CN1742636B - Technology for producing pollution-free liquid cigarette - Google Patents
Technology for producing pollution-free liquid cigarette Download PDFInfo
- Publication number
- CN1742636B CN1742636B CN 200410055377 CN200410055377A CN1742636B CN 1742636 B CN1742636 B CN 1742636B CN 200410055377 CN200410055377 CN 200410055377 CN 200410055377 A CN200410055377 A CN 200410055377A CN 1742636 B CN1742636 B CN 1742636B
- Authority
- CN
- China
- Prior art keywords
- temperature
- pipe tobacco
- destructive distillation
- flue gas
- retort
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 18
- 239000007788 liquid Substances 0.000 title claims abstract description 16
- 238000005516 engineering process Methods 0.000 title claims description 11
- 241000208125 Nicotiana Species 0.000 claims abstract description 40
- 235000002637 Nicotiana tabacum Nutrition 0.000 claims abstract description 40
- 238000000197 pyrolysis Methods 0.000 claims abstract description 19
- 238000001816 cooling Methods 0.000 claims abstract description 17
- 238000004519 manufacturing process Methods 0.000 claims abstract description 12
- 239000002994 raw material Substances 0.000 claims abstract description 11
- 238000000034 method Methods 0.000 claims abstract description 10
- SNICXCGAKADSCV-JTQLQIEISA-N (-)-Nicotine Chemical compound CN1CCC[C@H]1C1=CC=CN=C1 SNICXCGAKADSCV-JTQLQIEISA-N 0.000 claims abstract description 7
- 229960002715 nicotine Drugs 0.000 claims abstract description 7
- SNICXCGAKADSCV-UHFFFAOYSA-N nicotine Natural products CN1CCCC1C1=CC=CN=C1 SNICXCGAKADSCV-UHFFFAOYSA-N 0.000 claims abstract description 7
- 230000005494 condensation Effects 0.000 claims abstract description 5
- 238000009833 condensation Methods 0.000 claims abstract description 4
- 239000000463 material Substances 0.000 claims abstract description 4
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 claims description 25
- 239000003546 flue gas Substances 0.000 claims description 24
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 7
- 238000000855 fermentation Methods 0.000 claims description 5
- 230000004151 fermentation Effects 0.000 claims description 5
- 235000011194 food seasoning agent Nutrition 0.000 claims description 5
- 238000009413 insulation Methods 0.000 claims description 4
- 238000012545 processing Methods 0.000 claims description 4
- 210000000988 bone and bone Anatomy 0.000 claims description 3
- 238000003763 carbonization Methods 0.000 claims description 3
- 230000018044 dehydration Effects 0.000 claims description 3
- 238000006297 dehydration reaction Methods 0.000 claims description 3
- 238000012216 screening Methods 0.000 claims description 3
- 230000011218 segmentation Effects 0.000 claims description 3
- 238000001914 filtration Methods 0.000 abstract 1
- 238000000265 homogenisation Methods 0.000 abstract 1
- 238000004806 packaging method and process Methods 0.000 abstract 1
- 235000011389 fruit/vegetable juice Nutrition 0.000 description 14
- 230000006378 damage Effects 0.000 description 7
- 239000007789 gas Substances 0.000 description 7
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 description 3
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 3
- 239000012071 phase Substances 0.000 description 3
- 230000000391 smoking effect Effects 0.000 description 3
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 2
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 2
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 2
- 229940079593 drug Drugs 0.000 description 2
- 239000003814 drug Substances 0.000 description 2
- LELOWRISYMNNSU-UHFFFAOYSA-N hydrogen cyanide Chemical compound N#C LELOWRISYMNNSU-UHFFFAOYSA-N 0.000 description 2
- 239000007791 liquid phase Substances 0.000 description 2
- 239000007790 solid phase Substances 0.000 description 2
- 231100000331 toxic Toxicity 0.000 description 2
- 230000002588 toxic effect Effects 0.000 description 2
- 235000013619 trace mineral Nutrition 0.000 description 2
- 239000011573 trace mineral Substances 0.000 description 2
- 239000002699 waste material Substances 0.000 description 2
- 241000282326 Felis catus Species 0.000 description 1
- 206010028980 Neoplasm Diseases 0.000 description 1
- 229910021529 ammonia Inorganic materials 0.000 description 1
- 229910052785 arsenic Inorganic materials 0.000 description 1
- RQNWIZPPADIBDY-UHFFFAOYSA-N arsenic atom Chemical compound [As] RQNWIZPPADIBDY-UHFFFAOYSA-N 0.000 description 1
- 229910052793 cadmium Inorganic materials 0.000 description 1
- BDOSMKKIYDKNTQ-UHFFFAOYSA-N cadmium atom Chemical compound [Cd] BDOSMKKIYDKNTQ-UHFFFAOYSA-N 0.000 description 1
- 229910002092 carbon dioxide Inorganic materials 0.000 description 1
- 239000001569 carbon dioxide Substances 0.000 description 1
- 229910002091 carbon monoxide Inorganic materials 0.000 description 1
- 201000010099 disease Diseases 0.000 description 1
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 1
- 238000006073 displacement reaction Methods 0.000 description 1
- 238000005538 encapsulation Methods 0.000 description 1
- 239000008187 granular material Substances 0.000 description 1
- 239000000383 hazardous chemical Substances 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 229910001385 heavy metal Inorganic materials 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 239000005416 organic matter Substances 0.000 description 1
- 238000012536 packaging technology Methods 0.000 description 1
- 238000012856 packing Methods 0.000 description 1
- 150000002989 phenols Chemical class 0.000 description 1
- 125000005575 polycyclic aromatic hydrocarbon group Chemical group 0.000 description 1
- 238000012805 post-processing Methods 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 239000000779 smoke Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
Landscapes
- Manufacture Of Tobacco Products (AREA)
Abstract
The production process of nuisance-free liquid cigarette is characterized by that it selects the tobacco leaf whose total sugar content is less than 4% and nicotine content is less than 2% as raw material. Its production process includes the following procedures: selecting material, treating, dry distillation, cooling, condensation and homogenization, filtering, flavouring and packaging.
Description
Affiliated field
The present invention relates to technical field of cigarette production, particularly a kind of production technology of liquid cigarette.
Background technology
According to about research with measure, TPM about 4.5 * 10 contains hazardous substance in the cigarette smoke
12Grain, about tar content 40mg, the about 2.6mg of nicotine (being nicotine), carbon monoxide 100mg, carbon dioxide 150mg, phenolic compound 0.8mg, ammonia 7.5mg, acetone 2mg, formaldehyde 1.4mg, toluene 0.7mg, hydrogen cyanide 0.4mg, various polycyclic aromatic hydrocarbon 6.5mg, be lower than some kinds in 1.0mg heavy metal (cadmium, arsenic, plug with molten metal etc.), can cause or inspire various cancers and other diseases in various degree.And main granule phase substance matter, tar, nicotine are maximum to human body harm.Chinese patent " production technology of ZL 99121451X liquid cigarettes without public hazard " has many limitation, and definite liquid of only getting 380 ℃～420 ℃ of this section pyrolysis temperatures is that tobacco juice obviously is that receipts liquid rate is low, and quantity of three wastes is big, and does not also consider the disposal of three wastes, and cost is too high.
Summary of the invention
Purpose of the present invention just provide a kind of with the organic tobacco leaf of solid phase (S) through the non-isothermal thermal insulation destructive distillation of heating, make organic matter become gas phase (G) by solid phase (S), again with the gas extracting, collect, cooling, become liquid phase (L), be processed into a kind of production technology of liquid cigarette again through post processing, when people during in smoking tobacco juice become flue gas again, satisfy the needs of smoker's cigarette sense, without ignition, can eliminate harm to the involuntary smoker, there is not stub cigarette ash, do not have strong smog, eliminate disaster hidden-trouble and reach, and the toxic organics in the flue gas has reduced to the micro-degree to hazard to person sanitary destruction, and add human body beneficial's drug ingedient and trace element etc., reach the purpose of turning harm into good.
The objective of the invention is to be achieved through the following technical solutions:
A kind of production technology of liquid cigarette, technical process comprises choosing and handling of raw material, destructive distillation, cooling, condensation and homogeneous, smart filter, seasoning, canned program, the processing that it is characterized in that above-mentioned raw materials be select for use contain that the total reducing sugar amount is lower than 4%, nicotine is lower than 2% tobacco leaf and makes raw material, artificial screening removes earth and foreign material, squirts, and the leaf bone is flattened, chopping, the fermentation vat of putting into 40～50 ℃ soaked 3～4 hours, pull out pipe tobacco squeeze 85～90% moisture, become the pipe tobacco cake; The pipe tobacco cake is sent into the dehydration still, under 105 ℃ of temperature through 40 minutes destructive distillation, water becomes steam, again the pipe tobacco cake is sent into second retort, under 235 ℃ of temperature through 40 minutes adiabatic enclosed destructive distillation, produce first order flue gas, again the pipe tobacco cake is sent into the 3rd retort, under 430 ℃ of temperature after the adiabatic enclosed destructive distillation of 40 minutes middle temperature, produce second level flue gas, again the pipe tobacco cake of carbonization at low temperature is sent into the 4th retort, under 555 ℃ of temperature after 40 minutes high-temperature heat insulation enclosed destructive distillation, produce third level flue gas.
Above-mentioned retort process is that segmentation is carried out in four tower retorts of still.
The present invention drops into 1 kilogram of pipe tobacco, and the tobacco juice that can regain is 580 grams, establishes the raw material input and be K (unfilled corner mark 1), and tobacco juice withdrawal amount is K (a unfilled corner mark 2), yield K (unfilled corner mark 0)=K (unfilled corner mark 2)/K (unfilled corner mark 1) * %, and promptly 58%, production cost is low.Its product makes people's tobacco juice when smoking become flue gas again, can satisfy the needs of smoker's cigarette sense, without ignition, can eliminate harm, not have stub cigarette ash, not have strong smog the involuntary smoker, eliminating disaster hidden-trouble reaches sanitary destruction, and the toxic organics in the flue gas reduced to the micro-degree to hazard to person, and adds human body beneficial's drug ingedient and trace element etc., turns harm into good.
Description of drawings
Fig. 1 is the tower retort structural representation of still used in the present invention
The specific embodiment
A kind of production technology of liquid cigarette, technical process comprise choosing and handling of raw material, destructive distillation, cooling, condensation and homogeneous, smart filter, seasoning, canned program.The processing of raw material be select for use contain that the total reducing sugar amount is lower than 4%, nicotine is lower than 2% tobacco leaf and makes raw material, artificial screening removes earth and foreign material, squirts, the leaf bone is flattened, chopping, the fermentation vat of putting into 40～50 ℃ soaked 3～4 hours, pull out pipe tobacco squeeze 85～90% moisture, be treated as the pipe tobacco cake.
Destructive distillation is that segmentation is carried out in four tower retorts of still, retort process is: the pipe tobacco cake is sent into the dehydration still, under 105 ℃ of temperature through 40 minutes destructive distillation, water becomes steam, again the pipe tobacco cake is sent into second retort, under 235 ℃ of temperature through 40 minutes adiabatic enclosed destructive distillation, produce first order flue gas, again the pipe tobacco cake is sent into the 3rd retort, under 430 ℃ of temperature after the adiabatic enclosed destructive distillation of 40 minutes middle temperature, produce second level flue gas, again the pipe tobacco cake of carbonization at low temperature is sent into the 4th retort, under 555 ℃ of temperature after 40 minutes high-temperature heat insulation enclosed destructive distillation, produce third level flue gas.
Cooling, condensation program are the processes that the gas phase flue gas becomes the liquid phase tobacco juice, and the steam of assembling in the tower is imported coiled pipe in the pond from the beginning with appendix, and steam is cooled to hot water, hot water are sent into the feedwater of pipe tobacco fermentation vat again and are heated.The flue gas of assembling in two towers is entered the one-level flue gas cooling worm in steam cooling worm pond by appendix, the flue gas of coiled pipe enters second cooling worm in pond from the beginning again, the flue gas that the second pond coiled pipe comes out enters 25 ℃ condenser again, condensator outlet connects one-level tobacco juice liquid-collecting bottle, flue gas becomes tobacco juice, tobacco juice comes out directly to enter one-level tobacco juice liquid-collecting bottle from condenser, the flue gas that three towers are assembled is introduced second cooling worm in pond from the beginning by appendix, the cigarette that the second pond coiled pipe comes out is introduced the 3rd pond spiral coil cooling tube, the flue gas that the 3rd pond coiled pipe comes out enters-10 ℃ condenser, and condensator outlet inserts secondary tobacco juice liquid-collecting bottle; The flue gas of four tower collection chambers is introduced appendix, introduce the spiral coil cooling tube in the 3rd pond again, the flue gas that the 3rd pond cooling worm comes out inserts the spiral coil cooling tube in the 4th pond again, the flue gas that the 4th pond coiled pipe comes out enters the condenser of-20 ℃ of degree, and the tobacco juice of condensator outlet directly inserts three grades of tobacco juice liquid-collecting bottles.The water of cooling pond will be thrown sparge pipe in the pond into pump, and Chi Shui is carried out the nature cooling, and pond water temperature remains on about 15 ℃,
Homogeneous, smart filter, seasoning, the packaging technology of back processing handling procedure all are conventional technology.
Retort used in the present invention combines still with tower, establish four stills, four towers and be evenly distributed arrangement on an annulus that can regularly rotate 7, and still 4 is a circle on the below, and an oblong openings 5 is established in the bottom of still; Negative pressure tower 2 also is that the circle structure is gone up in the below, and tower covers on the still, and the tower cover is provided with venthole 3, and annulus 7 regularly rotates along clockwise direction at square half waist of still 4, per 40 minutes rotational displacement once, the retort that the pipe tobacco cake is written into successively different temperatures gasifies.The negative pressure cat head has collection chamber, collection chamber is sent into the fermentation vat Chi Shui that heats by will dewater gas in the still of appendix 1, the gas that each retort extracting goes out is entered cooling, the condenser of different temperatures respectively again through the negative pressure assembly by different gas pipelines, gas (G) is become liquid (L), enter different liquid-collecting bottles again, the first liquid of three kinds of tobacco juices of Here it is " liquid cigarette " different stage.Just after liquid process homogeneous, smart filter, blending, seasoning, the accent nutriment, just can canned or directly adorn smoking set, the encapsulation packing.
Claims (2)
1. the production technology of a liquid cigarette, technical process comprises choosing and handling of raw material, destructive distillation, cooling, condensation and homogeneous, smart filter, seasoning, canned program, the processing that it is characterized in that above-mentioned raw materials is to select for use to contain the total reducing sugar amount and be lower than 4%, nicotine is lower than 2% tobacco leaf and makes raw material, artificial screening removes earth and foreign material, squirts, and the leaf bone is flattened, chopping, the fermentation vat of putting into 40～50 ℃ soaked 3～4 hours, pull out pipe tobacco squeeze 85～90% moisture, become the pipe tobacco cake, the pipe tobacco cake is sent into the dehydration still, through 40 minutes destructive distillation, water became steam under 105 ℃ of temperature, again the pipe tobacco cake was sent into second retort, under 235 ℃ of temperature through 40 minutes adiabatic enclosed destructive distillation, produce first order flue gas, again the pipe tobacco cake sent into the 3rd retort, under 430 ℃ of temperature after the adiabatic enclosed destructive distillation of 40 minutes middle temperature, produce second level flue gas, again the pipe tobacco cake of carbonization at low temperature is sent into the 4th retort, under 555 ℃ of temperature after 40 minutes high-temperature heat insulation enclosed destructive distillation, produce third level flue gas.
2. the production technology of a kind of liquid cigarette according to claim 1 is characterized in that described retort process is that segmentation is carried out in four tower retorts of still.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 200410055377 CN1742636B (en) | 2004-09-02 | 2004-09-02 | Technology for producing pollution-free liquid cigarette |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 200410055377 CN1742636B (en) | 2004-09-02 | 2004-09-02 | Technology for producing pollution-free liquid cigarette |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1742636A CN1742636A (en) | 2006-03-08 |
| CN1742636B true CN1742636B (en) | 2010-10-06 |
Family
ID=36138285
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 200410055377 Expired - Fee Related CN1742636B (en) | 2004-09-02 | 2004-09-02 | Technology for producing pollution-free liquid cigarette |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN1742636B (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103169146A (en) * | 2013-02-07 | 2013-06-26 | 赵鸿 | Raw materials for cigarettes, production method and equipment thereof |
Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103315395B (en) * | 2013-07-11 | 2015-05-20 | 山东大学 | Pollution-free low-tar cigarette and manufacturing method thereof |
| CN104041936B (en) * | 2014-06-06 | 2016-08-24 | 山东中烟工业有限责任公司 | A kind of extracting method of electronic cigarette Chinese style mixing odor type style tobacco juice |
| CN104041935B (en) * | 2014-06-06 | 2016-08-24 | 山东中烟工业有限责任公司 | A kind of extracting method of electronic cigarette Chinese style flue-cured tobacco odor type style tobacco juice |
| CN104783323B (en) * | 2015-05-14 | 2016-08-17 | 安徽中烟工业有限责任公司 | A kind of tobacco juice for electronic smoke containing Dry distillated flavor |
| CN105199848A (en) * | 2015-09-07 | 2015-12-30 | 郑小柏 | Method for preparing flavor substance |
| CN105725265A (en) * | 2016-04-28 | 2016-07-06 | 湖南中烟工业有限责任公司 | Device and method for preparing tobacco source basic cigarette flavor material for novel tobacco products |
| CN113812668B (en) * | 2021-09-27 | 2023-03-21 | 浙江中烟工业有限责任公司 | Method for extracting rectified aroma substances by dry distillation of tobacco leaves |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4821747A (en) * | 1986-04-23 | 1989-04-18 | R. J. Reynolds Tobacco Company | Process for treating tobacco and similar organic materials |
| CN1050540A (en) * | 1990-09-06 | 1991-04-10 | 冯世型 | From tobacco, produce the technology of nicotine goods with dry distillation |
| CN1140035A (en) * | 1995-07-08 | 1997-01-15 | 李吉荣 | Method for preparing liquid cigarette |
| CN1168250A (en) * | 1996-11-26 | 1997-12-24 | 梅德章 | Gaseous tobacco product and its production method |
| CN1266655A (en) * | 2000-03-21 | 2000-09-20 | 靳巨龙 | Tobacco extract aerosol as cigarette substitute |
| CN1094048C (en) * | 1999-10-22 | 2002-11-13 | 于志刚 | Technology for producing liquid cigarettes without public hazard |
-
2004
- 2004-09-02 CN CN 200410055377 patent/CN1742636B/en not_active Expired - Fee Related
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4821747A (en) * | 1986-04-23 | 1989-04-18 | R. J. Reynolds Tobacco Company | Process for treating tobacco and similar organic materials |
| CN1050540A (en) * | 1990-09-06 | 1991-04-10 | 冯世型 | From tobacco, produce the technology of nicotine goods with dry distillation |
| CN1140035A (en) * | 1995-07-08 | 1997-01-15 | 李吉荣 | Method for preparing liquid cigarette |
| CN1168250A (en) * | 1996-11-26 | 1997-12-24 | 梅德章 | Gaseous tobacco product and its production method |
| CN1094048C (en) * | 1999-10-22 | 2002-11-13 | 于志刚 | Technology for producing liquid cigarettes without public hazard |
| CN1266655A (en) * | 2000-03-21 | 2000-09-20 | 靳巨龙 | Tobacco extract aerosol as cigarette substitute |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103169146A (en) * | 2013-02-07 | 2013-06-26 | 赵鸿 | Raw materials for cigarettes, production method and equipment thereof |
| CN103169146B (en) * | 2013-02-07 | 2015-07-22 | 赵鸿 | Raw materials for cigarettes, production method and equipment thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN1742636A (en) | 2006-03-08 |
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Granted publication date: 20101006 Termination date: 20110902 |