CN1029768C - Cured tobacco bud balm and using method thereof - Google Patents
Cured tobacco bud balm and using method thereof Download PDFInfo
- Publication number
- CN1029768C CN1029768C CN 93101941 CN93101941A CN1029768C CN 1029768 C CN1029768 C CN 1029768C CN 93101941 CN93101941 CN 93101941 CN 93101941 A CN93101941 A CN 93101941A CN 1029768 C CN1029768 C CN 1029768C
- Authority
- CN
- China
- Prior art keywords
- cigarette
- cured tobacco
- tobacco
- percent
- balm
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 235000002637 Nicotiana tabacum Nutrition 0.000 title claims abstract description 44
- 244000062730 Melissa officinalis Species 0.000 title claims abstract description 23
- 235000010654 Melissa officinalis Nutrition 0.000 title claims abstract description 23
- 239000000865 liniment Substances 0.000 title claims abstract description 23
- 238000000034 method Methods 0.000 title claims description 5
- 244000061176 Nicotiana tabacum Species 0.000 title 1
- 235000019504 cigarettes Nutrition 0.000 claims abstract description 56
- 241000208125 Nicotiana Species 0.000 claims abstract description 43
- 239000003205 fragrance Substances 0.000 claims abstract description 18
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims abstract description 12
- SNICXCGAKADSCV-JTQLQIEISA-N (-)-Nicotine Chemical compound CN1CCC[C@H]1C1=CC=CN=C1 SNICXCGAKADSCV-JTQLQIEISA-N 0.000 claims abstract description 8
- 239000006071 cream Substances 0.000 claims abstract description 8
- SNICXCGAKADSCV-UHFFFAOYSA-N nicotine Natural products CN1CCCC1C1=CC=CN=C1 SNICXCGAKADSCV-UHFFFAOYSA-N 0.000 claims abstract description 8
- 229960002715 nicotine Drugs 0.000 claims abstract description 8
- 229910052757 nitrogen Inorganic materials 0.000 claims abstract description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 5
- 229930013930 alkaloid Natural products 0.000 claims abstract description 4
- 150000003797 alkaloid derivatives Chemical class 0.000 claims abstract description 4
- 239000012153 distilled water Substances 0.000 claims abstract description 4
- 239000000203 mixture Substances 0.000 abstract description 7
- 239000000779 smoke Substances 0.000 abstract description 7
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 abstract description 4
- 239000000796 flavoring agent Substances 0.000 abstract description 3
- 235000019634 flavors Nutrition 0.000 abstract description 3
- 239000000126 substance Substances 0.000 abstract description 3
- 238000009472 formulation Methods 0.000 abstract description 2
- 235000007173 Abies balsamea Nutrition 0.000 abstract 2
- 239000004857 Balsam Substances 0.000 abstract 2
- 244000018716 Impatiens biflora Species 0.000 abstract 2
- 206010013911 Dysgeusia Diseases 0.000 abstract 1
- 241000196324 Embryophyta Species 0.000 abstract 1
- 238000012360 testing method Methods 0.000 description 10
- 238000000605 extraction Methods 0.000 description 5
- 239000007789 gas Substances 0.000 description 5
- 240000002853 Nelumbo nucifera Species 0.000 description 4
- 235000006508 Nelumbo nucifera Nutrition 0.000 description 4
- 235000006510 Nelumbo pentapetala Nutrition 0.000 description 4
- 239000000284 extract Substances 0.000 description 4
- 239000007788 liquid Substances 0.000 description 4
- 239000002932 luster Substances 0.000 description 4
- 239000000463 material Substances 0.000 description 4
- 238000011160 research Methods 0.000 description 4
- 239000003513 alkali Substances 0.000 description 3
- 239000012141 concentrate Substances 0.000 description 3
- 235000013599 spices Nutrition 0.000 description 3
- 238000004458 analytical method Methods 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 238000007689 inspection Methods 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 238000005259 measurement Methods 0.000 description 2
- 239000012452 mother liquor Substances 0.000 description 2
- 238000012856 packing Methods 0.000 description 2
- 241000282836 Camelus dromedarius Species 0.000 description 1
- 239000008896 Opium Substances 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 235000019506 cigar Nutrition 0.000 description 1
- 235000009508 confectionery Nutrition 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 230000002950 deficient Effects 0.000 description 1
- 201000010099 disease Diseases 0.000 description 1
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 1
- 230000008030 elimination Effects 0.000 description 1
- 238000003379 elimination reaction Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 244000037666 field crops Species 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 210000002189 macula lutea Anatomy 0.000 description 1
- QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 description 1
- 229910052753 mercury Inorganic materials 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 229960001027 opium Drugs 0.000 description 1
- 239000002304 perfume Substances 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
- 230000000638 stimulation Effects 0.000 description 1
- 238000012546 transfer Methods 0.000 description 1
Landscapes
- Manufacture Of Tobacco Products (AREA)
- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
Abstract
The cured tobacco bud balm is prepared by extracting cured tobacco buds, is a brownish red cream, has strong cured tobacco fragrance, is dissolved in distilled water, and contains 64 percent of alcohol soluble content, 36 percent of alcohol insoluble content, 1.2 to 1.5 percent of total plant alkaloid, 2.2 to 2.5 percent of total sugar and 4.2 to 4.5 percent of total nitrogen. The balsam can be used for perfuming cigarette, tobacco sheet and expanded cut stem, and can reduce the cost of leaf formulation, improve the fragrance and smoke flavor concentration of cigarette, reduce the woody smell of cut stem, improve the taste, and make the taste pure and mild, and the aftertaste clean and comfortable. The balsam has high effect on making up the low nicotine content and insufficient tobacco fragrance of tobacco leaves in China, and is an ideal flavoring substance.
Description
The invention belongs to balm and the using method class thereof from the flue-cured tobacco bud, extracted.
Cigarette market demands cigarette commodity have the attribute of " high fragrance, high concentration, high strength, low tar " both at home and abroad at present.And owing to low, the cigarette insufficient fragrance of nicotine content in China's raw tobacco, for the cigarette of producing this attribute has caused objective obstacle, this has not only influenced the domestic market of cigarette, also influences China's cigarette and squeezes into the international market.Be meeting the market requirement, remedy the raw tobacco defective, utilize material production cigarette, the reconstituted tobacoo of tobacco leaf itself, the perfuming material of expanded cut stem, thereby reform China cigarette composition is necessary.
Cigarette is to get the leaf material, presses the tobacco cultivation standard, must pinch and pluck bud.China's year plantation tobacco leaf can be plucked flue-cured tobacco dried flower flower bud every year more than 40,000 tons more than 2,000 ten thousand mu, and these buds were all thrown away in vain in the past, and this not only causes the wasting of resources, also causes tobacco diseases to propagate, and influences the land for growing field crops leaf tobacco production.
The objective of the invention is to develop a kind of flue-cured tobacco bud cream that from the flue-cured tobacco bud, extracts.Balm flue-cured tobacco fragrance is true to nature, is used for the perfuming of cigarette and reconstituted tobacoo, can increase cigarette flavor and smoke concentration, increases the physiological strength of cigarette, covers assorted gas, make jealous pure and mild, pleasant impression is totally comfortable, coordinate.
The objective of the invention is to realize in the following manner, flue-cured tobacco bud cream is extracted by the flue-cured tobacco bud, be the brownish red paste, has strong flue-cured tobacco cigarette fragrance, proportion (d25/25 ℃) 1.2-1.5, nicotine content 4-4.9% is dissolved in the distilled water, the molten amount 64% of alcohol, pure insoluble amount 36% contain total alkaloid 1.2-1.5%, total reducing sugar 2.2-2.5%, total nitrogen 4.2-4.5%.
The flue-cured tobacco bud is used for cigarette, reconstituted tobacoo, expanded cut stem perfuming, and the addition in reconstituted tobacoo is 0.8-1.4%, is excellent with 1-1.2%, and directly the addition in cigarette shreds is 0.3-1%, is excellent with 0.5-0.8%.
Balm of the present invention extracts from the flue-cured tobacco bud, its extraction process such as application for a patent for invention " extracting the technology of balm from tobacco bud " (application number 90107606.6, date of publication 910227) described technology: earlier bud is dried in the shade, screens impurity elimination, with 95% alcohol mixing, sealing preliminary treatment 5-7 days, pour in the extractor, the mother liquor that adds back operation generation carries out the extraction first time under the temperature in normal pressure.Under 1.8-2.7kg/cm2 pressure, 130-135 ℃, carry out the extraction second time again.Adding distil water carries out third and fourth time extraction under 95-100 ℃ again.First and second time collection liquid merges also and filters, and staticly settles, thermal release goes out Ca
++, Mg
++, again in vacuum concentration pot under negative pressure low temperature vacuum concentrate, take out and join perfume (or spice), quality inspection, packing and promptly get balm.The gas that produces when vacuum concentrates, liquid are through separating, liquid vacuum again concentrates, and gas pumps after cooling, with third and fourth time extract and staticly settle, the steam condensate after the thermal release filters, after staticly settling, clear liquid is made the mother liquor of first and second time extraction.
Balm of the present invention detects through Zhengzhou Tobacco Research Institute of CNTC, on average contains total reducing sugar 2.36%, total alkaloid 1.36%, total nitrogen 4.34%.
Detect through Institute of Analysis of Wuhan University and food inspection center, Hubei Province, its result is: be dissolved in the distilled water pure molten amount 64%, pure insoluble amount 36%, nicotine content 4%-4.9%.
Because of balm of the present invention is to extract from the flue-cured tobacco bud, spices extracts fully, and balm flue-cured tobacco fragrance is true to nature, can be used for reconstituted tobacoo cigarette and expanded cut stem perfuming.
The Changde Cigarette Factory scientific research institution has carried out adding the experimental formula of this balm in reconstituted tobacoo, first and second grades of Virginian-type cigarettes and first and second grades of blended type cigarettes, its experimental result is as follows:
1. to the influence of cigarette inherence, presentation quality:
In the first class Virginian-type cigarette, add 0.3%, 0.4%, 0.5%, 1% balm respectively, roll up by the machine cigarette, cure back the packing with YT13B, MK8/MA8, MK9-5/PATF3, unpack after seven days inspection, do not find that cigarette has propped up macula lutea, oil stain, the preproduction inherent quality is smoked panel test by national GB5606-5610-85 standard, its comparing result sees Table 1, table 2, table 3.
Table 1(measurement unit branch)
The assorted gas of test item color and luster fragrance stimulates pleasant impression to add up to
Testing result 14 37.75 14.25 9 17.5 92.5
Conclusion: in the first class Virginian-type cigarette, add this balm of 1%, it is strong and brisk in taste, stimulation reduces, pleasant impression is totally comfortable.To smoke panel test in the same old way 91 minutes.
Table 2(measurement unit branch)
The assorted gas of test item color and luster fragrance stimulates pleasant impression to add up to
Testing result 13.5 37.25 14.25 8.625 17.875 91.5
Conclusion: in the first class Virginian-type cigarette, add this balm of 1%, reduce in the prophyll assembly side 12% tobacco leaf service rating, only outside the dim spot, its fragrance, pleasant impression all are better than or equal prophyll assembly side cigarette gloss, reach first class cigarette standard a little, and cost reduces by 37%.To smoke panel test in the same old way 91 minutes.(table 3 is seen the literary composition back)
As seen from the table, add this balm after, the nicotine content of cigarette improves, tar content reduces, cigarette props up middle TPM, a mouthful number slightly reduces, resistance to suction equates, helps cigarette quality and improves.
2. the credit of cigarette branching is analysed and be the results are shown in Table 4.(table 4 is seen the literary composition back)
As seen from the table: after adding balm the main chemical compositions of cigarette cigarette itself is not had influence, chemical composition is coordinated, and only propping up at cigarette increases cigarette fragrance, strength, reduction tar when burning and sucking.
Jianshi cigar factory with in the flue-cured tobacco in first class Virginian-type cigarette " seedling man " and flat taste blended type cigarette " group camel " prescription two use instead in three, apply 0.7% flue-cured tobacco bud cream sample preparation then, contrast is smoked panel test through Zhengzhou tobacco scientific research institute, and strength increases, cigarette fragrance enrichment, coordination, cleaner.
Zhengzhou Tobacco Research Institute of CNTC adds the experiment of this balm amount in reconstituted tobacoo and pipe tobacco, its conclusion is: by smokeing panel test, identify, and more satisfactory with the 1.0-1.2% addition in reconstituted tobacoo, more satisfactory with 0.5-0.8% in pipe tobacco.Along with the increase of balm addition, inhaling flavor has improvement, the increase of cigarette fragrance, smoke concentration to increase, and strength slightly increases, improves color and luster, pleasant impression coordination, comfortable, clean, and combustibility improves.How Germany consults after tobacco spice company gives this balm opium factory of a few family of this state detect to smoke panel test, and thinks the novel tobacco aromatics using that cigarette is fabulous.
This flue-cured tobacco bud cream is water-soluble, has strong cigarette fragrance, be used for cigarette, reconstituted tobacoo, expanded cut stem perfuming, can change the tobacco leaf formulation service rating after the adding, reduce cost, improve the cigarette grade, improve smoke concentration, improve cigarette fragrance, improve jealous, alleviate the wooden breath of stem, stem and thin slice color and luster are significantly improved.China's nicotine content of tobacco leaves is low to remedying, the cigarette insufficient fragrance is fruitful for this balm, is desirable perfuming material.
Table 3
NO
Analysis result 123456
Analysis project
TPM (milligram /) 28.23 27.94 27.59 28.37 27.59 28.30
Moisture content (milligram /) 3.105 3.073 3.035 3.1207 3.035 3.113
Transfer alkali (milligram/prop up) 0.914 0.929 0.923 0.928 0.935 0.943
Tar (milligram /) 24.21 23.94 23.63 24.32 23.62 24.24
Mouth number (mouthful /) 9.5 9.2 9.0 9.5 9.4 9.6
Cigarette average weight (gram) 0.92 0.92 0.92 1.00 1.00 1.00
Cigarette Zhi Pingjun resistance to suction (millimetres of mercury) 60 ± 5 60 ± 5 60 ± 5 65 ± 5 65 ± 5 65 ± 5
Annotate: 1,4 is golden lotus cigarette in the table, and 2,3,5,6 for adding the golden lotus cigarette of this balm.
Table 4
NO total reducing sugar % total nicotine % total nitrogen % total alkali nitrogen % protein % total volatile alkaline % schmuck value candy alkali ratio
1 19.02 1.08 1.53 0.187 8.39 0.1210 2.27 17.61
2 19.15 1.10 1.47 0.190 8.00 0.1223 2.39 17.41
Annotate: 1 is golden lotus pipe tobacco contrast sample in the table, and 2 for adding the golden lotus cigarette sample of 0.5% balm.
Claims (3)
1, flue-cured tobacco bud cream is characterized in that being extracted by the flue-cured tobacco bud, is the brownish red paste, has strong flue-cured tobacco cigarette fragrance, and proportion (d25/25 ℃) 1.2-1.5 is dissolved in the distilled water, pure molten amount 64%, pure insoluble amount 36%; Contain total alkaloid 1.2-1.5%, total reducing sugar 2.2-2.5%, total nitrogen 4.2-4.5%, nicotine content 4-4.9%.
2, the using method of flue-cured tobacco bud cream is characterized in that can be used for cigarette, reconstituted tobacoo and expanded cut stem perfuming, and the addition in reconstituted tobacoo is 0.8-1.4%, and the addition in cigarette shreds is 0.3-1%.
3, using method according to claim 2 is characterized in that the addition of balm in reconstituted tobacoo is 1-1.2%, and the addition in cigarette shreds is 0.5-0.8%.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 93101941 CN1029768C (en) | 1993-02-18 | 1993-02-18 | Cured tobacco bud balm and using method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 93101941 CN1029768C (en) | 1993-02-18 | 1993-02-18 | Cured tobacco bud balm and using method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1077358A CN1077358A (en) | 1993-10-20 |
| CN1029768C true CN1029768C (en) | 1995-09-20 |
Family
ID=4983864
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 93101941 Expired - Fee Related CN1029768C (en) | 1993-02-18 | 1993-02-18 | Cured tobacco bud balm and using method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN1029768C (en) |
Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20100116281A1 (en) | 2008-11-07 | 2010-05-13 | Jerry Wayne Marshall | Tobacco products and processes |
| US8955523B2 (en) * | 2010-01-15 | 2015-02-17 | R.J. Reynolds Tobacco Company | Tobacco-derived components and materials |
| US20130014771A1 (en) | 2011-01-13 | 2013-01-17 | R. J. Reynolds Tobacco Company | Tobacco-derived components and materials |
| CN103190693B (en) * | 2013-04-19 | 2015-03-25 | 安徽中烟工业有限责任公司 | Extracting method for tobacco flower extract and application thereof |
| CN105212260A (en) * | 2014-05-26 | 2016-01-06 | 何氪 | A kind of reconstituted tobacoo and cigarette products |
-
1993
- 1993-02-18 CN CN 93101941 patent/CN1029768C/en not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| CN1077358A (en) | 1993-10-20 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN101768514B (en) | Alhagi sparsifolia extract and preparation method and application thereof | |
| CN105861563A (en) | Method for preparing lysimachia foenum-graecum herb composite perfume through synthesis technology and application thereof | |
| CN108384637A (en) | A kind of preparation method of aroma type maillard flavour and its application in cigarette | |
| CN102703217B (en) | Noni extract and application thereof | |
| CN1029768C (en) | Cured tobacco bud balm and using method thereof | |
| CN108142984A (en) | A kind of method for preparing tobacco leaf clout fragrance using the golden flower bacterium fermentation of tea source | |
| CN115537268B (en) | A mixed system Maillard reaction flavor based on multi-stage extraction and its batch stability control method | |
| CN101455442B (en) | Grape extractum and preparation method thereof and use thereof in cigarette performing | |
| CN1029386C (en) | Burley bud balm and using method thereof | |
| CN102920008A (en) | A kind of preparation method of shredded burley tobacco for cigarette | |
| CN113913244A (en) | A kind of preparation method of low-sugar high-flavor tobacco flavor and application of tobacco flavor | |
| CN115005493B (en) | Bean flavor characteristic extract, preparation method thereof and cigarette | |
| CN1025935C (en) | Method for producing burley tobacco extract | |
| CN104178519A (en) | Fragaria ananassa Duchesne fermented extract and preparation method and application thereof | |
| CN1860947A (en) | Supercritical carrot extractive juice, and its application in perfuming of cigarette | |
| CN113826942A (en) | Preparation method of sun-cured tobacco extract with sweet characteristic and processing method of sun-cured tobacco | |
| CN101342019B (en) | Petroleum ether extracted green tea extract and preparation method and application thereof | |
| CN1319477C (en) | Chinese medicine cigarette for reducing toxin | |
| CN115918954A (en) | Preparation method and application of tobacco root extract for cigarettes | |
| CN111334374A (en) | Preparation of loquat flower volatile oil and application of loquat flower volatile oil in cigarette flavoring | |
| CN104178523B (en) | Allium tuberosum fermented extract and preparation method and application thereof | |
| CN115386428B (en) | Multistage extraction-based Maillard reaction essence of drug-flavor mixed system | |
| CN102687903A (en) | Pomelo leaf extract and application thereof | |
| CN117179353B (en) | Preparation method of fenugreek flavor group series products | |
| CN111334437A (en) | Preparation method of fermented tree flower extract for cigarettes |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| AD01 | Patent right deemed abandoned | ||
| C20 | Patent right or utility model deemed to be abandoned or is abandoned | ||
| AD01 | Patent right deemed abandoned | ||
| C20 | Patent right or utility model deemed to be abandoned or is abandoned | ||
| C19 | Lapse of patent right due to non-payment of the annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |