließen während des Trocknens in derartigen Schränken zu Platten zusammen, die nur langsam durchtrocknen und die am Ende des Trocknungsverfahrens wieder zerkleinert werden müssen. Die Trocknen in Schränken ist daher sehr unwirtschaftlich, und es ist darüber hinaus in den Fällen, in denen das getrocknete Produkt in Form von Kügelchen oder Perlen verlangt wird, auch dann nicht anwendbar, wenn die Perlen beim Trocknen nicht zu einer homogenen Platte zusammenfließen, sondern nur verkleben, weil die Veränderungen in Form und Qualität der Perlen als erheblicher Nachteil empfunden werden.It is known to place plastic powder in drying cabinets on racks to dry. Most plastic powders stick, bake, or flow during the Drying in such cabinets to form sheets that dry out slowly and which have to be shredded again at the end of the drying process. The drying in cupboards is therefore very uneconomical, and it is also in the cases in which the dried product is required in the form of beads or pearls, also not applicable if the pearls do not become homogeneous when drying Plate flow together, but only stick together because the changes in shape and The quality of the pearls can be perceived as a significant disadvantage.

Auch bei Anwendung anderer bekannter Trockner, z. B. der Band-, Trommel-, Walzen- oder Muldentröckner, treten die oben bezeichneten Mängel auf. Zudem kleben die Kunststoffteilchen an den Gehäusewänden, bewegten Teilen und sonstigen Einbauten zu schwer lösbaren Krusten fest, oder sie ballen sich zu Klumpen zusammen. Umständliche Reinigungsarbeiten, Produktverluste, Qualitätsminderungen und nachträgliches Zerkleinern sind unvermeidlich.Even when using other known dryers, e.g. B. the band, drum, Roller or trough dryer, the above-mentioned defects occur. In addition, glue the plastic particles on the housing walls, moving parts and other fixtures to hard-to-dissolve crusts or they clump together into lumps. Awkward Cleaning work, product loss, deterioration in quality and subsequent shredding are inevitable.

In jüngerer Zeit wird zur Trocknung pulverförmiger oder feinkörniger Stoffe vielfach das Wirbelbettverfahren angewendet. Die zur Durchführung dieses Verfahrens üblichen Apparate bestehen im wesentlichen aus einem zylindrischen oder kegelig verjüngten Oberteil, das über einen Siebboden als Warmluftverteiler mit einem kegelig verjüngten Unterteil verbunden ist. Unter dem Einfluß der durch den Siebboden zuströmenden Warmluft bildet das zu trocknende Gut im Oberteil ein Wirbelbett mit flüssigkeitsähnlichen Eigenschaften. Zur Trocknung von Kunststoffpulvern, z. B. Perlpolymerisaten, sind die bekannten Apparate dieser Art nicht geeignet. Es bilden sich in kurzer Zeit Verkrustungen an der Schachtwand, die Verteiler verstopfen sich; in den toten Winkeln, insbesondere an der Verbindungsstelle Schachtwand-Siebboden treten Zusammenballungen ein, und im Wirbelbett entstehen Luftdurchbrüche, die zu Ungleichmäßigkeiten in der Trocknung und zu teilweiser Überhitzung empfindlichen Gutes führen. Durch Einbau von Rührern konventioneller Art gelingt es nicht, die geschilderten Mängel zu beheben, sie werden vielmehr noch vermehrt, weil durch die Rührer die Zugänglichkeit, die Entleerung und Reinigung des Apparates stark behindert sind.More recently, powdery or fine-grained drying has been used Substances often used the fluidized bed process. The ones to carry out this Process usual apparatus consist essentially of a cylindrical or conically tapered upper part, which has a sieve base as a hot air distributor a conically tapered lower part is connected. Under the influence of the Warm air flowing into the sieve bottom forms the material to be dried in the upper part of a fluidized bed with liquid-like properties. For drying plastic powders, e.g. B. bead polymers, the known apparatus of this type are not suitable. It In a short time, incrustations form on the shaft wall and clog the distributors themselves; in the blind spots, especially at the connection point between the shaft wall and the sieve bottom agglomerations occur, and air breakthroughs occur in the fluidized bed, which lead to Irregularities in drying and partial overheating susceptible Lead good. By installing stirrers of the conventional type, it is not possible to achieve the To remedy the deficiencies described, they are rather increased because by the Stirrer severely impedes access, emptying and cleaning of the apparatus are.

Es wird nun ein Wirbelbetttrockner für die eingangs genannten Stoffe vorgeschlagen. Dieser Wirbelbetttrockner besteht aus einem nach unten verjüngten Schacht, durch dessen Siebboden das Behandlungsgas aufwärts strömt und der absatzweise mit Stoff beschickt wird. Erfindungsgemäß ist der Wirbelbetttrockner gekennzeichnet durch einen die gesamte vom Stoff bedeckte Schachtwand und den Siebboden in geringem Abstand von Schachtwand und Siebboden bestreichenden Rührer, dessen Rührwirkung zugleich auch den gesamten vom Gut gefüllten Schachtraum erfaßt.There is now a fluid bed dryer for the substances mentioned above suggested. This fluid bed dryer consists of a downwardly tapered one Shaft through the sieve bottom of which the treatment gas flows upwards and which is intermittent is loaded with fabric. According to the invention, the fluidized bed dryer is characterized through the entire shaft wall covered by the material and the sieve bottom in a small amount Distance from the shaft wall and the sieve bottom, the stirrer, its stirring effect at the same time the entire shaft space filled by the material is recorded.

Der neue Trockner kann einen Rührer besitzen, bestehend aus einem an einer zentralen lotrechten Welle befestigten, der Trocknungsraumform angepaßten äußeren Rahmen, an dem den Trocknungsraum durchsetzende, vorzugsweise horizontal und radial gerichtete Stäbe mit Abstand übereinander angeordnet sind.The new dryer can have a stirrer consisting of one attached to a central vertical shaft, adapted to the shape of the drying room outer frame on which the drying room penetrates, preferably horizontal and radially directed rods are arranged at a distance one above the other.

Die Zeichnung zeigt den neuen Wirbelbetttrockner in einer Ausführungsform. Der kegelige Schacht ist mit 1, der Siebboden mit 2 und der Rührer mit 3 bezeichnet. Die Warmluft strömt über einen Diffusor 4 zu, an dessen Unterteil ein Entleerungsstutzen 5 angeordnet ist. Der Schacht 1 läuft in einen Beruhigungsraum 6 aus, zu dem ein Füllstutzen 7 führt. 8 stellt ein Schlauchfilter dar, das in eine ringförmige Kammer 9 in bekannter Weise eingesetzt ist. Mit 10 ist ein Abluft- oder Abgasstutzen bezeichnet, mit 11 der Antrieb des Rührers.The drawing shows the new fluidized bed dryer in one embodiment. The conical shaft is designated with 1, the sieve bottom with 2 and the stirrer with 3. The warm air flows in via a diffuser 4, on the lower part of which an emptying nozzle 5 is arranged. The shaft 1 runs out into a calming space 6 to which a filler neck 7 leads. Figure 8 shows a bag filter inserted into an annular chamber 9 in a known manner. With 10 an exhaust air or exhaust pipe is designated, with 11 the drive of the stirrer.

Zum Betrieb des Trockners wird das Feuchtgut durch den Stutzen 7 in den Schacht 1 eingetragen. Die über den Siebboden 2 zuströmende Warmluft bläht den Eintrag zu einem Wirbelbett auf, das mittels des Rührers 3 fortlaufend durchmischt wird. Der von der Abluft aus dem Beruhigungsraum 6 mitgerissene Feinstanteil des Gutes wird von dem Filter zurückgehalten und durch Rütteln in den Schacht 1 zurückgefördert. Nach beendeter Trocknung werden Rührer und Luftzufuhr abgestellt, das Wirbelbett stürzt zusammen, das trockene Gut rieselt durch die Verteilerplatte und kann aus dem Stutzen 5 in Behälter üblicher Art abgefüllt werden. Durch Wiederingangsetzen des Rührers läßt sich der Entleerungsvorgang abkürzen. Zur Erleichterung der Entleerung kann der Siebboden in bekannter Weise ein Schieber sein.To operate the dryer, the moist material is fed through the nozzle 7 in entered the shaft 1. The warm air flowing in through the sieve bottom 2 inflates the Entry to a fluidized bed, which is continuously mixed by means of the stirrer 3 will. The fine fraction of the entrained by the exhaust air from the calming chamber 6 Good is retained by the filter and returned to the shaft 1 by shaking. After drying is complete, the stirrer and air supply are turned off, the fluidized bed collapses, the dry material trickles through the distributor plate and can out the nozzle 5 are filled into containers of the usual type. By restarting The emptying process can be shortened with the stirrer. To facilitate emptying the sieve bottom can be a slide in a known manner.

Claims (2)

PATENTANSPRACHE: 1. Wirbelbetttrockner für im feuchten Zustand klebende und nicht rieselfähige Pulver, insbesondere thermoplastische Kunststoffe, z. B. Perlpolymerisate; bestehend aus einem nach unten verjüngten Schacht, durch dessen Siebboden das Behandlungsgas aufwärts strömt und der absatzweise mit Stoff beschickt wird, gekennzeichnet durch einen die gesamte vom Stoff bedeckte Schachtwand und den Siebboden in geringem Abstand von Schachtwand und Siebboden bestreichenden Rührer, dessen Rührwirkung zugleich auch den gesamten vom Gut gefüllten Schachtraum erfaßt. PATENT APPEAL: 1. Fluid bed dryer for sticky and non-free-flowing powders when wet, in particular thermoplastics, e.g. B. pearl polymers; Consists of a downwardly tapered shaft, through whose sieve bottom the treatment gas flows upwards and which is charged with substance in batches, characterized by a stirrer which sweeps the entire shaft wall covered by the substance and the sieve base at a short distance from the shaft wall and sieve base, whose stirring effect also applies to the covers the entire shaft space filled by the material. 2. Trockner nach Anspruch 1, gekennzeichnet durch einen Rührer, bestehend aus einem an einer zentralen lotrechten Welle befestigten, der Trocknungsraumform angepaßten äußeren Rahmen (3), an dem den Trocknungsraum (1) durchsetzende, vorzugsweise horizontal und radial gerichtete Stäbe mit Abstand übereinander angeordnet sind. In Betracht gezogene Druckschriften: Deutsche Patentschriften Nr. 444 847, 473 367, 555 219, 875 475, 887 178; britische Patentschrift Nr. 729 186; USA.-Patentschriften Nr. 1255 843, 1984 380, 2 212 120, 2 485 024; Chemie Ingenieur Technik, 1951, S, 445.2. Dryer according to claim 1, characterized by a stirrer, consisting of a fixed to a central vertical shaft, the drying room shape adapted outer frame (3) on which the drying room (1) penetrating, preferably horizontally and radially directed rods arranged at a distance one above the other are. Considered publications: German Patent Nos. 444 847, 473 367, 555 219, 875 475, 887 178; British Patent No. 729 186; USA. Patent No. 1255 843, 1984380, 2212120, 2485024. Chemical engineer technology, 1951, p. 445.
DEF17366A 1955-04-20 1955-04-20 Fluid bed dryer Pending DE1063530B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
DEF17366A DE1063530B (en) 1955-04-20 1955-04-20 Fluid bed dryer

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DEF17366A DE1063530B (en) 1955-04-20 1955-04-20 Fluid bed dryer

Publications (1)

Publication Number Publication Date
DE1063530B true DE1063530B (en) 1959-08-13

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ID=7088560

Family Applications (1)

Application Number Title Priority Date Filing Date
DEF17366A Pending DE1063530B (en) 1955-04-20 1955-04-20 Fluid bed dryer

Country Status (1)

Country Link
DE (1) DE1063530B (en)

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE1201773B (en) * 1960-11-16 1965-09-23 Muehlen Und Naehrmittelwerke H Cylindrical dryer for solid-liquid mixtures
DE1227840B (en) * 1960-08-25 1966-10-27 Haas Friedrich Maschf Continuously working fluid bed dryer
DE1232340B (en) * 1963-03-16 1967-01-12 Bayer Ag Device for drying rubber crumbs
DE1795396A1 (en) * 1968-09-26 1972-01-05 Basf Ag Process for removing volatile components from finely divided olefin polymers
DE2632054A1 (en) * 1976-07-16 1978-01-26 Hoechst Ag PROCESS FOR DRYING CHLORINATED POLYMERS
DE2745179A1 (en) * 1977-10-07 1979-04-12 Loedige Maschbau Gmbh Geb Mixing drying and granulating tower - has inert gas and moisture injected into bottom chamber with paddles and cutters

Citations (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US1255843A (en) * 1917-07-17 1918-02-05 John B Adt Drying apparatus.
DE444847C (en) * 1924-03-07 1927-05-28 I G Farbenindustrie Akt Ges Process for drying and glowing in pots
DE473367C (en) * 1929-03-14 Werke Kiel Akt Ges Deutsche Internal combustion engine in which the forces acting in the cylinder are transmitted to the crankshaft bearing by tie rods
DE555219C (en) * 1930-10-07 1932-07-19 Jacques Philippe Robert Louste Drying device for salt
US1984380A (en) * 1929-12-17 1934-12-18 William W Odell Process of producing chemical reactions
US2212120A (en) * 1939-11-24 1940-08-20 Robert D Kneale Method of roasting coffee
US2485024A (en) * 1945-03-21 1949-10-18 Amalgamated Wireless Australas Electromagnetically operated vacuum sealed relay
DE875475C (en) * 1950-09-27 1953-05-04 Borsig Ag Device for loosening grainy masses, preferably for steaming out moist seed extraction residues
DE887178C (en) * 1939-02-08 1953-08-20 Metallgesellschaft Ag Device for post-treatment, cooling or clearing of dry goods in spray dryers
GB729186A (en) * 1952-05-07 1955-05-04 Celleco Ab Improvements in or relating to drying of materials in the form of particles

Patent Citations (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE473367C (en) * 1929-03-14 Werke Kiel Akt Ges Deutsche Internal combustion engine in which the forces acting in the cylinder are transmitted to the crankshaft bearing by tie rods
US1255843A (en) * 1917-07-17 1918-02-05 John B Adt Drying apparatus.
DE444847C (en) * 1924-03-07 1927-05-28 I G Farbenindustrie Akt Ges Process for drying and glowing in pots
US1984380A (en) * 1929-12-17 1934-12-18 William W Odell Process of producing chemical reactions
DE555219C (en) * 1930-10-07 1932-07-19 Jacques Philippe Robert Louste Drying device for salt
DE887178C (en) * 1939-02-08 1953-08-20 Metallgesellschaft Ag Device for post-treatment, cooling or clearing of dry goods in spray dryers
US2212120A (en) * 1939-11-24 1940-08-20 Robert D Kneale Method of roasting coffee
US2485024A (en) * 1945-03-21 1949-10-18 Amalgamated Wireless Australas Electromagnetically operated vacuum sealed relay
DE875475C (en) * 1950-09-27 1953-05-04 Borsig Ag Device for loosening grainy masses, preferably for steaming out moist seed extraction residues
GB729186A (en) * 1952-05-07 1955-05-04 Celleco Ab Improvements in or relating to drying of materials in the form of particles

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE1227840B (en) * 1960-08-25 1966-10-27 Haas Friedrich Maschf Continuously working fluid bed dryer
DE1201773B (en) * 1960-11-16 1965-09-23 Muehlen Und Naehrmittelwerke H Cylindrical dryer for solid-liquid mixtures
DE1232340B (en) * 1963-03-16 1967-01-12 Bayer Ag Device for drying rubber crumbs
DE1795396A1 (en) * 1968-09-26 1972-01-05 Basf Ag Process for removing volatile components from finely divided olefin polymers
DE2632054A1 (en) * 1976-07-16 1978-01-26 Hoechst Ag PROCESS FOR DRYING CHLORINATED POLYMERS
DE2745179A1 (en) * 1977-10-07 1979-04-12 Loedige Maschbau Gmbh Geb Mixing drying and granulating tower - has inert gas and moisture injected into bottom chamber with paddles and cutters

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