CN1923748A - Gold color circle seven-color particle porcelain tile and preparation method thereof - Google Patents
Gold color circle seven-color particle porcelain tile and preparation method thereof Download PDFInfo
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- CN1923748A CN1923748A CN 200610122253 CN200610122253A CN1923748A CN 1923748 A CN1923748 A CN 1923748A CN 200610122253 CN200610122253 CN 200610122253 CN 200610122253 A CN200610122253 A CN 200610122253A CN 1923748 A CN1923748 A CN 1923748A
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- 239000002245 particle Substances 0.000 title claims description 16
- 229910052573 porcelain Inorganic materials 0.000 title claims description 5
- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 title abstract 2
- 239000010931 gold Substances 0.000 title 1
- 229910052737 gold Inorganic materials 0.000 title 1
- 238000002360 preparation method Methods 0.000 title 1
- 239000004576 sand Substances 0.000 claims abstract description 39
- 239000000843 powder Substances 0.000 claims abstract description 25
- 239000004575 stone Substances 0.000 claims abstract description 15
- 239000012780 transparent material Substances 0.000 claims abstract description 14
- 239000005995 Aluminium silicate Substances 0.000 claims abstract description 9
- 235000012211 aluminium silicate Nutrition 0.000 claims abstract description 9
- NLYAJNPCOHFWQQ-UHFFFAOYSA-N kaolin Chemical compound O.O.O=[Al]O[Si](=O)O[Si](=O)O[Al]=O NLYAJNPCOHFWQQ-UHFFFAOYSA-N 0.000 claims abstract description 9
- 238000001035 drying Methods 0.000 claims abstract description 8
- 238000004519 manufacturing process Methods 0.000 claims abstract description 8
- 238000000465 moulding Methods 0.000 claims abstract description 7
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 claims abstract description 5
- 238000005498 polishing Methods 0.000 claims abstract description 4
- 238000005507 spraying Methods 0.000 claims abstract description 3
- 239000000463 material Substances 0.000 claims description 57
- 239000000203 mixture Substances 0.000 claims description 17
- 238000009738 saturating Methods 0.000 claims description 15
- 238000005469 granulation Methods 0.000 claims description 12
- 230000003179 granulation Effects 0.000 claims description 12
- 229910052777 Praseodymium Inorganic materials 0.000 claims description 9
- PUDIUYLPXJFUGB-UHFFFAOYSA-N praseodymium atom Chemical compound [Pr] PUDIUYLPXJFUGB-UHFFFAOYSA-N 0.000 claims description 9
- 238000005516 engineering process Methods 0.000 claims description 8
- 238000000034 method Methods 0.000 claims description 8
- 239000002002 slurry Substances 0.000 claims description 8
- 238000010304 firing Methods 0.000 claims description 7
- 230000002631 hypothermal effect Effects 0.000 claims description 7
- 238000000498 ball milling Methods 0.000 claims description 6
- 239000002994 raw material Substances 0.000 claims description 5
- 238000002347 injection Methods 0.000 claims description 4
- 239000007924 injection Substances 0.000 claims description 4
- 239000004567 concrete Substances 0.000 claims description 3
- 238000009472 formulation Methods 0.000 claims description 3
- 239000003086 colorant Substances 0.000 claims description 2
- 150000001875 compounds Chemical class 0.000 claims description 2
- 238000007689 inspection Methods 0.000 claims description 2
- 238000012856 packing Methods 0.000 claims description 2
- 239000007921 spray Substances 0.000 claims description 2
- 238000007873 sieving Methods 0.000 claims 1
- 239000011449 brick Substances 0.000 abstract description 5
- 239000000919 ceramic Substances 0.000 abstract description 3
- 238000007639 printing Methods 0.000 abstract description 3
- 239000013078 crystal Substances 0.000 abstract 1
- 238000000227 grinding Methods 0.000 abstract 1
- 238000002156 mixing Methods 0.000 abstract 1
- 238000005245 sintering Methods 0.000 abstract 1
- 235000013339 cereals Nutrition 0.000 description 35
- 230000000694 effects Effects 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- 238000003825 pressing Methods 0.000 description 2
- 230000035807 sensation Effects 0.000 description 2
- 229910004298 SiO 2 Inorganic materials 0.000 description 1
- 235000019892 Stellar Nutrition 0.000 description 1
- 229910010413 TiO 2 Inorganic materials 0.000 description 1
- 230000004075 alteration Effects 0.000 description 1
- 239000004566 building material Substances 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000009792 diffusion process Methods 0.000 description 1
- 238000005562 fading Methods 0.000 description 1
- 235000013312 flour Nutrition 0.000 description 1
- 239000008187 granular material Substances 0.000 description 1
- 239000010977 jade Substances 0.000 description 1
Landscapes
- Compositions Of Oxide Ceramics (AREA)
Abstract
The invention discloses a gold ring seven-color ceramic permeating polishing brick and manufacturing method, which comprises the following steps: allocating crystal transparent material with 30-40% white stone powder, 10-15% Chaozhou sand, 5-10% Guangxi sand, 10-15% low-temperature sand, 15-25% super-white sand, 0-10% kaolin and 5-10% black mud; preparing super-white formula with 5-15% white stone powder, 5-15% Chaozhou sand, 20-35% Guangxi sand, 10-25% super-white sand, 10-15% low-temperature sand, 0-10% kaolin, 3-10% black mud, 10-20% Nanchang sand and 5-10% high-alumina sand; grinding; mixing color; spraying; drying; graining; moulding; drying; printing; assisting permeating; sintering; polishing to obtain the product.
Description
Technical field
The present invention relates to the production method of a kind of golden ring seven coloured particles porcelain seep curlicue polished tile and this product.
Background technology
Along with improving constantly of people's living standard, pursue stone effect, the estheticism of back to nature also improves day by day, and people are also more and more higher to the requirement of decorating.Common to ooze colored polished tile heavy partially because of its tone, and color is abundant, dim pattern, can not satisfy the requirement that people pursue the life grade, common macrobead is because granulometric composition is too simple, level is abundant inadequately, gives the sensation of terrazzo, the building materials market of fading out gradually.The particle pattern permeating tile that also has some producers to release is also dark excessively owing to the brick background color, the particle collocation is too simple, lack special border colored particles with colour circle effect, it is serious to ooze the diffusion of floral pattern lines simultaneously, dim pattern, to ooze flower also poor than common for decorative effect after the whole paving, can not satisfy market and requirement of client.Though the lithotome rich color, aberration is big, and radioactivity exceeds standard, and can not satisfy the pursuit of people to healthy living, makes us talking stone and becomes, and has greatly limited use range.
Summary of the invention
In order to remedy the deficiency on the existing production technology, purpose of the present invention just provides the production method of a kind of golden colour circle seven coloured particles ceramic brick with permeated pattern and this product.
For achieving the above object, the technical scheme of composition of raw materials provided by the invention is: the quartzy transparent material formulation compositing range of this pattern permeating tile is: white stone powder 30-40, Chaozhou sand 10-15, Guangxi sand 5-10, hypothermia grait 10-15, super-white sand 15-25, kaolin 0-10, black mud 5-10;
The super-white marerial prescription is formed: white stone powder 5-15, Chaozhou sand 5-15, Guangxi sand 20-35, super-white sand 10-25, hypothermia grait 10-15, kaolin 10-15, black mud 3-10, Nanchang sand 10-20, high alumina sand 5-10.
The concrete steps of the production method of pattern permeating tile of the present invention are:
(1), batching:, batching is entered feeding machine release mill by the selected domestic high-quality natural matter of prescription;
(2), ball milling: the raw material that has entered feeding machine sieves through deironing after ball milling is qualified to moisture content, fineness, viscosity, and to put into stock tank old, concrete processing parameter: slurry ball milling time 10-12 hour, slurry moisture content 30-35%, slurry fineness 0.8-1.2%, slurry viscosity 30-45 second;
(3), colour mixture: according to proportioning colorant is added and to be stirred well to evenly colour mixture processing parameter: pink material super-white marerial 100%+LX-013 0.1-1.0% in the mud
+LX-116 0.5-1.5％
The yellow material of powder super-white marerial 100%+LX-115 0.5-1.0%
+ high safe praseodymium yellow 0.1-0.5%
Whitewash material super-white marerial 100%+LX-106 1.5-2.5%
Saturating ash material quartzy transparent material+LX-012 0.1-0.5%
+ high safe praseodymium yellow 0.1-0.5%
Saturating yellow material quartzy transparent material+LX-011 0.1-0.5%
+ high safe praseodymium yellow 0.1-0.5%
(4), spraying drying: spray-dried moisture content and the qualified powder of particle grating of making of mud mill base, spray tower powder moisture content 7-8%, granulation powder moisture content 10-11%;
(5), granulation: granulation process parameters moisture content 9.5-11%, granulation pressure 8-10Pa grain composition parameter
| The particle title | The A1 grain | The A2 grain | The A3 grain | T is transparent | The B grain | The C grain | The D grain |
| Grating (order) | 8-12 | 4-8 | 4-8 | 4-8 | 6-10 | 4-10 | 8-12 |
(6), moulding: form base-material by 7 kinds of different powders, the compound of forming with 7 kinds of variable grains again, wherein:
The base-material proportioning
| Material is planted | Super-white marerial | Pink material | The yellow material of powder | Transparent material | Saturating yellow material | Saturating ash material | Whitewash |
| Ratio | 15-25％ | 35-45％ | 20-30％ | 5-10％ | 1-3％ | 3-8％ | 2-5％ |
Mix material proportioning
| Material is planted | Base-material | The A1 grain | The A2 grain | T is transparent | The B grain | The C grain | The D grain | The A3 grain |
| Ratio | 93-97％ | 0.2-0.5％ | 0.2-0.5％ | 0.1-0.5％ | 0.5-1.0％ | 0.1-0.5％ | 1.0-2.0％ | 0.1-2.0％ |
(7), drying: moulding adobe drying is qualified to moisture content, make adobe that certain intensity be arranged, adapt to the postorder operation;
(8), stamp helps and ooze: according to space of a whole page difference, print the different fancy glazes that oozes, glazing line adopts 4 stamps and helps the technology of oozing 4 times, glaze Wiring technology parameter: ooze fancy glaze viscosity 2-3 minute, help and ooze injection flow rate 76-78g;
(9), burn till: product burns till through 1270 ℃ of high temperature, and firing period reaches 90 minutes, and the finished product water-intake rate is less than 0.1;
(10), polishing: will burn till the adobe surface finish to certain glossiness, through the quality inspection packing warehouse entry that is up to the standards.
The fragmentary golden colour circle enwrapped granule that distributes of product surface of the present invention shows luxurious style, seven coloured particles levels are rich grain grain differences, the charm of more apparent superpower imitative stone, especially quartzy transparent grain and the reasonably combined use of powder, be randomly distributed in the surface of brick, saturating like the sparkling and crystal-clear jade of stellar scintillation, floral pattern is oozed on the surface, come from the characteristics that Spain's Filetto Rosso stone material has the lines clear and natural, the smoothness of seemingly racking, extraordinary refined, whole paving is reproduced like stone material to people's sensation, show consummate stone-imitation art, build the living space of noble graceful atmosphere.Simultaneously, the raw materials used radioactivity that do not contain has thoroughly broken away from the lithotome radiocontamination.
Embodiment:
The present invention is further described below in conjunction with two embodiment.
Embodiment 1:
1, prescription and chemical constitution:
Quartzy transparent material formulation: white stone powder 37, Chaozhou sand 13, Guangxi sand 5.5, hypothermia grait 12, super-white sand 18, kaolin 8, black mud 7.5;
Super-white marerial prescription: white stone powder 5, Chaozhou sand 7, Guangxi sand 24, super-white sand 19, hypothermia grait 13, kaolin 12, black mud 4.5, Nanchang sand 12, high alumina sand 5.5.
The chemical constitution of above-mentioned raw materials is:
| SiO 2 | Al 2O 3 | Fe 2O 3 | TiO 2 | CaO | MgO | K 2O | Na 2O | I.L | |
| White stone powder | 73.44 | 15.86 | 0.25 | 0.06 | 0.51 | 0.23 | 4.57 | 2.82 | 2.31 |
| Chaozhou sand | 77.76 | 15.41 | 0.23 | 0.01 | 0.28 | 0.19 | 3.01 | 0.33 | 2.66 |
| Guangxi sand | 75.82 | 16.57 | 0.31 | 0.07 | 0.27 | 0.13 | 3.73 | 0.11 | 3.08 |
| The Hunan stone flour | 65.15 | 22.43 | 0.15 | 0.10 | 0.31 | 0.09 | 0.12 | 9.98 | 1.62 |
| Super-white sand | 70.80 | 17.71 | 0.26 | 0.08 | 0.18 | 0.33 | 1.73 | 6.94 | 1.73 |
| Kaolin | 52.67 | 33.03 | 0.82 | 0.30 | 0.08 | 0.15 | 1.03 | 0.11 | 11.96 |
| Black mud | 57.36 | 27.64 | 1.07 | 0.48 | 0.15 | 0.21 | 0.77 | 0.01 | 12.60 |
| High alumina sand | 69.39 | 21.29 | 0.48 | 0.15 | 0.22 | 0.15 | 0.56 | 0.11 | 7.54 |
| Hypothermia grait | 68.44 | 19.32 | 0.19 | 0.16 | 0.47 | 0.10 | 0.22 | 9.62 | 1.69 |
| Nanchang sand | 77.68 | 16.06 | 0.21 | 0.07 | 0.12 | 0.05 | 0.84 | 0.12 | 5.05 |
2, colour mixture processing parameter:
Pink material super-white marerial 100%+LX-013 0.13%
+LX-116 0.78％
The yellow material of powder super-white marerial 100%+LX-115 0.88%
+ high safe praseodymium yellow 0.28%
Whitewash material super-white marerial 100%+LX-106 1.5%
The quartzy transparent material+LX-012 0.4% of saturating ash material
+ high safe praseodymium yellow 0.25%
The quartzy transparent material+LX-011 0.2% of saturating yellow material
+ high safe praseodymium yellow 0.25%
3, granulation process parameters
| The particle title | The A1 grain | The A2 grain | The A3 grain | T is transparent | The B grain | The C grain | The D grain |
| Grating (order) | 12 | 6 | 4 | 6 | 10 | 10 | 10 |
Granulation moisture content 10%
Granulation pressure 10Pa
4, molding technique parameter
1. base-material proportioning
| Material is planted | Super-white marerial | Pink material | The yellow material of powder | Transparent material | Saturating yellow material | Saturating ash material | Whitewash |
| Ratio | 22％ | 42％ | 26％ | 5％ | 1.3％ | 3.7％ | 2％ |
2. mix material proportioning
| Material is planted | Base-material | The A1 grain | The A2 grain | The A3 grain | T is transparent | The B grain | The C grain | The D grain |
| Ratio | 96％ | 0.3％ | 0.5％ | 0.1％ | 0.36％ | 0.9％ | 0.4％ | 1.0％ |
1. moisture content: base-material moisture content 7.7%.
2. pressing mode: malleation.Pressure 350bar.
5, glaze Wiring technology parameter
Printing screen plate numbering NP63804
Oozed fancy glaze viscosity 2 minutes
Help and ooze injection flow rate 78g
6, firing process parameter
Firing temperature
| Firing zone | 1 | 2 | 3 | 4 | 5 | 6 | 7 | 8 | 9 | 10 |
| The face temperature | 1014 | 1086 | 1135 | 1189 | 1196 | 1217 | 1249 | 1215 | 1269 | 1273 |
| End temperature | 1086 | 1215 | 1238 | 1245 | 1251 | 1258 | 1260 | 1267 | 1248 | 1269 |
| Firing zone | 11 | 12 | 13 | 14 | 15 | 16 | 17 | 18 | 19 | 20 |
| The face temperature | 1273 | 1271 | 1269 | 1268 | 1263 | 1264 | 1257 | 1189 | 1110 | 992 |
| End temperature | 1259 | 1164 | 1260 | 1269 | 1261 | 1264 | 1249 | 1189 | 1078 | 950 |
Embodiment 2:
1, prescription and chemical constitution: identical with embodiment 1
2, colour mixture processing parameter: identical with embodiment 1
3, granulation process parameters: identical with embodiment 1
4, molding technique parameter:
1. base-material proportioning
| Material is planted | Super-white marerial | Pink material | The yellow material of powder | Transparent material | Saturating yellow material | Saturating ash material | Whitewash |
| Ratio | 22％ | 42％ | 26％ | 5％ | 1.3％ | 3.7％ | 2％ |
2. mix material proportioning
| Material is planted | Base-material | The A1 grain | The A2 grain | The A3 grain | T is transparent | The B grain | The C grain | The D grain |
| Ratio | 96％ | 0.3％ | 0.5％ | 0.1％ | 0.36％ | 0.9％ | 0.4％ | 1.0％ |
Moisture content: base-material moisture content 7.7%; Pressing mode: malleation; Pressure: 350bar.
5, glaze Wiring technology parameter
Printing screen plate numbering SP6B02
Oozed fancy glaze viscosity 2 minutes
Help and ooze injection flow rate 78g
6, firing process parameter: identical with embodiment 1.
By above two embodiments, we print the golden colour circle seven coloured particles ceramic brick with permeated pattern that different patterns obtains two kinds of different-styles.
Claims (2)
1, a kind of golden colour circle seven coloured particles porcelain seep curlicue polished tile, it is characterized in that: the quartzy transparent material formulation compositing range of this pattern permeating tile is: white stone powder 30-40, Chaozhou sand 10-15, Guangxi sand 5-10, hypothermia grait 10-15, super-white sand 15-25, kaolin 0-10, black mud 5-10; The super-white marerial prescription is formed: white stone powder 5-15, Chaozhou sand 5-15, Guangxi sand 20-35, super-white sand 10-25, hypothermia grait 10-15, kaolin 10-15, black mud 3-10, Nanchang sand 10-20, high alumina sand 5-10.
2, a kind of production method of golden colour circle seven coloured particles porcelain seep curlicue polished tile, it is characterized in that: the concrete steps of this production method are:
(1), batching:, batching is entered feeding machine release mill by the selected domestic high-quality natural matter of prescription;
(2), ball milling: the raw material that has entered feeding machine is after ball milling is qualified to moisture content, fineness, viscosity, sieving through deironing, to put into stock tank old, processing parameter: slurry ball milling time 10-12 hour, slurry moisture content 30-35%, slurry fineness 0.8-1.2%, slurry viscosity 30-45 second;
(3), colour mixture: according to proportioning colorant is added and to be stirred well to evenly colour mixture processing parameter: pink material super-white marerial 100%+LX-013 0.1-1.0% in the mud
+LX-116 0.5-1.5％
The yellow material of powder super-white marerial 100%+LX-115 0.5-1.0%
+ high safe praseodymium yellow 0.1-0.5%
Whitewash material super-white marerial 100%+LX-106 1.5-2.5%
Saturating ash material quartzy transparent material+LX-012 0.1-0.5%
+ high safe praseodymium yellow 0.1-0.5%
Saturating yellow material quartzy transparent material+LX-011 0.1-0.5%
+ high safe praseodymium yellow 0.1-0.5%
(4), spraying drying: spray-dried moisture content and the qualified powder of particle grating of making of mud mill base, spray tower powder moisture content 7-8%, granulation powder moisture content 10-11%;
(5), granulation: granulation process parameters moisture content 9.5-11%, granulation pressure 8-10Pa grain composition parameter
The particle title The A1 grain The A2 grain The A3 grain T is transparent The B grain The C grain The D grain
Grating (order) 8-12 4-8 4-8 4-8 6-10 4-10 8-12
(6), moulding: form base-material by 7 kinds of different powders, the compound of forming with 7 kinds of variable grains again, wherein:
The base-material proportioning
Material is planted Super-white marerial Pink material The yellow material of powder Transparent material Saturating yellow material Saturating ash material Whitewash
Ratio 15-25％ 35-45％ 20-30％ 5-10％ 1-3％ 3-8％ 2-5％
Mix material proportioning
Material is planted Base-material The A1 grain The A2 grain T is transparent The B grain The C grain The D grain The A3 grain
Ratio 93-97 ％ 0.2-0.5 ％ 0.2-0.5％ 0.1-0.5％ 0.5-1.0％ 0.1-0.5 ％ 1.0-2.0 ％ 0.1-2.0％
(7), drying: moulding adobe drying is qualified to moisture content, make adobe that certain intensity be arranged, adapt to the postorder operation;
(8), stamp helps and ooze: according to space of a whole page difference, print the different fancy glazes that oozes, glazing line adopts 4 stamps and helps the technology of oozing 4 times, glaze Wiring technology parameter: ooze fancy glaze viscosity 2-3 minute, help and ooze injection flow rate 76-78g;
(9), burn till: product burns till through 1270 ℃ of high temperature, and firing period reaches 90 minutes, and the finished product water-intake rate is less than 0.1;
(10), polishing: will burn till the adobe surface finish to certain glossiness, through the quality inspection packing warehouse entry that is up to the standards.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 200610122253 CN1923748A (en) | 2006-09-19 | 2006-09-19 | Gold color circle seven-color particle porcelain tile and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 200610122253 CN1923748A (en) | 2006-09-19 | 2006-09-19 | Gold color circle seven-color particle porcelain tile and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN1923748A true CN1923748A (en) | 2007-03-07 |
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ID=37816597
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 200610122253 Pending CN1923748A (en) | 2006-09-19 | 2006-09-19 | Gold color circle seven-color particle porcelain tile and preparation method thereof |
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| Country | Link |
|---|---|
| CN (1) | CN1923748A (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105712702A (en) * | 2015-09-18 | 2016-06-29 | 安庆惠嘉新型建材有限公司 | Process for producing tiles in walls |
| CN107746254A (en) * | 2017-11-15 | 2018-03-02 | 恩平市华昌陶瓷有限公司 | The ceramic toner produced using natural mineral raw |
| CN113968727A (en) * | 2021-09-26 | 2022-01-25 | 蒙娜丽莎集团股份有限公司 | Gold polishing particle, gold polishing terrazzo ceramic plate and preparation method thereof |
| CN116477928A (en) * | 2023-04-25 | 2023-07-25 | 湖南旭日陶瓷有限公司 | A kind of imitation black stone grain and its manufacturing method |
-
2006
- 2006-09-19 CN CN 200610122253 patent/CN1923748A/en active Pending
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105712702A (en) * | 2015-09-18 | 2016-06-29 | 安庆惠嘉新型建材有限公司 | Process for producing tiles in walls |
| CN107746254A (en) * | 2017-11-15 | 2018-03-02 | 恩平市华昌陶瓷有限公司 | The ceramic toner produced using natural mineral raw |
| CN107746254B (en) * | 2017-11-15 | 2021-01-15 | 恩平市华昌陶瓷有限公司 | Ceramic toner produced by using natural mineral raw materials |
| CN113968727A (en) * | 2021-09-26 | 2022-01-25 | 蒙娜丽莎集团股份有限公司 | Gold polishing particle, gold polishing terrazzo ceramic plate and preparation method thereof |
| CN116477928A (en) * | 2023-04-25 | 2023-07-25 | 湖南旭日陶瓷有限公司 | A kind of imitation black stone grain and its manufacturing method |
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