CN1245111C - Health product extracting from hard clam and sea weeds, and its preparation method - Google Patents
Health product extracting from hard clam and sea weeds, and its preparation method Download PDFInfo
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Abstract
本发明涉及一种由文蛤和海带提取的保健品及其制备方法。其特征在于以文蛤和海带为原料，通过原料预处理、冷提取、热提取、浓缩等工艺过程，得到一种能显著增强机体抗病能力的保健品。本发明保健品为纯天然生物提取物制品，安全无毒，效果明显，每天服用适量，可达到预防感冒、增强抗病能力之功效，坚持服用，有助于增强体质、改善健康状况的作用。The invention relates to a health product extracted from clams and kelp and a preparation method thereof. It is characterized in that clams and kelp are used as raw materials, and a health product that can significantly enhance the body's disease resistance is obtained through raw material pretreatment, cold extraction, hot extraction, concentration and other processes. The health care product of the present invention is a pure natural biological extract product, which is safe, non-toxic, and has obvious effects. Taking an appropriate amount every day can prevent colds and enhance disease resistance. If you take it consistently, it can help strengthen your body and improve your health.
Description
技术领域technical field
本发明涉及一种由文蛤和海带提取的保健品及其制备方法。The invention relates to a health product extracted from clams and kelp and a preparation method thereof.
背景技术Background technique
文蛤(Meretrix meretrix)是一种海鲜珍品，含有蛋白质10％，脂肪1.2％，碳水化合物2.5％，还有人体易吸收的各种氨基酸和维生素及钙、钾、镁、磷、铁等多种人体必需的矿物质。其味道鲜美、营养价值高，而且有很高的食疗药用价值：有清热利湿、化痰、散结的功效，对肝癌有明显的抑制作用，对哮喘、慢性气管炎、肾虚、糖尿病等也有明显疗效。Meretrix meretrix is a seafood treasure, containing 10% protein, 1.2% fat, 2.5% carbohydrates, and various amino acids and vitamins that are easily absorbed by the human body, as well as calcium, potassium, magnesium, phosphorus, iron, etc. essential minerals. It tastes delicious, has high nutritional value, and has high dietary and medicinal value: it has the effects of clearing away heat and dampness, reducing phlegm, and dispelling stagnation, and has obvious inhibitory effect on liver cancer. Also has obvious curative effect.
海带(Laminaria japonica)国内外广泛食用，每百克海带含多糖32％、粗蛋白质8.2克，维生素A、B1、B2、B12、C、D、尼克酸、胡萝卜素等。还有丰富的碘、钙、铁以及磷、铜、钾、钴、氟等矿物质。其性寒，味咸、苦，归肝、肾、胃经，为软坚散结、消痰利水之品。Kelp (Laminaria japonica) is widely eaten at home and abroad. Every 100 grams of kelp contains 32% polysaccharide, 8.2 grams of crude protein, vitamins A, B 1 , B 2 , B 12 , C, D, niacin, carotene, etc. It is also rich in iodine, calcium, iron, phosphorus, copper, potassium, cobalt, fluorine and other minerals. It is cold in nature, salty and bitter in taste, and returns to the liver, kidney, and stomach meridian.
发明内容Contents of the invention
本发明的目的在于开发出一种由文蛤和海带提取的能显著增强机体抗病能力的保健品及其制备方法。The purpose of the present invention is to develop a health product extracted from clams and kelp that can significantly enhance the body's disease resistance and a preparation method thereof.
本发明以文蛤和海带为原料，通过原料预处理、冷提取、热提取、浓缩等工艺过程，得到一种能显著增强机体抗病能力的保健品，从而实现了本发明的目的。The present invention uses clams and kelp as raw materials, and through processes such as raw material pretreatment, cold extraction, hot extraction, and concentration, obtains a health product that can significantly enhance the body's disease resistance, thereby achieving the purpose of the present invention.
本发明由文蛤和海带提取的保健品的技术特征在于组成中含有由下述制备方法得到的物质，所述的制备方法包括以下几个步骤：The technical feature of the health product extracted from clams and kelp of the present invention is that the composition contains substances obtained by the following preparation method, and the preparation method includes the following steps:
(1)a.原料文蛤去壳取肉，切碎；(1) a. The raw material clam is shelled to get the meat, and chopped;
b.按质量分数30％～40％的乙醇与上述文蛤肉(湿重)的质量比为5～8∶1的比例将二者混合，冷浸20～60天；B. the mass ratio of the ethanol of 30%～40% by mass fraction and above-mentioned meretrix meretrix meat (wet weight) is the ratio of 5～8: 1 that the two are mixed, and cold soaked for 20～60 days;
c.将上述提取液分离，取上清液；c. separating the above extract and taking the supernatant;
d.将上清液的乙醇回收后得A液；d. Recover the ethanol in the supernatant to obtain liquid A;
(2)a.原料海带洗净，切碎；(2) a. The raw material kelp is washed and chopped;
b.按质量分数20％～30％的乙醇与上述海带(湿重)的质量比为5～8∶1的比例将二者混合于40～50℃回流提取2～4小时；b. The mass ratio of ethanol and above-mentioned sea-tangle (wet weight) by mass fraction 20%～30% is 5～8: 1 ratio, the two are mixed in 40～50 ℃ of reflux extraction 2～4 hours;
c.将提取液分离，取上清液；c. Separate the extract and take the supernatant;
d.将上清液的乙醇回收后得B液；d. Obtain liquid B after recovering the ethanol in the supernatant;
(3)按A液与B液中可溶性固含物的质量比为3～1∶1的比例将二者混合，得混合清液，即本发明保健品。(3) The mass ratio of the soluble solids in liquid A and liquid B is mixed in a ratio of 3 to 1:1 to obtain a mixed clear liquid, which is the health care product of the present invention.
本发明保健品作为口服液时步骤(3)得到的混合清液最好加热至90～100℃保持10～20分钟，冷却后，分离除杂，再收集清液。When the health product of the present invention is used as an oral liquid, the mixed clear liquid obtained in step (3) is preferably heated to 90-100° C. for 10-20 minutes, and after cooling, the mixed clear liquid is separated and removed, and then the clear liquid is collected.
本发明中上述各步骤中所述的分离采用常规的方法，例如过滤、离心等；所述步骤(1)d所得的A液和(2)d所得的B液太稀时最好浓缩，以便使用和加工，浓缩的程度没有严格要求，根据需要有所不同，例如作为口服液可以浓缩至可溶性固含物含量为质量分数1％～5％，要制粒时按需要可以浓缩至含量为质量分数1％～85％等。In the present invention, the separation described in the above-mentioned steps adopts conventional methods, such as filtration, centrifugation, etc.; the A liquid obtained in the step (1) d and the B liquid obtained in (2) d are preferably concentrated when they are too thin, so that Use and processing, the degree of concentration is not strictly required, and it varies according to needs. For example, as an oral liquid, it can be concentrated to a soluble solid content of 1% to 5% by mass. When granulating, it can be concentrated to a content of mass fraction as needed. Score 1% to 85%, etc.
本发明保健品的组分中还可以含有一种或一种以上的辅料。所述的辅料是制药品和食品时通常加入的例如调味剂如阿斯巴甜、蔗糖等和填充剂如淀粉、糊精等。所述的辅料含量没有严格限制，根据工艺和需要可以不同。The components of the health care product of the present invention may also contain one or more than one auxiliary materials. The adjuvants are usually added in pharmaceuticals and foods, for example flavoring agents such as aspartame, sucrose, etc. and fillers such as starch, dextrin, etc. The content of the auxiliary materials is not strictly limited, and can be different according to the process and needs.
本发明由文蛤和海带提取的保健品的制备方法的技术特征在于包括上述(1)～(3)三个步骤；各步骤中最佳的实验条件同上。The technical feature of the preparation method of the health product extracted from clams and kelp of the present invention is that it includes the above three steps (1) to (3); the best experimental conditions in each step are the same as above.
本发明保健品的制备方法还可以在所述的步骤(3)得到的混合清液或除杂后的清液中加入一种或一种以上的辅料，例如可以加入调味剂如阿斯巴甜、蔗糖等，作为口服液，按常规方法装瓶、轧盖，灭菌；也可以在所述的混合清液中加入填充剂例如淀粉、糊精等，还可以加入调味剂例如阿斯巴甜等，按常规方法制成颗粒或其它剂型。所述的辅料加入量没有严格限制，根据工艺和需要可以不同。The preparation method of the health care product of the present invention can also add one or more adjuvants to the mixed clear liquid obtained in the step (3) or the clear liquid after removing impurities, for example, flavoring agents such as aspartame can be added , sucrose, etc., as an oral liquid, bottled, capped, and sterilized according to conventional methods; fillers such as starch, dextrin, etc. can also be added to the mixed clear liquid, and flavoring agents such as aspartame can also be added etc., made into granules or other dosage forms according to conventional methods. The addition amount of the auxiliary materials is not strictly limited, and can be different according to the process and needs.
本发明保健品原清液作为口服液每天服用一次，每次10～150mL(按固含物含量为质量分数1％～5％计)，作为其它剂型可根据在清液中加入的辅料量，折算出服用量。The original clear liquid of the health care product of the present invention is taken once a day as an oral liquid, each 10-150mL (according to the solid content is 1%-5% by mass fraction), as other dosage forms can be according to the amount of adjuvant added in the clear liquid, Calculate the dosage.
本发明保健品为纯天然生物提取物制品，安全无毒，效果明显，每天服用适量，可达到预防感冒、增强抗病能力之功效，坚持服用，有助于增强体质、改善健康状况的作用。The health care product of the present invention is a pure natural biological extract product, which is safe, non-toxic, and has obvious effects. Taking an appropriate amount every day can prevent colds and enhance disease resistance. If you take it consistently, it can help strengthen your body and improve your health.
具体实施方式Detailed ways
实施例1：Example 1:
将原料文蛤去壳后，取其肉10kg，切碎后，用乙醇含量为质量分数30％的食用乙醇50kg冷浸20天；将提取液离心，取上清液，置于真空浓缩器中加热回收乙醇，乙醇回收完全后再继续浓缩至可溶性固含物含量达3％，即得A液。将原料海带洗净，切成小块，取30kg，与乙醇含量为质量分数20％的食用乙醇150kg混合，加热至40℃回流提取3小时；将提取液离心，取上清液，置于真空浓缩器中加热回收乙醇，乙醇回收完全后再继续浓缩至可溶性固含物含量达质量分数2％，即得B液。取A液、B液各20kg混合，加热升温至100℃，保持15分钟；待冷却至40℃后，过滤除去细小杂质，将得到的清液，装入玻璃瓶中，轧盖，于110℃灭菌40分钟，即得成品。使用时每日一次，每次服30～50mL。After shelling the raw material clam, take 10kg of its meat, chop it, and cold-soak with 50kg of edible ethanol with an ethanol content of 30% for 20 days; centrifuge the extract, take the supernatant, and heat it in a vacuum concentrator Recover the ethanol, and then continue to concentrate until the soluble solid content reaches 3% after the ethanol is recovered completely, to obtain liquid A. Wash the raw material kelp, cut it into small pieces, take 30kg, mix it with 150kg of edible ethanol whose ethanol content is 20% by mass fraction, heat to 40°C and reflux for extraction for 3 hours; centrifuge the extract, take the supernatant, and put it in a vacuum Heat in the concentrator to recover ethanol, and then continue to concentrate until the content of soluble solids reaches 2% by mass fraction after the recovery of ethanol is complete, to obtain liquid B. Mix 20kg of liquid A and liquid B, heat up to 100°C, and keep for 15 minutes; after cooling to 40°C, filter to remove fine impurities, put the obtained clear liquid into a glass bottle, cap it, and store it at 110°C Sterilize for 40 minutes to get the finished product. When used once a day, take 30-50mL each time.
实施例2：Example 2:
将原料文蛤去壳后，取其肉10kg，切碎后，用乙醇含量为质量分数35％的食用乙醇50kg冷浸60天；将提取液离心，取上清液，置于真空浓缩器中加热回收乙醇，乙醇回收完全后即得A液(可溶性固含物含量为1％)。将原料海带洗净，切成小块，取30kg，与乙醇含量为质量分数30％的食用乙醇150kg混合，加热至50℃回流提取2小时；将提取液离心，取上清液，置于真空浓缩器中加热回收乙醇，乙醇回收完全后即得B液(可溶性固含物含量为1％)。取A液75kg、B液25kg混合，加热升温至95℃，保持10分钟；待冷却至40℃后，过滤除去细小杂质，得到的清液，加入质量分数0.05％的阿斯巴甜后装入玻璃瓶中，轧盖，于110(2灭菌40分钟，即得成品。使用时每日一次，每次服75～150mL。After shelling the raw material clam, take 10kg of its meat, chop it, and cold-soak with 50kg of edible ethanol whose ethanol content is 35% by mass fraction for 60 days; centrifuge the extract, take the supernatant, and heat it in a vacuum concentrator The ethanol is recovered, and after the recovery of the ethanol is completed, the A solution (the content of soluble solids is 1%) is obtained. Wash the raw kelp, cut it into small pieces, take 30kg, mix it with 150kg of edible ethanol whose ethanol content is 30% by mass fraction, heat to 50°C and reflux for extraction for 2 hours; centrifuge the extract, take the supernatant, and put it in a vacuum Ethanol is recovered by heating in the concentrator, and liquid B (with a soluble solid content of 1%) is obtained after the recovery of ethanol is complete. Mix 75kg of liquid A and 25kg of liquid B, heat up to 95°C, and keep for 10 minutes; after cooling to 40°C, filter to remove fine impurities, and add 0.05% aspartame to the obtained clear liquid Put it in a glass bottle, crimp the cap, and sterilize at 110 (2) for 40 minutes to obtain the finished product. When used once a day, take 75-150 mL each time.
实施例3：Example 3:
将原料文蛤去壳后，取其肉10kg，切碎后，用乙醇含量为质量分数40％的食用乙醇80kg冷浸40天；将提取液离心，取上清液，置于真空浓缩器中加热回收乙醇，乙醇回收完全后再继续浓缩至可溶性固含物含量达10％，即得A液。将原料海带洗净，切成小块，取30kg，与乙醇含量为质量分数25％的食用乙醇240kg混合，加热至45℃回流提取4小时；将提取液离心，取上清液，置于真空浓缩器中加热回收乙醇，乙醇回收完全后再继续浓缩至可溶性固含物含量达质量分数10％，即得B液。取A液、B液各20kg混合，加入0.02kg的阿斯巴甜调味剂和4kg的可溶性淀粉，烘干粉碎，制成颗粒，即得成品。服用量每日一次，每次1～2g。After shelling the raw material clam, take 10kg of its meat, chop it, and soak it with 80kg of edible ethanol whose ethanol content is 40% by mass fraction for 40 days; centrifuge the extract, take the supernatant, and heat it in a vacuum concentrator Recover the ethanol, and then continue to concentrate until the soluble solids content reaches 10% after the ethanol is recovered completely, to obtain liquid A. Wash the raw kelp, cut it into small pieces, take 30kg, mix it with 240kg of edible ethanol with an ethanol content of 25% by mass, heat it to 45°C and extract it under reflux for 4 hours; centrifuge the extract, take the supernatant, and put it in a vacuum Heat in the concentrator to recover ethanol, and then continue to concentrate until the content of soluble solids reaches 10% by mass fraction after the recovery of ethanol is complete, to obtain liquid B. Mix 20 kg of liquid A and liquid B, add 0.02 kg of aspartame flavoring agent and 4 kg of soluble starch, dry and pulverize, and make granules to obtain the finished product. Dosage once a day, 1-2g each time.
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