CN201027197Y - Microwave drum dry distillation device - Google Patents
Microwave drum dry distillation device Download PDFInfo
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- CN201027197Y CN201027197Y CN 200720093337 CN200720093337U CN201027197Y CN 201027197 Y CN201027197 Y CN 201027197Y CN 200720093337 CN200720093337 CN 200720093337 CN 200720093337 U CN200720093337 U CN 200720093337U CN 201027197 Y CN201027197 Y CN 201027197Y
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- 238000000197 pyrolysis Methods 0.000 title claims abstract description 38
- 239000002893 slag Substances 0.000 claims abstract description 14
- 239000000463 material Substances 0.000 claims abstract description 10
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 5
- 230000005540 biological transmission Effects 0.000 claims description 3
- 238000010079 rubber tapping Methods 0.000 claims description 3
- 239000004058 oil shale Substances 0.000 abstract description 27
- 238000010438 heat treatment Methods 0.000 abstract description 11
- 239000002028 Biomass Substances 0.000 abstract description 4
- 239000003245 coal Substances 0.000 abstract description 4
- 239000010813 municipal solid waste Substances 0.000 abstract description 4
- 239000003575 carbonaceous material Substances 0.000 abstract description 2
- 230000003749 cleanliness Effects 0.000 abstract description 2
- 230000007613 environmental effect Effects 0.000 abstract description 2
- 238000000034 method Methods 0.000 description 18
- 239000002245 particle Substances 0.000 description 18
- 239000007789 gas Substances 0.000 description 10
- 239000007787 solid Substances 0.000 description 7
- 238000003763 carbonization Methods 0.000 description 6
- 238000006073 displacement reaction Methods 0.000 description 4
- 239000011343 solid material Substances 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- 229910000831 Steel Inorganic materials 0.000 description 2
- 239000000919 ceramic Substances 0.000 description 2
- 239000000571 coke Substances 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 239000011521 glass Substances 0.000 description 2
- 239000010959 steel Substances 0.000 description 2
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 1
- 238000009825 accumulation Methods 0.000 description 1
- 238000009833 condensation Methods 0.000 description 1
- 230000005494 condensation Effects 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000005265 energy consumption Methods 0.000 description 1
- 239000003546 flue gas Substances 0.000 description 1
- 239000000446 fuel Substances 0.000 description 1
- 239000011261 inert gas Substances 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 230000035515 penetration Effects 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 239000004576 sand Substances 0.000 description 1
- 239000003079 shale oil Substances 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 239000013589 supplement Substances 0.000 description 1
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- Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)
Abstract
本实用新型涉及含碳材料的热解干馏领域,是一种微波滚筒干馏装置,其特点是它包括:在机座上置的微波炉体、支撑托滚,在支撑托滚上设有内螺旋滚筒,内螺旋滚筒具有进料口、出渣筒和与出渣筒连通的出气管,内螺旋滚筒的中段置于微波炉体内,内螺旋滚筒的进料口与螺旋输送机连接。由于采用螺旋输送机和内螺旋滚筒输送料及微波加热结构,具有结构简单,操作方便,干馏速度快,能量利用率高,清洁、环保等优点。可广泛用于油页岩、煤、生物质及垃圾的干馏热解。
The utility model relates to the field of pyrolysis and dry distillation of carbonaceous materials, which is a microwave drum dry distillation device, which is characterized in that it includes: a microwave oven body placed on a machine base, a supporting roller, and an inner spiral roller is arranged on the supporting roller , the inner spiral drum has a feed inlet, a slag discharge cylinder and an air outlet pipe connected with the slag discharge cylinder, the middle section of the inner spiral drum is placed in the microwave oven body, and the feed inlet of the inner spiral drum is connected with a screw conveyor. Due to the use of screw conveyors and inner screw drums to convey materials and microwave heating structure, it has the advantages of simple structure, convenient operation, fast dry distillation speed, high energy utilization rate, cleanliness and environmental protection. It can be widely used in dry distillation and pyrolysis of oil shale, coal, biomass and garbage.
Description
技术领域 technical field
本实用新型涉及含碳材料的热解干馏领域,是一种微波滚筒干馏装置,适用于油页岩、煤、生物质、垃圾等固体物料的干馏。The utility model relates to the field of pyrolysis and dry distillation of carbonaceous materials, which is a microwave drum dry distillation device, which is suitable for dry distillation of solid materials such as oil shale, coal, biomass and garbage.
背景技术 Background technique
现有对油页岩、煤、生物质、垃圾等固体物料的干馏主要有两种方法,即:气体热载体法和固体热载体法。上述两种方法均属于热传导和热对流加热方式,这种对物料的常规加热方式通常称为外加热。以油页岩干馏为例:采用气体热载体法是靠加热干馏瓦斯气作为干馏热源,当干馏瓦斯气的量不充足时须补充蒸汽或氮气等惰性气体,有时为把油页岩加热到450~600℃,除了采用上述方法外,还同时需要燃烧油页岩或其它燃料产生的高温烟气补充不足的热量。为提高干馏炉内油页岩堆积的孔隙率、加热的均匀性,气体热载体法一般处理15~75mm的大颗粒油页岩,而15mm以下的小颗粒的油页岩不能送入干馏炉内被利用,而白白的浪费掉,因此该方法能源消耗高、工艺复杂、油页岩利用率低;采用固体热载体法是将干馏后的半焦通过燃烧或将沙子等固体颗粒加热到一定温度后成为固体热载体与油页岩混合,在此接触过程中,固体热载体通过导热将热量传给油页岩将其加热到450~600℃实现油页岩干馏。虽然该方法主要处理25mm以下的小颗粒的油页岩,但其主要缺点是需要额外的固体颗粒加热炉并需将固体颗粒以气力输送的形式送入干馏炉内,因此装置复杂庞大,磨损严重、连续运行时间短、能量利用率低。Currently, there are mainly two methods for dry distillation of solid materials such as oil shale, coal, biomass, and garbage, namely: the gas heat carrier method and the solid heat carrier method. The above two methods belong to heat conduction and heat convection heating methods, and this conventional heating method for materials is usually called external heating. Take oil shale dry distillation as an example: the gas heat carrier method relies on heating dry distillation gas as the heat source for dry distillation. When the amount of dry distillation gas is insufficient, inert gases such as steam or nitrogen must be added. Sometimes the oil shale is heated to 450 ~600°C, in addition to the above methods, it is also necessary to supplement the insufficient heat with high-temperature flue gas produced by burning oil shale or other fuels. In order to improve the porosity of oil shale accumulation in the retort furnace and the uniformity of heating, the gas heat carrier method generally treats large-grained oil shale of 15-75mm, while small-grained oil shale below 15mm cannot be sent into the retort furnace Therefore, the energy consumption of this method is high, the process is complicated, and the utilization rate of oil shale is low; the solid heat carrier method is to burn the semi-coke after dry distillation or heat solid particles such as sand to a certain temperature Then it becomes a solid heat carrier and mixes with oil shale. During this contact process, the solid heat carrier transfers heat to oil shale through heat conduction and heats it to 450-600°C to realize oil shale carbonization. Although this method mainly treats oil shale with small particles below 25mm, its main disadvantage is that an additional solid particle heating furnace is required and the solid particles need to be sent into the carbonization furnace in the form of pneumatic conveying, so the device is complex and large, and the wear is serious , Continuous running time is short, energy utilization rate is low.
发明内容 Contents of the invention
本实用新型所要解决的技术问题是:克服现有技术的不足,提供一种能够对物料进行内加热,结构简单,操作方便,干馏速度快,能量利用率高,清洁、环保,可连续、稳定的运行的微波滚筒干馏装置。The technical problem to be solved by the utility model is: to overcome the deficiencies of the prior art, to provide a kind of internal heating for materials, simple in structure, convenient in operation, fast in retort speed, high in energy utilization rate, clean, environmentally friendly, continuous and stable The operation of the microwave drum retort apparatus.
解决其技术问题采用的技术方案是:解决其技术问题采用的技术方案是:一种微波滚筒干馏装置,其特征在于,它包括机座2,在机座2上置有微波炉体1、支撑托滚18,在支撑托滚18上设有内螺旋滚筒9,内螺旋滚筒9具有进料口20、出渣筒5和与出渣筒5连通的出气管7,在内螺旋滚筒9设有动力轮13,内螺旋滚筒9的中段置于微波炉体1内,内螺旋滚筒9的进料口20与螺旋输送机15连接。The technical solution adopted to solve the technical problem is: the technical solution adopted to solve the technical problem is: a microwave drum retort device, characterized in that it includes a machine base 2, on which a microwave oven body 1, a support bracket Roller 18, an inner
所述微波炉体1与微波发生器11连接组成微波炉。The microwave oven body 1 is connected with a microwave generator 11 to form a microwave oven.
所述内螺旋滚筒9的结构是,具有内螺旋推料叶片12,在置于微波炉体1内的内螺旋滚筒9的中段还设有扬料倾斜叶片10。The structure of the inner
所述内螺旋滚筒9的结构是,具有内螺旋推料叶片12。The structure of the inner
所述内螺旋滚筒9的结构是,具有导料槽25。The structure of the inner
所述动力轮13为链轮,且通过传动链与电机17a轴上的链轮21连接。The power wheel 13 is a sprocket, and is connected with the sprocket 21 on the shaft of the motor 17a through a transmission chain.
所述螺旋输送机15的结构是,具有简体23,在简体23上设有喂料斗14,在筒体23内置有相配合的螺旋杆24,螺旋杆24与电机22b的轴连接。The structure of the screw conveyor 15 is to have a simplified body 23, on which a feeding hopper 14 is arranged, and a matching screw rod 24 is built in the cylindrical body 23, and the screw rod 24 is connected with the shaft of the motor 22b.
在所述内螺旋滚筒9穿装于微波炉体1的两端口6处均置有微波抑制器19。
在所述内螺旋滚筒9上固连有定位圈8,定位圈8置于在机座2上固定的定位滚轮3之间。A positioning ring 8 is fixedly connected to the internal
所述出渣筒5置于水封槽4内。The slag discharge cylinder 5 is placed in the water seal tank 4 .
本实用新型与现有技术相比,由于本实用新型采用了内螺旋滚筒送料和微波加热结构,并将微波滚筒干馏装置作为干馏热解油页岩的应用,在加热过程中,油页岩颗粒沿内螺旋滚筒不断位移,当油页岩颗粒沿内螺旋滚筒而进入微波炉体内置段的内螺旋滚筒时,在滚筒内螺旋位移的同时翻滚,其表面不断得到更新,滚筒内油页岩颗粒均有机会在其表面受到微波的加热,增强了油页岩颗粒的受热均匀性,这样既解决了微波穿透小的局限性,又大大提高了微波的利用率;同时,油页岩颗粒在翻滚过程中,温度快速升高至450~600℃进行干馏热解,干馏出的气体很快得到扩散,加快了微波干馏的速率,保证了干馏质量;由于采用螺旋推动,微波加热,对油页岩颗粒的粒度要求大大降低,0~30mm颗粒的固体物料都能被均匀加热干馏;干馏油页岩颗粒的处理量可以通过调节螺旋输送机的转速和内螺旋滚筒的旋转速度以及微波功率的大小等方法来进行;整个干馏过程是在连续、稳定状态下进行的,对于干馏油页岩颗粒预处理要求低,自动化程度高,劳动力消耗少。具有结构简单,操作方便,干馏速度快,能量利用率高,清洁、环保等优点。本实用新型还可用于煤、生物质及垃圾的干馏热解。Compared with the prior art, the utility model adopts the internal spiral drum feeding and microwave heating structure, and uses the microwave drum dry distillation device as the application of dry distillation pyrolysis oil shale. During the heating process, the oil shale particles Continuous displacement along the inner spiral drum, when the oil shale particles enter the inner spiral drum of the built-in section of the microwave oven body along the inner spiral drum, they roll while the inner spiral displacement of the drum, and its surface is constantly renewed, and the oil shale particles in the drum are uniform There is an opportunity to be heated by microwaves on its surface, which enhances the heating uniformity of oil shale particles, which not only solves the limitation of microwave penetration, but also greatly improves the utilization of microwaves; at the same time, oil shale particles are tumbling During the process, the temperature rises rapidly to 450-600°C for carbonization and pyrolysis, and the gas from carbonization is quickly diffused, which speeds up the rate of microwave carbonization and ensures the quality of carbonization; The particle size requirements are greatly reduced, and solid materials with 0-30mm particles can be uniformly heated and retorted; the processing capacity of retorted oil shale particles can be adjusted by adjusting the speed of the screw conveyor, the rotation speed of the inner screw drum and the size of the microwave power, etc. method; the whole retort process is carried out in a continuous and steady state, with low requirements for pretreatment of retort oil shale particles, high degree of automation, and low labor consumption. It has the advantages of simple structure, convenient operation, fast dry distillation speed, high energy utilization rate, cleanliness and environmental protection. The utility model can also be used for dry distillation and pyrolysis of coal, biomass and garbage.
附图说明 Description of drawings
图1为微波滚筒干馏装置结构示意图。Figure 1 is a schematic diagram of the structure of a microwave drum dry distillation device.
图2为图1中内螺旋滚筒结构立体剖视放大示意图。Fig. 2 is an enlarged schematic diagram of a three-dimensional cross-sectional view of the inner spiral drum structure in Fig. 1 .
图3为只具有内螺旋推料叶片12的内螺旋滚筒结构立体剖视放大示意图。FIG. 3 is an enlarged schematic perspective view of an inner helical drum structure with only inner
图4为具有导料槽25的内螺旋滚筒结构立体剖视放大示意图。FIG. 4 is an enlarged perspective view of a three-dimensional cross-sectional view of an inner spiral drum structure with a
图5为只具有直筒内螺旋滚筒结构剖视放大示意图。Fig. 5 is an enlarged schematic cross-sectional view of a structure with only a straight inner spiral drum.
图中:1微波炉体、2机座、3定位滚轮、4水封槽、5出渣筒、6端口、7出气管、8定位圈、9内螺旋滚筒、10扬料倾斜叶片、11微波发生器、12螺旋推料叶片、13动力轮、14喂料斗、15螺旋输送机、16机械密封、17a电机、18托滚、19微波抑制器、20进料口、21链轮、22b电机、23简体、24螺旋杆、25导料槽。In the figure: 1 microwave oven body, 2 machine base, 3 positioning roller, 4 water seal groove, 5 slag discharge cylinder, 6 port, 7 air outlet pipe, 8 positioning ring, 9 inner spiral drum, 10 inclined blade for lifting material, 11 microwave generator Device, 12 screw pusher blade, 13 power wheel, 14 feeding hopper, 15 screw conveyor, 16 mechanical seal, 17a motor, 18 support roller, 19 microwave suppressor, 20 feed port, 21 sprocket, 22b motor, 23 Simplified, 24 screw rods, 25 guide grooves.
具体实施方式 Detailed ways
参照图1,微波滚筒干馏装置具有机座2,在机座2上置有微波炉体1、支撑托滚18。在支撑托滚18上设有内螺旋滚筒9,内螺旋滚筒9具有进料口20、出渣筒5和与出渣筒5连通的出气管7,在内螺旋滚筒9设有动力轮13。内螺旋滚筒9的进料口20通过机械密封16与螺旋输送机15连接。内螺旋滚筒9通过机械密封16与出渣筒5和与出渣筒5连通的出气管7连接。内螺旋滚筒9由透过微波的耐高温、高强度材料制成,其材料可以是耐热陶瓷和耐热玻璃钢,耐热陶瓷和耐热玻璃钢还具有耐磨性,可大大提高装置的运行周期和使用寿命。内螺旋滚筒9的中段置于微波炉体1内,内螺旋滚筒9的进料口20与螺旋输送机15连接。所述微波炉体1与微波发生器11连接组成微波炉。微波炉体1由不锈钢板制成,微波发生器11为多个微波发生器,其功率大小可根据进料量,进料种类设定。Referring to FIG. 1 , the microwave drum dry distillation device has a machine base 2 on which a microwave oven body 1 and supporting rollers 18 are placed. An inner
参照图1和2,所述内螺旋滚筒9的结构是,具有内螺旋推料叶片12,在置于微波炉体1内的内螺旋滚筒9的中段还设有扬料倾斜叶片10。此种内螺旋滚筒9为最佳结构。Referring to FIGS. 1 and 2 , the structure of the inner
参照图3,所述内螺旋滚筒9或只具有内螺旋推料叶片12。Referring to FIG. 3 , the inner
参照图4,所述内螺旋滚筒9或具有若干个导料槽25。Referring to FIG. 4 , the inner
参照图5,所述内螺旋滚筒9或只具有直筒。Referring to Fig. 5, the inner
图4和图5所示的只具有内螺旋推料叶片12的内螺旋滚筒9和直筒内螺旋滚筒9设置时,进料端相对出料端的倾斜角度为5~15°。When the inner
参照图1,所述动力轮13为链轮,且通过传动链与电机17a轴上的链轮21连接。电机17a为调速电机。所述螺旋输送机15的结构是,具有筒体23,在筒体23上设有喂料斗14,在筒体23内置有相配合的螺旋杆24,螺旋杆24与电机22b的轴连接。在所述内螺旋滚筒9穿装于微波炉体1的两端口6处均置有防止微波泄漏用的微波抑制器19。在所述内螺旋滚筒9上固连有定位圈8,定位圈8置于在机座2上固定的定位滚轮3之间。所述出渣筒5置于水封槽4内。Referring to FIG. 1 , the power wheel 13 is a sprocket, and is connected to the sprocket 21 on the shaft of the motor 17a through a transmission chain. The motor 17a is a speed regulating motor. The structure of the screw conveyor 15 is that it has a cylinder body 23, on which a feeding hopper 14 is arranged, and a matching screw rod 24 is built in the cylinder body 23, and the screw rod 24 is connected with the shaft of the motor 22b.
下面利用图1和2,简述微波滚筒干馏装置作为干馏热解油页岩的具体应用实例:将粒度为0~30mm的油页岩颗粒,由螺旋输送机15的喂料斗14进入螺旋输送机15送入内螺旋滚筒9内,油页岩颗粒在内螺旋滚筒9螺旋推料叶片12的推动下,沿内螺旋滚筒9螺旋位移从微波炉体1进口端进入,在内螺旋滚筒9螺旋推料叶片12和扬料倾斜叶片10的双重作用下,沿内螺旋滚筒9螺旋位移的同时翻滚,油页岩颗粒在微波炉体1吸收微波,干馏热解后,从微波炉体1出口端移出,再由内螺旋滚筒9的螺旋推料叶片12推出内螺旋滚筒9,排入出渣筒5,在水封槽4得到冷却,所产气体由出气管7导出,经干馏、冷凝得到页岩油、瓦斯气和半焦。Using Figures 1 and 2, a specific application example of the microwave drum retort device as retort pyrolysis oil shale is briefly described below: the oil shale particles with a particle size of 0-30 mm are fed into the screw conveyor 15 through the feeding hopper 14 15 into the inner
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Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101020828B (en) * | 2007-02-15 | 2011-05-04 | 东北电力大学 | Microwave drum dry distiller and its application in dry distilling and pyrolyzing oil shale |
| CN102206515A (en) * | 2011-04-26 | 2011-10-05 | 山东大学 | Biomass poly-generation comprehensive utilization method and device |
| CN102226112A (en) * | 2011-06-03 | 2011-10-26 | 徐州燃控科技股份有限公司 | Microwave entrained flow bed two-stage biomass gasifying technique |
| CN102649725A (en) * | 2011-02-24 | 2012-08-29 | 中国科学院金属研究所 | Microwave-enhanced esterification rectifying device and process |
| CN104129608A (en) * | 2014-07-15 | 2014-11-05 | 湖州大周高分子材料有限公司 | Powder conveying and heating device and powder conveying and heating method |
| CN104759446A (en) * | 2015-03-26 | 2015-07-08 | 广东新优威印刷装备科技有限公司 | A method for heat storage microwave treatment of waste or coal |
| CN105154115A (en) * | 2015-08-06 | 2015-12-16 | 南京师范大学 | Helical continuous microwave pyrolyzating and charing apparatus for biomass |
| CN115505414A (en) * | 2021-06-07 | 2022-12-23 | 中国石油化工股份有限公司 | Oil production system and method of small-particle oil shale |
-
2007
- 2007-02-15 CN CN 200720093337 patent/CN201027197Y/en not_active Expired - Lifetime
Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101020828B (en) * | 2007-02-15 | 2011-05-04 | 东北电力大学 | Microwave drum dry distiller and its application in dry distilling and pyrolyzing oil shale |
| CN102649725A (en) * | 2011-02-24 | 2012-08-29 | 中国科学院金属研究所 | Microwave-enhanced esterification rectifying device and process |
| CN102649725B (en) * | 2011-02-24 | 2014-04-16 | 中国科学院金属研究所 | Microwave-enhanced esterification rectifying device and process |
| CN102206515A (en) * | 2011-04-26 | 2011-10-05 | 山东大学 | Biomass poly-generation comprehensive utilization method and device |
| CN102226112A (en) * | 2011-06-03 | 2011-10-26 | 徐州燃控科技股份有限公司 | Microwave entrained flow bed two-stage biomass gasifying technique |
| CN104129608A (en) * | 2014-07-15 | 2014-11-05 | 湖州大周高分子材料有限公司 | Powder conveying and heating device and powder conveying and heating method |
| CN104759446A (en) * | 2015-03-26 | 2015-07-08 | 广东新优威印刷装备科技有限公司 | A method for heat storage microwave treatment of waste or coal |
| CN105154115A (en) * | 2015-08-06 | 2015-12-16 | 南京师范大学 | Helical continuous microwave pyrolyzating and charing apparatus for biomass |
| CN105154115B (en) * | 2015-08-06 | 2017-06-23 | 南京师范大学 | A kind of spiral biomass continuous microwave pyrolysis charring device |
| CN115505414A (en) * | 2021-06-07 | 2022-12-23 | 中国石油化工股份有限公司 | Oil production system and method of small-particle oil shale |
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