CN102311887B - 一种含碘的抗菌洗涤剂 - Google Patents
一种含碘的抗菌洗涤剂 Download PDFInfo
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- 238000005406 washing Methods 0.000 title claims abstract description 19
- ZCYVEMRRCGMTRW-UHFFFAOYSA-N 7553-56-2 Chemical compound [I] ZCYVEMRRCGMTRW-UHFFFAOYSA-N 0.000 title claims abstract description 16
- 230000000844 anti-bacterial effect Effects 0.000 title claims abstract description 16
- 239000011630 iodine Substances 0.000 title claims abstract description 16
- 229910052740 iodine Inorganic materials 0.000 title claims abstract description 16
- 239000003795 chemical substances by application Substances 0.000 title abstract description 6
- -1 hand cleansers Substances 0.000 claims abstract description 21
- 239000003599 detergent Substances 0.000 claims abstract description 16
- 229940051841 polyoxyethylene ether Drugs 0.000 claims abstract description 7
- 229920000056 polyoxyethylene ether Polymers 0.000 claims abstract description 7
- 239000002270 dispersing agent Substances 0.000 claims abstract description 5
- 239000002994 raw material Substances 0.000 claims abstract description 3
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 claims description 10
- 125000000118 dimethyl group Chemical group [H]C([H])([H])* 0.000 claims description 10
- 239000000203 mixture Substances 0.000 claims description 9
- QUSNBJAOOMFDIB-UHFFFAOYSA-N monoethyl amine Natural products CCN QUSNBJAOOMFDIB-UHFFFAOYSA-N 0.000 claims description 9
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims description 6
- 239000000463 material Substances 0.000 claims description 5
- WAKDCENNLPKPHZ-UHFFFAOYSA-N dimethyl(propyl)-lambda3-chlorane Chemical compound C(CC)Cl(C)C WAKDCENNLPKPHZ-UHFFFAOYSA-N 0.000 claims description 4
- ILRSCQWREDREME-UHFFFAOYSA-N dodecanamide Chemical compound CCCCCCCCCCCC(N)=O ILRSCQWREDREME-UHFFFAOYSA-N 0.000 claims description 4
- HSEMFIZWXHQJAE-UHFFFAOYSA-N hexadecanamide Chemical compound CCCCCCCCCCCCCCCC(N)=O HSEMFIZWXHQJAE-UHFFFAOYSA-N 0.000 claims description 4
- 230000008719 thickening Effects 0.000 claims description 4
- 241000282326 Felis catus Species 0.000 claims description 3
- 239000003921 oil Substances 0.000 claims description 3
- SNRUBQQJIBEYMU-UHFFFAOYSA-N Dodecane Natural products CCCCCCCCCCCC SNRUBQQJIBEYMU-UHFFFAOYSA-N 0.000 claims description 2
- LFTQUMPQEIHWLA-UHFFFAOYSA-N [Cl+].C(CCCCCCCCCCCCCCC)[N+](CC1=CC=CC=C1)(C)C Chemical compound [Cl+].C(CCCCCCCCCCCCCCC)[N+](CC1=CC=CC=C1)(C)C LFTQUMPQEIHWLA-UHFFFAOYSA-N 0.000 claims description 2
- 125000000217 alkyl group Chemical group 0.000 claims description 2
- 150000001412 amines Chemical class 0.000 claims description 2
- 125000002704 decyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 claims description 2
- ICMYIQTVBRLNEE-UHFFFAOYSA-N decyl(dimethyl)azanium;chloride Chemical compound Cl.CCCCCCCCCCN(C)C ICMYIQTVBRLNEE-UHFFFAOYSA-N 0.000 claims description 2
- 125000003438 dodecyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 claims description 2
- LUAJORAYKAAWIF-UHFFFAOYSA-N dodecyl(dimethyl)-lambda3-chlorane Chemical compound C(CCCCCCCCCCC)Cl(C)C LUAJORAYKAAWIF-UHFFFAOYSA-N 0.000 claims description 2
- SYELZBGXAIXKHU-UHFFFAOYSA-N dodecyldimethylamine N-oxide Chemical compound CCCCCCCCCCCC[N+](C)(C)[O-] SYELZBGXAIXKHU-UHFFFAOYSA-N 0.000 claims description 2
- BXWNKGSJHAJOGX-UHFFFAOYSA-N hexadecan-1-ol Chemical group CCCCCCCCCCCCCCCCO BXWNKGSJHAJOGX-UHFFFAOYSA-N 0.000 claims description 2
- 229940116335 lauramide Drugs 0.000 claims description 2
- QEALYLRSRQDCRA-UHFFFAOYSA-N myristamide Chemical compound CCCCCCCCCCCCCC(N)=O QEALYLRSRQDCRA-UHFFFAOYSA-N 0.000 claims description 2
- 125000001421 myristyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 claims description 2
- UTTVXKGNTWZECK-UHFFFAOYSA-N n,n-dimethyloctadecan-1-amine oxide Chemical compound CCCCCCCCCCCCCCCCCC[N+](C)(C)[O-] UTTVXKGNTWZECK-UHFFFAOYSA-N 0.000 claims description 2
- LYRFLYHAGKPMFH-UHFFFAOYSA-N octadecanamide Chemical compound CCCCCCCCCCCCCCCCCC(N)=O LYRFLYHAGKPMFH-UHFFFAOYSA-N 0.000 claims description 2
- 125000002347 octyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 claims description 2
- 230000003647 oxidation Effects 0.000 claims description 2
- 238000007254 oxidation reaction Methods 0.000 claims description 2
- 125000004079 stearyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 claims description 2
- 239000003760 tallow Substances 0.000 claims description 2
- SZYJELPVAFJOGJ-UHFFFAOYSA-N trimethylamine hydrochloride Chemical compound Cl.CN(C)C SZYJELPVAFJOGJ-UHFFFAOYSA-N 0.000 claims description 2
- NLKNQRATVPKPDG-UHFFFAOYSA-M potassium iodide Chemical compound [K+].[I-] NLKNQRATVPKPDG-UHFFFAOYSA-M 0.000 abstract description 12
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 abstract description 8
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 abstract description 8
- 239000007788 liquid Substances 0.000 abstract description 7
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract description 5
- 229960000583 acetic acid Drugs 0.000 abstract description 4
- 229910000147 aluminium phosphate Inorganic materials 0.000 abstract description 4
- 238000002360 preparation method Methods 0.000 abstract description 4
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- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 description 8
- WKBOTKDWSSQWDR-UHFFFAOYSA-N Bromine atom Chemical compound [Br] WKBOTKDWSSQWDR-UHFFFAOYSA-N 0.000 description 8
- GDTBXPJZTBHREO-UHFFFAOYSA-N bromine Substances BrBr GDTBXPJZTBHREO-UHFFFAOYSA-N 0.000 description 8
- 229910052794 bromium Inorganic materials 0.000 description 8
- PNDPGZBMCMUPRI-UHFFFAOYSA-N iodine Chemical compound II PNDPGZBMCMUPRI-UHFFFAOYSA-N 0.000 description 4
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 3
- 229960004839 potassium iodide Drugs 0.000 description 3
- 235000007715 potassium iodide Nutrition 0.000 description 3
- 239000000047 product Substances 0.000 description 3
- HIXDQWDOVZUNNA-UHFFFAOYSA-N 2-(3,4-dimethoxyphenyl)-5-hydroxy-7-methoxychromen-4-one Chemical compound C=1C(OC)=CC(O)=C(C(C=2)=O)C=1OC=2C1=CC=C(OC)C(OC)=C1 HIXDQWDOVZUNNA-UHFFFAOYSA-N 0.000 description 2
- 230000000249 desinfective effect Effects 0.000 description 2
- 238000002156 mixing Methods 0.000 description 2
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- 230000001737 promoting effect Effects 0.000 description 2
- MEIRRNXMZYDVDW-MQQKCMAXSA-N (2E,4E)-2,4-hexadien-1-ol Chemical compound C\C=C\C=C\CO MEIRRNXMZYDVDW-MQQKCMAXSA-N 0.000 description 1
- 241000894006 Bacteria Species 0.000 description 1
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
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- 241000726221 Gemma Species 0.000 description 1
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 description 1
- 241001465754 Metazoa Species 0.000 description 1
- 241001597008 Nomeidae Species 0.000 description 1
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 1
- 235000019484 Rapeseed oil Nutrition 0.000 description 1
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 1
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 1
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 description 1
- 229930006000 Sucrose Natural products 0.000 description 1
- 241000700605 Viruses Species 0.000 description 1
- DPDMMXDBJGCCQC-UHFFFAOYSA-N [Na].[Cl] Chemical compound [Na].[Cl] DPDMMXDBJGCCQC-UHFFFAOYSA-N 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- 239000013543 active substance Substances 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- 239000004411 aluminium Substances 0.000 description 1
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- QDYLMAYUEZBUFO-UHFFFAOYSA-N cetalkonium chloride Chemical compound CCCCCCCCCCCCCCCC[N+](C)(C)CC1=CC=CC=C1 QDYLMAYUEZBUFO-UHFFFAOYSA-N 0.000 description 1
- 229910052801 chlorine Inorganic materials 0.000 description 1
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- Detergent Compositions (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
本发明公开了一种含碘的抗菌洗涤剂及其制备方法，该洗涤剂是用以下原料制得的：质量分数为95％的碘4.5％，质量分数为99％的碘化钾0.5％，两性表面活性剂6％～15％，1∶1.5H的尼钠尔4％质量分数为99％的脂肪醇聚氧乙烯醚不少于26％，阳离子表面活性剂1％～5％，TJQH螯合分散剂A-10.01％～0.1％，TJQH增稠剂S0.5％，质量分数为85％的磷酸0.1％，冰乙酸0.1％，余为去离子水或蒸馏水。本发明的含碘抗菌洗涤剂不但具有洗涤效果，而且具有杀菌作用，是较理想的洗衣液。制成的洗衣液既能洗涤，又能消毒。适用于超浓缩洗衣液、洗手液、洗发露、丝毛洗涤剂等不同品种。
Description
技术领域
本发明涉及洗涤剂，具体来说，涉及含碘的洗涤剂。
背景技术
众所周知，含碘洗涤剂具有消毒抗菌的作用。含碘抗菌剂由单质碘、碘化钾、磷酸或乙酸复配物、氯化钠、多种表面活性剂复配物等组成，具有安全、广谱、高效、除菌作用，可杀灭细菌繁殖体、芽孢、真菌、原虫和部分病毒。用于抗菌的洗涤剂中，表面活性剂采用植物源、动物源活性剂，主要成分为:椰子油或棕榈油或菜籽油、山梨醇、脂肪醇、蔗糖、葡萄糖、琥珀酸、柠檬酸衍生物等。抗菌洗涤剂是含碘的抗菌洗涤剂，与肌肤毛发的pH值（弱酸性）相等，不含对氯间二甲苯酚（PCMX）、苯类、烷基酚、荧光增白剂、香精、磷、铝、乙二醇醚等，也不像氯系强氧化剂的洗涤产品，洗涤漂白衣物后，易生成致癌物卤代甲烷等。
中国专利数据库中涉及含碘洗涤剂的专利仅有95102774.3号《消毒型洗涤剂及其制备方法》，该专利提供的该洗涤剂的配方为：脂肪醇聚氧乙烯醚硫酸钠、烷基苯磺酸盐、络合型非离子表面活性剂、稳定剂、羧甲基纤维素钠、乙二胺四乙酸钠、碘、碘化盐、其余量为水。其抗菌效果并未公开。因此，人们继续探索具有抗菌功能的洗涤剂。
发明内容
本发明的目的在于提供一种含碘的抗菌洗涤剂，以满足人们日常生活中对具有抗菌功能的洗涤剂的需要。
本发明的又一目的在于提供上述含碘抗菌洗涤剂的制备方法，使之得以工业化生产，满足市场需求。
发明人提供的含碘的抗菌洗涤剂是按照以下原料的质量配比制得的:
碘（含量95％） 4.5％
碘化钾（含量99％） 0.5％
两性表面活性剂 6％～15％
尼钠尔（1∶1.5H） 4％
脂肪醇聚氧乙烯醚（折合含量99％） 不少于26％
阳离子表面活性剂 1％～5％
TJQH螯合分散剂A-1 0.01％～0.1％
TJQH增稠剂S 0.5％
磷酸（折合85％） 0.1％
冰乙酸 0.1％
去离子水或蒸馏水 余量；
上述两性表面活性剂是十八烷基二甲基氧化胺、月桂基二甲基氧化胺、椰油烷基二甲基氧化胺、十四烷基二羟乙基氧化胺、十六烷基二羟乙基氧化胺、十二烷基二羟乙基氧化胺、十八烷基二羟乙基氧化胺、牛油基二甲基氧化胺中的一种或几种。
上述阳离子表面活性剂是十六醇聚氧乙烯醚基二甲基辛烷基氯化铵、十二醇聚氧乙烯醚基二甲基甲基氯化铵、辛基酚聚氧乙烯醚基二甲基癸烷基溴化铵、辛基酚聚氧乙烯醚基二甲基癸烷基氯化铵、十八烷基二甲基氯（或溴）化铵、十六烷基二甲基氯（或溴）化铵、十四烷基二甲基氯（或溴）化铵、十二烷基二甲基氯（或溴）化铵、癸烷基二甲基氯（或溴）化铵、辛烷基二甲基氯（或溴）化铵、十六酰胺丙基二甲基/十八酰胺丙基二甲基氯（或溴）化铵、十四酰胺丙基二甲基/十二酰胺丙基二甲基氯（或溴）化铵、中的一种或多种。
上述TJQH螯合分散剂A-1、TJQH增稠剂S是天津市轻化工业研究院生产的市售产品。
发明人提供的含碘的抗菌洗涤剂的制备，是常规的混合、搅拌、包装方法。
上述各步骤都可在常温下进行操作。
本发明的含碘抗菌洗涤剂不但具有洗涤效果，而且具有杀菌作用，是较理想的洗衣液。制成的洗衣液既能洗涤，又能消毒。适用于洗衣液、洗手液、洗发露、丝毛洗涤剂等不同品种。
具体实施方式
以下通过具体实施方式，进一步说明本发明的有益效果。
实施例：取碘（含量95%）4.5g，碘化钾（含量99％）0.5g，十二烷基二羟乙基氧化胺10g，尼钠尔（1∶1.5H）4g，脂肪醇聚氧乙烯醚（折合含量99％）28g，十六烷基二甲基溴化铵3g，TJQH螯合分散剂A-1 0.1g，TJQH增稠剂S 0.5g，磷酸（折合85％）0.1g，冰乙酸0.1g; 将按照配方称量的各物质在高剪切分散乳化机中充分分散混合，灌装包装即可。
Claims (1)
1.一种含碘的抗菌洗涤剂，其特征在于该洗涤剂是按照以下原料的质量配比制得的:
所述两性表面活性剂是十八烷基二甲基氧化胺、月桂基二甲基氧化胺、椰油烷基二甲基氧化胺、十四烷基二羟乙基氧化胺、十六烷基二羟乙基氧化胺、十二烷基二羟乙基氧化胺、十八烷基二羟乙基氧化胺、牛油基二甲基氧化胺中的一种或几种;
所述阳离子表面活性剂是十六醇聚氧乙烯醚基二甲基辛烷基氯化铵、十二醇聚氧乙烯醚基二甲基甲基氯化铵、辛基酚聚氧乙烯醚基二甲基癸烷基溴化铵、辛基酚聚氧乙烯醚基二甲基癸烷基氯化铵、十八烷基二甲基氯/溴化铵、十六烷基二甲基氯/溴化铵、十四烷基二甲基氯/溴化铵、十二烷基二甲基氯/溴化铵、癸烷基二甲基氯/溴化 铵、辛烷基二甲基氯/溴化铵、十六酰胺丙基二甲基/十八酰胺丙基二甲基氯/溴化铵、十四酰胺丙基二甲基/十二酰胺丙基二甲基氯/溴化铵中的一种或多种;
所述TJQH螯合分散剂A-1、TJQH增稠剂S是天津市轻化工业研究院生产的市售产品。
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| CN103006464A (zh) * | 2011-09-20 | 2013-04-03 | 天津博克尼科技发展有限公司 | 一种含碘的免水消毒洗手液 |
| CN103897826A (zh) * | 2012-12-26 | 2014-07-02 | 青岛锦涟鑫商贸有限公司 | 一种新型洗涤剂 |
| CN104430326A (zh) * | 2014-11-26 | 2015-03-25 | 金科 | 一种两性表面活性剂组合物的制备方法 |
| CN106135274A (zh) * | 2015-04-22 | 2016-11-23 | 苏州泰利三佳纳米科技有限公司 | 一种含碘的衣物皮肤除菌剂组成及其制备方法 |
| CN106190608A (zh) * | 2016-07-11 | 2016-12-07 | 武汉柏康科技股份有限公司 | 一种pgqa胶体泡沫清洁剂及其生产工艺 |
| CN114158567B (zh) * | 2021-11-25 | 2022-11-15 | 佛山市正典生物技术有限公司 | 包含含有羟基的多元醇醚的含碘消毒剂及其制备方法、用途 |
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