CN1690085A - Water-soluble polysaccharide and its production process - Google Patents
Water-soluble polysaccharide and its production process Download PDFInfo
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- CN1690085A CN1690085A CN 200410019165 CN200410019165A CN1690085A CN 1690085 A CN1690085 A CN 1690085A CN 200410019165 CN200410019165 CN 200410019165 CN 200410019165 A CN200410019165 A CN 200410019165A CN 1690085 A CN1690085 A CN 1690085A
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- water
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- saccharan
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- 238000004519 manufacturing process Methods 0.000 title claims description 13
- 150000004676 glycans Chemical class 0.000 title abstract 4
- 229920001282 polysaccharide Polymers 0.000 title abstract 4
- 239000005017 polysaccharide Substances 0.000 title abstract 4
- 238000002156 mixing Methods 0.000 claims abstract description 13
- 238000001816 cooling Methods 0.000 claims abstract description 10
- 150000001720 carbohydrates Chemical class 0.000 claims abstract description 9
- 238000006243 chemical reaction Methods 0.000 claims abstract description 7
- 238000010438 heat treatment Methods 0.000 claims abstract description 7
- 239000002253 acid Substances 0.000 claims abstract description 5
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 21
- 239000002994 raw material Substances 0.000 claims description 18
- 235000014633 carbohydrates Nutrition 0.000 claims description 8
- 235000000346 sugar Nutrition 0.000 claims description 7
- 238000002203 pretreatment Methods 0.000 claims description 6
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 claims description 5
- 239000008103 glucose Substances 0.000 claims description 5
- 150000002632 lipids Chemical class 0.000 claims description 5
- FBPFZTCFMRRESA-FSIIMWSLSA-N D-Glucitol Natural products OC[C@H](O)[C@H](O)[C@@H](O)[C@H](O)CO FBPFZTCFMRRESA-FSIIMWSLSA-N 0.000 claims description 4
- FEWJPZIEWOKRBE-JCYAYHJZSA-N Dextrotartaric acid Chemical compound OC(=O)[C@H](O)[C@@H](O)C(O)=O FEWJPZIEWOKRBE-JCYAYHJZSA-N 0.000 claims description 4
- 229930091371 Fructose Natural products 0.000 claims description 4
- 239000005715 Fructose Substances 0.000 claims description 4
- RFSUNEUAIZKAJO-ARQDHWQXSA-N Fructose Chemical compound OC[C@H]1O[C@](O)(CO)[C@@H](O)[C@@H]1O RFSUNEUAIZKAJO-ARQDHWQXSA-N 0.000 claims description 4
- 239000000843 powder Substances 0.000 claims description 4
- 239000000600 sorbitol Substances 0.000 claims description 4
- 229940095064 tartrate Drugs 0.000 claims description 4
- 150000002148 esters Chemical class 0.000 claims description 2
- 125000002791 glucosyl group Chemical group C1([C@H](O)[C@@H](O)[C@H](O)[C@H](O1)CO)* 0.000 claims description 2
- 239000000376 reactant Substances 0.000 claims 1
- HVYWMOMLDIMFJA-DPAQBDIFSA-N cholesterol Chemical compound C1C=C2C[C@@H](O)CC[C@]2(C)[C@@H]2[C@@H]1[C@@H]1CC[C@H]([C@H](C)CCCC(C)C)[C@@]1(C)CC2 HVYWMOMLDIMFJA-DPAQBDIFSA-N 0.000 abstract description 16
- 239000007795 chemical reaction product Substances 0.000 abstract description 11
- 238000012856 packing Methods 0.000 abstract description 11
- 235000012000 cholesterol Nutrition 0.000 abstract description 8
- 235000004213 low-fat Nutrition 0.000 abstract description 2
- 239000000463 material Substances 0.000 abstract 2
- 238000000034 method Methods 0.000 abstract 2
- 125000001931 aliphatic group Chemical group 0.000 abstract 1
- 235000013402 health food Nutrition 0.000 abstract 1
- 235000013305 food Nutrition 0.000 description 18
- 239000000047 product Substances 0.000 description 10
- 235000013325 dietary fiber Nutrition 0.000 description 7
- 238000005516 engineering process Methods 0.000 description 6
- 238000010521 absorption reaction Methods 0.000 description 5
- 210000004369 blood Anatomy 0.000 description 5
- 239000008280 blood Substances 0.000 description 5
- AIHDCSAXVMAMJH-GFBKWZILSA-N levan Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)OC[C@@H]1[C@@H](O)[C@H](O)[C@](CO)(CO[C@@H]2[C@H]([C@H](O)[C@@](O)(CO)O2)O)O1 AIHDCSAXVMAMJH-GFBKWZILSA-N 0.000 description 5
- 238000010298 pulverizing process Methods 0.000 description 5
- DLRVVLDZNNYCBX-UHFFFAOYSA-N Polydextrose Polymers OC1C(O)C(O)C(CO)OC1OCC1C(O)C(O)C(O)C(O)O1 DLRVVLDZNNYCBX-UHFFFAOYSA-N 0.000 description 4
- 239000000835 fiber Substances 0.000 description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
- 206010010774 Constipation Diseases 0.000 description 3
- 206010012601 diabetes mellitus Diseases 0.000 description 3
- 235000005911 diet Nutrition 0.000 description 3
- 210000000936 intestine Anatomy 0.000 description 3
- UFTFJSFQGQCHQW-UHFFFAOYSA-N triformin Chemical compound O=COCC(OC=O)COC=O UFTFJSFQGQCHQW-UHFFFAOYSA-N 0.000 description 3
- 241000193830 Bacillus <bacterium> Species 0.000 description 2
- 241000894006 Bacteria Species 0.000 description 2
- 241001465754 Metazoa Species 0.000 description 2
- 230000037213 diet Effects 0.000 description 2
- 235000014113 dietary fatty acids Nutrition 0.000 description 2
- 201000010099 disease Diseases 0.000 description 2
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 2
- 229930195729 fatty acid Natural products 0.000 description 2
- 239000000194 fatty acid Substances 0.000 description 2
- 150000004665 fatty acids Chemical class 0.000 description 2
- 230000012010 growth Effects 0.000 description 2
- 210000004185 liver Anatomy 0.000 description 2
- 229920001542 oligosaccharide Polymers 0.000 description 2
- 150000002482 oligosaccharides Chemical class 0.000 description 2
- 210000002381 plasma Anatomy 0.000 description 2
- 239000001259 polydextrose Substances 0.000 description 2
- 235000013856 polydextrose Nutrition 0.000 description 2
- 229940035035 polydextrose Drugs 0.000 description 2
- MEIRRNXMZYDVDW-MQQKCMAXSA-N (2E,4E)-2,4-hexadien-1-ol Chemical compound C\C=C\C=C\CO MEIRRNXMZYDVDW-MQQKCMAXSA-N 0.000 description 1
- OWEGMIWEEQEYGQ-UHFFFAOYSA-N 100676-05-9 Natural products OC1C(O)C(O)C(CO)OC1OCC1C(O)C(O)C(O)C(OC2C(OC(O)C(O)C2O)CO)O1 OWEGMIWEEQEYGQ-UHFFFAOYSA-N 0.000 description 1
- 241000252983 Caecum Species 0.000 description 1
- 208000024172 Cardiovascular disease Diseases 0.000 description 1
- 239000004375 Dextrin Substances 0.000 description 1
- 229920001353 Dextrin Polymers 0.000 description 1
- GUBGYTABKSRVRQ-PICCSMPSSA-N Maltose Natural products O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@@H]1O[C@@H]1[C@@H](CO)OC(O)[C@H](O)[C@H]1O GUBGYTABKSRVRQ-PICCSMPSSA-N 0.000 description 1
- 206010067482 No adverse event Diseases 0.000 description 1
- 208000008589 Obesity Diseases 0.000 description 1
- 206010033307 Overweight Diseases 0.000 description 1
- 241000607142 Salmonella Species 0.000 description 1
- 229930006000 Sucrose Natural products 0.000 description 1
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 description 1
- LPQOADBMXVRBNX-UHFFFAOYSA-N ac1ldcw0 Chemical compound Cl.C1CN(C)CCN1C1=C(F)C=C2C(=O)C(C(O)=O)=CN3CCSC1=C32 LPQOADBMXVRBNX-UHFFFAOYSA-N 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 238000013019 agitation Methods 0.000 description 1
- 238000010171 animal model Methods 0.000 description 1
- 230000003712 anti-aging effect Effects 0.000 description 1
- 230000000259 anti-tumor effect Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000004071 biological effect Effects 0.000 description 1
- 230000001851 biosynthetic effect Effects 0.000 description 1
- 239000004067 bulking agent Substances 0.000 description 1
- 201000011510 cancer Diseases 0.000 description 1
- 239000003183 carcinogenic agent Substances 0.000 description 1
- 210000004534 cecum Anatomy 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 238000004939 coking Methods 0.000 description 1
- 210000004351 coronary vessel Anatomy 0.000 description 1
- 208000002925 dental caries Diseases 0.000 description 1
- 230000000378 dietary effect Effects 0.000 description 1
- 235000019621 digestibility Nutrition 0.000 description 1
- 230000029087 digestion Effects 0.000 description 1
- 230000001079 digestive effect Effects 0.000 description 1
- 150000002016 disaccharides Chemical class 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000009647 facial growth Effects 0.000 description 1
- 238000000855 fermentation Methods 0.000 description 1
- 230000004151 fermentation Effects 0.000 description 1
- 235000021191 food habits Nutrition 0.000 description 1
- 230000000855 fungicidal effect Effects 0.000 description 1
- 235000021552 granulated sugar Nutrition 0.000 description 1
- 208000006454 hepatitis Diseases 0.000 description 1
- 231100000283 hepatitis Toxicity 0.000 description 1
- 235000021192 high fiber diet Nutrition 0.000 description 1
- 230000036737 immune function Effects 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 210000002429 large intestine Anatomy 0.000 description 1
- 230000037356 lipid metabolism Effects 0.000 description 1
- 230000004132 lipogenesis Effects 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 201000007270 liver cancer Diseases 0.000 description 1
- 208000014018 liver neoplasm Diseases 0.000 description 1
- 206010025482 malaise Diseases 0.000 description 1
- 230000004060 metabolic process Effects 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 235000016709 nutrition Nutrition 0.000 description 1
- 230000035764 nutrition Effects 0.000 description 1
- 235000020824 obesity Nutrition 0.000 description 1
- 150000003904 phospholipids Chemical class 0.000 description 1
- 230000035479 physiological effects, processes and functions Effects 0.000 description 1
- 244000144977 poultry Species 0.000 description 1
- 230000001835 salubrious effect Effects 0.000 description 1
- 239000002689 soil Substances 0.000 description 1
- 210000002784 stomach Anatomy 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000005720 sucrose Substances 0.000 description 1
- 150000008163 sugars Chemical class 0.000 description 1
- 235000019605 sweet taste sensations Nutrition 0.000 description 1
- 231100000419 toxicity Toxicity 0.000 description 1
- 230000001988 toxicity Effects 0.000 description 1
- 235000013311 vegetables Nutrition 0.000 description 1
- 239000011782 vitamin Substances 0.000 description 1
- 229940088594 vitamin Drugs 0.000 description 1
- 229930003231 vitamin Natural products 0.000 description 1
- 235000013343 vitamin Nutrition 0.000 description 1
- 150000003722 vitamin derivatives Chemical class 0.000 description 1
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- Coloring Foods And Improving Nutritive Qualities (AREA)
Abstract
TThe invention discloses a simple technique for producing water-soluble polysaccharide. Such polysaccharide can be got from saccharide of 80-98 weight percent with the existence of aliphatic acid in the temperature of 120-260 Deg. C, and its average molecular weight is between 10000-30000. The method comprises the following steps: pre-treating, mixing and heating reaction with material; cooling, disintegrating, packing and warehouse-in with the reaction products. the polysaccharide produced in the invention caters for health demands of modern people, used as main material for health food with low calorie, low fat, low cholesterol and good taste.
Description
Technical field
The present invention relates to field of food, in particular, relate to a kind of water-soluble saccharan and production method thereof.
Background technology
Along with improving constantly of quality of life, people have been not only to satisfy to have enough to eat and wear to the requirement of food, and it more is healthy pursuing.At present, people have been well off, variation has taken place in people's food habits, diet formula is crossed essence, meticulous, and food processor is in order to guarantee the mouthfeel of food, tend in product to add a large amount of carbohydrates, make people's dietary structure trend high calorie, thereby cause the sickness rate of higher fatty acid, obesity, diabetes, cardiovascular diseases, constipation, malignant tumour etc. day by day to increase.Pursuing under the healthy agitation, when guaranteeing the food mouthfeel, production and edible low fat, low sugar, food low in calories, that contain the suitable quantity of water soluble dietary fiber become a kind of new trend.The demand of water-soluble dietary fibre constantly increases thereupon, and the production of water-soluble saccharan provides possibility for the production of heath food, and can constantly satisfy the demand of its growth.
Summary of the invention
The present invention replenishes as the useful of prior art, and simple water-soluble saccharan of a kind of technology and production method thereof are provided.
The water-soluble saccharan of the present invention, what reaction obtained under 120 ℃～260 ℃ conditions in the presence of the lipid acid, its molecular-weight average is between 10000～30000 by the carbohydrate of weight percent 80～98%.
Described carbohydrate is glucose or fructose.
Described lipid acid is citric acid or tartrate, and its weight percent is 0.1%～5%.
Also include 1%～20% Sorbitol Powder.
0.01%～1% the citric acid that includes also that form with sugar ester exists.
The water-soluble saccharan production method of the present invention comprises the steps: that pre-treatment, batch mixing, reacting by heating, the cooling of reaction product, pulverizing, the packing of raw material put in storage.Processing parameter: raw material stoving (80 ℃～105 ℃, 4 ~ 8 hours), by the proper ratio batch mixing, at 120 ℃～260 ℃, the pressure of 0 ~ 60mmHg post reaction down with the reaction product cooling, was pulverized, by promptly obtaining finished product behind the 40 order mesh screens after 1 ~ 32 hour.Can put in storage after packing with the weather-proof dressing thing then.
Water-soluble saccharan comprises poly-dextrose and levan, and it has following advantage as a kind of raw material for food:
Water-soluble dietary fibre is not had toxicity to human body, and can reduce the caloric value of food, food back blood sugar does not have the phenomenon of increasing, so can be used as the prescription of diabetic subject and the required special food of overweight person, to lower the picked-up of heat and carbohydrate, also can satisfy normal population to the high nutrition of food, requirement low in calories.
Water-soluble dietary fibre is the polycondensate of a class by the random bonding of monose or disaccharide, still in conjunction with a spot of sorbyl alcohol and citric acid, heat utilization ratio is 1kcal/g only in the molecule, is a kind of water solutable edible fiber low in calories, alternative granulated sugar and the sense of lipogenesis entity are difficult for causing carious tooth.Human Physiology is act as: increase excremental volume, shorten the path of passing through in the intestines, increase digestive function and remove constipation: reduce the danger of carcinogenic substance in absorption or the absorption food, the absorption that hinders or prolong glucose; In conjunction with or emit that mineral substance is sharp to produce voltaile fatty acid by fermentation, can stop the absorption of cholesterol; Simultaneously the effect of obvious reducing blood-fat is also arranged, thereby prevent the generation of painstaking effort disease.
Research report shows: high fiber diet can reduce total lipids matter, cholesterol and the triglyceride of laboratory animal; In diet, add water-soluble dietary fibre, the generation that can reduce inner cholesterol and delay coronary artery congee shape disease.
Many studies show that, water insoluble dietary fiber, its ability that reduces blood plasma lipide is very weak, even can not reduce blood matter, can promote the increase of cholesterol output in the ight soil.
Be presented in the result of study in the biosynthetic digestibility carbohydrate, poly-dextrose, general fiber, Nutriflora P and maltose etc. can reduce TL in the blood plasma, total cholesterol and triglyceride, and can increase the liver phospholipid and shorten digestion and pass through the time.Poly-dextrin and soy oligosaccharide can increase caecum weight, and soy oligosaccharide can reduce total cholesterol of liver and increase large intestine weight.
Water-soluble saccharan (food fibre), this type of saccharan are just catering to the demand of modern to health, the main raw material of the heath food of, lower fat low in calories for producing, low sugar, low-cholesterol, good mouthfeel.
Water-soluble saccharan is a class fine water-soluble dietary fibre, is again the low calorie bulking agents of a class uniqueness, and the metabolism of subparticipation human body is only arranged, and the heat that it produced has only 1kcal/g.When it serves as weighting agent and replaces other sugars in the food raw material or fat, the heat that is provided be respectively carbohydrate 25%, fat 11%.
Levan has the physiologic function of following excellence:
1. bifidus bacillus in the propagation human body suppresses the growth of interior Salmonellas of intestines and spoilage organism, promotes functions of intestines and stomach, anti-treating constipation, and increase the resultant quantity of VITAMIN, improve immune function of human body.Especially the elderly there is good anti-aging effects.
2. oligofructose is similar to water-soluble vegetable fibre, can blood fat reducing, improve lipid metabolism, reduce the content of cholesterol and triglyceride level in the blood.
3. low in calories, it seldom is converted into fat, is beneficial to fat-reducing.
4. levan has no adverse effects for tooth, and it is not utilized by caries bacteria.
5. levan is difficult for making blood sugar increasing, can supply diabetes patient.
6. use in the adding makeup, can suppress the growth of face and skin surface unwanted bacteria.
7. oligofructose has said function to domestic animal, poultry, is functional feedstuff additive, is called as plasmosin (PPE).
8. bifidus bacillus has anti-tumor activity.
9. discover that levan helps the rehabilitation of hepatitis, alleviate the state of an illness of liver cancer patient etc.;
Oligofructose is applied to have the following advantages in the foodstuffs industry:
1. fungicidal properties is better, and made food is convenient to preserve, and is difficult for mouldy souring.
2. water absorbability is lower, and it is rotten to reduce the food moisture absorption;
3. thermostability is higher, less coking variable color when being heated;
4. sweet taste is pure, and is salubrious than sucrose;
5. as oral liquid prepare burden, can improve the wherein biological activity of composition.
Embodiment
Below in conjunction with embodiment the present invention is described further.
Embodiment 1:
Get glucose 8000g, citric acid 10g, according to following step production: the cooling of the pre-treatment of raw material, batch mixing, reacting by heating, reaction product, pulverizing, packing warehouse-in.Concrete technology is: raw material stoving, under 80 ℃, dried 4 hours, with the above-mentioned raw materials batch mixing, at 120 ℃, the pressure of 20mmHg post reacts after 30 hours down, with the reaction product cooling, pulverize, by promptly obtaining finished product behind the 40 order mesh screens, the finished product molecular-weight average can be put in storage after packing with the weather-proof dressing thing then between 10000～30000.
Embodiment 2:
Get fructose 10000g, tartrate 50g, Sorbitol Powder 30g, according to following step production: the cooling of the pre-treatment of raw material, batch mixing, reacting by heating, reaction product, pulverizing, packing warehouse-in.Concrete technology is: raw material stoving, dried 8 hours down at 105 ℃, with the above-mentioned raw materials batch mixing, at 240 ℃, the pressure of 40mmHg post reaction down after 4 hours cools off reaction product, pulverize, by promptly obtaining finished product behind the 40 order mesh screens, the finished product molecular-weight average can be put in storage after packing with the weather-proof dressing thing then between 10000～30000.
Embodiment 3:
Get glucose 9000g, citric acid 30g, Sorbitol Powder 100g, according to following step production: the cooling of the pre-treatment of raw material, batch mixing, reacting by heating, reaction product, pulverizing, packing warehouse-in.Concrete technology is: raw material stoving, under 90 ℃, dried 20 hours, with the above-mentioned raw materials batch mixing, at 200 ℃, the pressure of 30mmHg post reacts after 15 hours down, with the reaction product cooling, pulverize, by promptly obtaining finished product behind the 40 order mesh screens, the finished product molecular-weight average can be put in storage after packing with the weather-proof dressing thing then between 10000～30000.
Embodiment 4:
Get fructose 10000g, tartrate 40g,, according to following step production: the cooling of the pre-treatment of raw material, batch mixing, reacting by heating, reaction product, pulverizing, packing warehouse-in.Concrete technology is: raw material stoving, dried 8 hours down at 95 ℃, with the above-mentioned raw materials batch mixing, at 200 ℃, the pressure of 40mmHg post reaction down after 16 hours cools off reaction product, pulverize, by promptly obtaining finished product behind the 40 order mesh screens, the finished product molecular-weight average can be put in storage after packing with the weather-proof dressing thing then between 10000～30000.
Claims (6)
1. a water-soluble saccharan is characterized in that, what reaction obtained under 120 ℃～260 ℃ conditions in the presence of the lipid acid, its molecular-weight average is between 10000～30000 by the carbohydrate of weight percent 80～98%.
2. water-soluble saccharan according to claim 1 is characterized in that, described carbohydrate is glucose or fructose.
3. water-soluble saccharan according to claim 1 is characterized in that, described lipid acid is citric acid or tartrate, and its weight percent is 0.1%～5%.
4. water-soluble saccharan according to claim 1 is characterized in that, also includes 1%～20% Sorbitol Powder.
5. water-soluble saccharan according to claim 1 is characterized in that, 0.01%～1% the citric acid that includes also that form with sugar ester exists.
6. a water-soluble saccharan production method according to claim 1 is characterized in that, comprises the steps:
(1) pre-treatment of raw material: under 80 ℃～105 ℃ conditions, dried 4～8 hours,
(2) batch mixing: in the described ratio batch mixing of claim 1,
(3) reacting by heating: under 120 ℃～260 ℃, the pressure of 0～60mmHg post, the cooling of 1～32 hour afterreaction product of reaction,
(4) above-mentioned reactant is pulverized, is packed warehouse-in.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 200410019165 CN1690085A (en) | 2004-04-30 | 2004-04-30 | Water-soluble polysaccharide and its production process |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 200410019165 CN1690085A (en) | 2004-04-30 | 2004-04-30 | Water-soluble polysaccharide and its production process |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN1690085A true CN1690085A (en) | 2005-11-02 |
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| CN 200410019165 Pending CN1690085A (en) | 2004-04-30 | 2004-04-30 | Water-soluble polysaccharide and its production process |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102439048A (en) * | 2009-05-07 | 2012-05-02 | 泰莱配料法国有限公司 | Compositions and methods for making alpha-(1,2)-branched alpha-(1,6) oligodextrans |
-
2004
- 2004-04-30 CN CN 200410019165 patent/CN1690085A/en active Pending
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102439048A (en) * | 2009-05-07 | 2012-05-02 | 泰莱配料法国有限公司 | Compositions and methods for making alpha-(1,2)-branched alpha-(1,6) oligodextrans |
| US8816067B2 (en) | 2009-05-07 | 2014-08-26 | Tate & Lyle Ingredients France SAS | Compositions and methods for making alpha-(1,2)-branched alpha-(1,6) oligodextrans |
| US9512239B2 (en) | 2009-05-07 | 2016-12-06 | Tate & Lyle Ingredients France SAS | Compositions and methods for making alpha-(1,2)-branched alpha-(1,6) oligodextrans |
| US10167346B2 (en) | 2009-05-07 | 2019-01-01 | Tate & Lyle Ingredients France SAS | Compositions and methods for making alpha-(1,2)-branched alpha-(1,6) oligodextrans |
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