CN1011891B - 一种制备含有尿素和硫酸胺肥料颗粒及其类似颗粒的方法 - Google Patents
一种制备含有尿素和硫酸胺肥料颗粒及其类似颗粒的方法Info
- Publication number
- CN1011891B CN1011891B CN86106555A CN86106555A CN1011891B CN 1011891 B CN1011891 B CN 1011891B CN 86106555 A CN86106555 A CN 86106555A CN 86106555 A CN86106555 A CN 86106555A CN 1011891 B CN1011891 B CN 1011891B
- Authority
- CN
- China
- Prior art keywords
- urea
- weight
- ammonium sulfate
- solution
- ammonium sulphate
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 title claims abstract description 67
- 239000004202 carbamide Substances 0.000 title claims abstract description 67
- 239000008187 granular material Substances 0.000 title claims abstract description 15
- 239000003337 fertilizer Substances 0.000 title claims abstract description 12
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 title description 6
- 238000004519 manufacturing process Methods 0.000 title description 3
- 229910021653 sulphate ion Inorganic materials 0.000 title description 2
- BFNBIHQBYMNNAN-UHFFFAOYSA-N ammonium sulfate Chemical compound N.N.OS(O)(=O)=O BFNBIHQBYMNNAN-UHFFFAOYSA-N 0.000 claims abstract description 52
- 229910052921 ammonium sulfate Inorganic materials 0.000 claims abstract description 52
- 235000011130 ammonium sulphate Nutrition 0.000 claims abstract description 52
- 238000000034 method Methods 0.000 claims abstract description 20
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 5
- 239000000203 mixture Substances 0.000 claims abstract description 4
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims abstract 2
- 238000002425 crystallisation Methods 0.000 claims description 15
- 230000008025 crystallization Effects 0.000 claims description 15
- 239000012467 final product Substances 0.000 claims description 5
- -1 aluminum compound Chemical class 0.000 claims description 3
- AZDRQVAHHNSJOQ-UHFFFAOYSA-N alumane Chemical class [AlH3] AZDRQVAHHNSJOQ-UHFFFAOYSA-N 0.000 claims description 2
- 229910052782 aluminium Inorganic materials 0.000 claims description 2
- 239000012141 concentrate Substances 0.000 claims 2
- 239000001166 ammonium sulphate Substances 0.000 abstract description 16
- 238000005469 granulation Methods 0.000 abstract description 13
- 230000003179 granulation Effects 0.000 abstract description 13
- 239000013078 crystal Substances 0.000 abstract description 6
- 239000000654 additive Substances 0.000 abstract 2
- 230000000996 additive effect Effects 0.000 abstract 2
- 229910052717 sulfur Inorganic materials 0.000 description 22
- 239000002245 particle Substances 0.000 description 17
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 16
- 239000011593 sulfur Substances 0.000 description 14
- 229910052757 nitrogen Inorganic materials 0.000 description 9
- 239000000725 suspension Substances 0.000 description 7
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 6
- 239000000047 product Substances 0.000 description 6
- 239000002689 soil Substances 0.000 description 6
- 239000007787 solid Substances 0.000 description 5
- 239000000155 melt Substances 0.000 description 4
- 239000000843 powder Substances 0.000 description 4
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 description 3
- DIZPMCHEQGEION-UHFFFAOYSA-H aluminium sulfate (anhydrous) Chemical compound [Al+3].[Al+3].[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O DIZPMCHEQGEION-UHFFFAOYSA-H 0.000 description 3
- YYRMJZQKEFZXMX-UHFFFAOYSA-N calcium;phosphoric acid Chemical group [Ca+2].OP(O)(O)=O.OP(O)(O)=O YYRMJZQKEFZXMX-UHFFFAOYSA-N 0.000 description 3
- 239000000084 colloidal system Substances 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 239000012530 fluid Substances 0.000 description 3
- 239000002426 superphosphate Substances 0.000 description 3
- 238000012360 testing method Methods 0.000 description 3
- MNNHAPBLZZVQHP-UHFFFAOYSA-N diammonium hydrogen phosphate Chemical compound [NH4+].[NH4+].OP([O-])([O-])=O MNNHAPBLZZVQHP-UHFFFAOYSA-N 0.000 description 2
- 238000002474 experimental method Methods 0.000 description 2
- 230000004720 fertilization Effects 0.000 description 2
- 239000007789 gas Substances 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 239000008188 pellet Substances 0.000 description 2
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 description 1
- 239000004254 Ammonium phosphate Substances 0.000 description 1
- 239000005696 Diammonium phosphate Substances 0.000 description 1
- 238000009825 accumulation Methods 0.000 description 1
- LFVGISIMTYGQHF-UHFFFAOYSA-N ammonium dihydrogen phosphate Chemical compound [NH4+].OP(O)([O-])=O LFVGISIMTYGQHF-UHFFFAOYSA-N 0.000 description 1
- 229910000387 ammonium dihydrogen phosphate Inorganic materials 0.000 description 1
- 229910000148 ammonium phosphate Inorganic materials 0.000 description 1
- 235000019289 ammonium phosphates Nutrition 0.000 description 1
- AOBXGGAGUYYNQH-UHFFFAOYSA-N ammonium sulfate urea Chemical compound [NH4+].[NH4+].NC(N)=O.[O-]S([O-])(=O)=O AOBXGGAGUYYNQH-UHFFFAOYSA-N 0.000 description 1
- 238000003889 chemical engineering Methods 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 238000010924 continuous production Methods 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 230000002950 deficient Effects 0.000 description 1
- 230000001627 detrimental effect Effects 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 229910000388 diammonium phosphate Inorganic materials 0.000 description 1
- 235000019838 diammonium phosphate Nutrition 0.000 description 1
- 238000004090 dissolution Methods 0.000 description 1
- 239000010459 dolomite Substances 0.000 description 1
- 229910000514 dolomite Inorganic materials 0.000 description 1
- 239000000428 dust Substances 0.000 description 1
- 239000007970 homogeneous dispersion Substances 0.000 description 1
- 239000003112 inhibitor Substances 0.000 description 1
- 238000011835 investigation Methods 0.000 description 1
- 238000002386 leaching Methods 0.000 description 1
- VTHJTEIRLNZDEV-UHFFFAOYSA-L magnesium dihydroxide Chemical compound [OH-].[OH-].[Mg+2] VTHJTEIRLNZDEV-UHFFFAOYSA-L 0.000 description 1
- 239000000347 magnesium hydroxide Substances 0.000 description 1
- 229910001862 magnesium hydroxide Inorganic materials 0.000 description 1
- 239000000395 magnesium oxide Substances 0.000 description 1
- CPLXHLVBOLITMK-UHFFFAOYSA-N magnesium oxide Inorganic materials [Mg]=O CPLXHLVBOLITMK-UHFFFAOYSA-N 0.000 description 1
- 159000000003 magnesium salts Chemical class 0.000 description 1
- AXZKOIWUVFPNLO-UHFFFAOYSA-N magnesium;oxygen(2-) Chemical compound [O-2].[Mg+2] AXZKOIWUVFPNLO-UHFFFAOYSA-N 0.000 description 1
- 238000003801 milling Methods 0.000 description 1
- 235000019837 monoammonium phosphate Nutrition 0.000 description 1
- 239000006012 monoammonium phosphate Substances 0.000 description 1
- 239000000618 nitrogen fertilizer Substances 0.000 description 1
- 239000002686 phosphate fertilizer Substances 0.000 description 1
- 238000011165 process development Methods 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05C—NITROGENOUS FERTILISERS
- C05C9/00—Fertilisers containing urea or urea compounds
- C05C9/005—Post-treatment
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05C—NITROGENOUS FERTILISERS
- C05C3/00—Fertilisers containing other salts of ammonia or ammonia itself, e.g. gas liquor
- C05C3/005—Post-treatment
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Fertilizers (AREA)
- Detergent Compositions (AREA)
- Medicines Containing Antibodies Or Antigens For Use As Internal Diagnostic Agents (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| NL8502838A NL8502838A (nl) | 1985-10-17 | 1985-10-17 | Werkwijze ter vervaardiging van ureum en ammoniumsulfaat bevattende meststofkorrels. |
| NL8502838 | 1985-10-17 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN86106555A CN86106555A (zh) | 1987-04-15 |
| CN1011891B true CN1011891B (zh) | 1991-03-06 |
Family
ID=19846728
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN86106555A Expired CN1011891B (zh) | 1985-10-17 | 1986-10-16 | 一种制备含有尿素和硫酸胺肥料颗粒及其类似颗粒的方法 |
Country Status (21)
| Country | Link |
|---|---|
| US (1) | US4943308A (pt) |
| EP (1) | EP0223276B1 (pt) |
| JP (1) | JPH0784355B2 (pt) |
| CN (1) | CN1011891B (pt) |
| AT (1) | ATE54438T1 (pt) |
| AU (1) | AU590015B2 (pt) |
| BR (1) | BR8605068A (pt) |
| CA (1) | CA1281911C (pt) |
| DE (1) | DE3672569D1 (pt) |
| ES (1) | ES2016797B3 (pt) |
| FI (1) | FI88150C (pt) |
| GR (1) | GR3001016T3 (pt) |
| IE (1) | IE59436B1 (pt) |
| IN (1) | IN166616B (pt) |
| MX (1) | MX172709B (pt) |
| MY (1) | MY100026A (pt) |
| NL (1) | NL8502838A (pt) |
| NO (1) | NO168636C (pt) |
| NZ (1) | NZ217900A (pt) |
| SU (1) | SU1671162A3 (pt) |
| ZA (1) | ZA867665B (pt) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN100413812C (zh) * | 2004-08-23 | 2008-08-27 | 徐耀武 | 复合硫基大颗粒尿素生产工艺 |
Families Citing this family (28)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| NL8700913A (nl) * | 1987-04-16 | 1988-11-16 | Nl Stikstof | Werkwijze voor het vervaardigen van kunstmestgranules. |
| US4994100A (en) * | 1988-12-29 | 1991-02-19 | Freeport Mcmoran Resource Partners | Homogeneous granular nitrogen fertilizer |
| GB9014985D0 (en) * | 1990-07-06 | 1990-08-29 | Dyno Industrier As | Formaldehyde resin curing agents |
| US5330552A (en) * | 1993-07-08 | 1994-07-19 | Rizzo John M | Method for increasing crop yield |
| AUPM383594A0 (en) * | 1994-02-11 | 1994-03-10 | Incitec Ltd | Granular urea |
| US6299663B1 (en) | 1996-04-19 | 2001-10-09 | Airborne Industrial Minerals Inc. | Granulation method and apparatus therefor |
| DE69716695T2 (de) * | 1996-04-19 | 2003-07-03 | Airborne Industrial Minerals Inc., Calgary | Methode zur granulierung. |
| NZ331531A (en) * | 1997-09-04 | 2000-01-28 | Toyo Engineering Corp | method for granulation and granulator |
| US6293985B1 (en) | 1998-04-17 | 2001-09-25 | Airborne Industrial Minerals | Fertilizer granulation method |
| US6132484A (en) * | 1998-04-17 | 2000-10-17 | Airborne Industrial Minerals Inc. | Wet granulation method for generating fertilizer granules |
| US6454979B1 (en) | 1998-04-17 | 2002-09-24 | Airborne Industrial Minerals Inc. | Wet granulation method for generating granules |
| US6331193B1 (en) | 1998-04-17 | 2001-12-18 | Airborne Industrial Minerals Inc. | Wet granulation method generating sulfur granules |
| DE19826570C2 (de) | 1998-06-15 | 2002-10-31 | Piesteritz Stickstoff | Verfahren zur Herstellung von Harnstoff und Ammonsulfat enthaltenden Düngemittel-Granulaten |
| AU773866B2 (en) | 1999-05-05 | 2004-06-10 | Agronomic Growth Industries Ltd. | Compost granulation method |
| DE10001082B4 (de) | 2000-01-13 | 2004-11-18 | Skw Stickstoffwerke Piesteritz Gmbh | Verfahren zur Herstellung eines Ammoniumsulfat und Harnstoff enthaltenden Düngemittels |
| AU785075C (en) | 2000-07-03 | 2007-07-12 | Nft Industries, Llc | Controlled release agricultural products and processes for making same |
| JP4633954B2 (ja) * | 2001-04-03 | 2011-02-16 | パナソニック電工Ｓｕｎｘ株式会社 | 電子機器 |
| RU2219146C1 (ru) * | 2002-09-23 | 2003-12-20 | Серебряков Александр Иванович | Способ получения азотно-сульфатного удобрения и азотно-сульфатное удобрение |
| DE102004005907B4 (de) * | 2004-02-05 | 2006-01-05 | Uhde Gmbh | Anlage zur Herstellung von biuretarmem harnstoffhaltigem Düngemittelgranulat |
| NO326272B1 (no) * | 2004-07-01 | 2008-10-27 | Yara Int Asa | Fremgangsmate for produksjon av gjodningsmiddel som inneholder urea og ammoniumsulfat |
| EP2431346A1 (en) * | 2010-09-15 | 2012-03-21 | Uhde Fertilizer Technology B.V. | Method for producing urea fertilizer with low moisture absorption tendencies |
| US8617286B2 (en) | 2010-10-21 | 2013-12-31 | John M. Rizzo | Method for increasing crop yield |
| EP2489429A1 (en) | 2011-02-21 | 2012-08-22 | Urea Casale S.A. | Fluid bed granulation of urea and related apparatus |
| NO336052B1 (no) * | 2012-08-29 | 2015-04-27 | Yara Int Asa | Sikre blandinger av ammoniumnitrat (AN) med urea, eller av et AN-omfattende produkt med et urea-omfattende produkt |
| MX353366B (es) | 2013-08-23 | 2018-01-10 | Koch Agronomic Services Llc | Composiciones estabilizadoras de urea y nitrógeno. |
| EP3542899A1 (en) | 2018-03-20 | 2019-09-25 | Yara International ASA | Method and reactor for producing urea ammonium sulphate |
| DE102021108187A1 (de) | 2021-03-31 | 2022-10-06 | Skw Stickstoffwerke Piesteritz Gmbh | Granuliertes pH-neutrales Harnstoff-Ammoniumsulfat-Düngemittel mit Ureaseinhibitor |
| EP4347536A2 (en) * | 2021-08-11 | 2024-04-10 | INWATEC GmbH & Co. KG | Composition for granular urea-based fertilizer |
Family Cites Families (18)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US101803A (en) * | 1870-04-12 | Improvement in padlocks | ||
| GB810760A (en) * | 1956-08-03 | 1959-03-25 | Bergwerksgesellschaft Hibernia | A method for the preparation of a fertilizer containing urea and ammonium sulphate, with a high nitrogen content |
| DE1112091B (de) * | 1957-11-21 | 1961-08-03 | Inventa A G Fuer Forschung | Verfahren zur Herstellung von lagerbestaendigen, granulierten Mischduengemitteln ausHarnstoff und Ammoniumsulfat |
| CH364277A (de) * | 1962-05-24 | 1962-09-15 | Lonza Ag | Verfahren zur Herstellung von biuretarmen, magnesiumhaltigen Harnstoffprills |
| CH431576A (de) * | 1964-01-07 | 1967-03-15 | Inventa Ag | Verfahren zum Granulieren von stickstoffhaltigen Düngemitteln |
| US3785796A (en) * | 1972-01-27 | 1974-01-15 | Tennessee Valley Autority | Production of urea-ammonium sulfate |
| US4033747A (en) * | 1974-08-05 | 1977-07-05 | Union Oil Company Of California | Silvicultural fertilization |
| US3928015A (en) * | 1974-10-29 | 1975-12-23 | Tennessee Valley Authority | Manufacture of urea-ammonium sulate from sulfuric acid, ammonia, and urea |
| SU635080A1 (ru) * | 1976-01-15 | 1978-11-30 | Предприятие П/Я В-2609 | Способ получени граннулированного карбамида |
| IE46841B1 (en) * | 1977-06-09 | 1983-10-05 | Azote Sa Cie Neerlandaise | Improvements in or relating to urea granulation |
| GB1581761A (en) * | 1977-06-09 | 1980-12-17 | Azote Sa Cie Neerlandaise | Urea granulation |
| US4388101A (en) * | 1979-03-14 | 1983-06-14 | Occidental Chemical Agricultural Products, Inc. | Non-pressure nitrogen carrier fertilizer solutions and dispersions and process of manufacture |
| US4239522A (en) * | 1979-06-13 | 1980-12-16 | Phillips Petroleum Company | Fertilizer solutions containing sulfur and having low crystallization temperature |
| NL8002912A (nl) * | 1980-05-20 | 1981-12-16 | Azote Sa Cie Neerlandaise | Werkwijze voor het maken van ureumkorrels, alsmede aldus verkregen ureumkorrels bevattende kunstmestmengsels. |
| NL184769C (nl) * | 1981-07-03 | 1989-11-01 | Azote Sa Cie Neerlandaise | Werkwijze voor het vervaardigen van ureumkorrels. |
| NL8103210A (nl) * | 1981-07-03 | 1983-02-01 | Azote Sa Cie Neerlandaise | Werkwijze voor het maken van ureumkorrels. |
| DE3223139C2 (de) * | 1981-07-03 | 1985-02-07 | Compagnie Néerlandaise de l'Azote S.A., Bruxelles | Verfahren zur Herstellung von Harnstoff als Hauptbestandteil enthaltenden Düngemittelkörnern |
| UST101803I4 (en) | 1981-07-27 | 1982-05-04 | Jones Thomas M | Production of urea-ammonium sulfate suspension fertilizer |
-
1985
- 1985-10-17 NL NL8502838A patent/NL8502838A/nl not_active Application Discontinuation
-
1986
- 1986-10-07 IN IN728/CAL/86A patent/IN166616B/en unknown
- 1986-10-08 ZA ZA867665A patent/ZA867665B/xx unknown
- 1986-10-13 IE IE269786A patent/IE59436B1/en not_active IP Right Cessation
- 1986-10-13 FI FI864127A patent/FI88150C/fi active IP Right Grant
- 1986-10-13 NZ NZ217900A patent/NZ217900A/xx unknown
- 1986-10-14 CA CA000520373A patent/CA1281911C/en not_active Expired - Lifetime
- 1986-10-16 AT AT86201807T patent/ATE54438T1/de not_active IP Right Cessation
- 1986-10-16 AU AU64168/86A patent/AU590015B2/en not_active Ceased
- 1986-10-16 MX MX004056A patent/MX172709B/es unknown
- 1986-10-16 BR BR8605068A patent/BR8605068A/pt not_active IP Right Cessation
- 1986-10-16 JP JP61244292A patent/JPH0784355B2/ja not_active Expired - Fee Related
- 1986-10-16 ES ES86201807T patent/ES2016797B3/es not_active Expired - Lifetime
- 1986-10-16 SU SU864028383A patent/SU1671162A3/ru active
- 1986-10-16 EP EP86201807A patent/EP0223276B1/en not_active Expired - Lifetime
- 1986-10-16 DE DE8686201807T patent/DE3672569D1/de not_active Expired - Lifetime
- 1986-10-16 CN CN86106555A patent/CN1011891B/zh not_active Expired
- 1986-10-17 NO NO864144A patent/NO168636C/no unknown
- 1986-10-17 MY MYPI86000020A patent/MY100026A/en unknown
-
1988
- 1988-12-28 US US07/291,310 patent/US4943308A/en not_active Expired - Lifetime
-
1990
- 1990-07-12 GR GR90400397T patent/GR3001016T3/el unknown
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN100413812C (zh) * | 2004-08-23 | 2008-08-27 | 徐耀武 | 复合硫基大颗粒尿素生产工艺 |
Also Published As
| Publication number | Publication date |
|---|---|
| MY100026A (en) | 1989-04-20 |
| ATE54438T1 (de) | 1990-07-15 |
| DE3672569D1 (de) | 1990-08-16 |
| IE862697L (en) | 1987-04-17 |
| EP0223276B1 (en) | 1990-07-11 |
| BR8605068A (pt) | 1987-07-21 |
| CN86106555A (zh) | 1987-04-15 |
| MX172709B (es) | 1994-01-10 |
| FI88150B (fi) | 1992-12-31 |
| AU6416886A (en) | 1987-04-30 |
| ZA867665B (en) | 1987-05-27 |
| NZ217900A (en) | 1990-01-29 |
| GR3001016T3 (en) | 1991-12-30 |
| US4943308A (en) | 1990-07-24 |
| FI88150C (fi) | 1993-04-13 |
| IN166616B (pt) | 1990-06-16 |
| NL8502838A (nl) | 1987-05-18 |
| IE59436B1 (en) | 1994-02-23 |
| FI864127L (fi) | 1987-04-18 |
| JPH0784355B2 (ja) | 1995-09-13 |
| EP0223276A1 (en) | 1987-05-27 |
| NO864144L (no) | 1987-04-21 |
| ES2016797B3 (es) | 1990-12-01 |
| CA1281911C (en) | 1991-03-26 |
| JPS6291484A (ja) | 1987-04-25 |
| NO864144D0 (no) | 1986-10-17 |
| FI864127A0 (fi) | 1986-10-13 |
| AU590015B2 (en) | 1989-10-26 |
| NO168636B (no) | 1991-12-09 |
| NO168636C (no) | 1992-03-18 |
| SU1671162A3 (ru) | 1991-08-15 |
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Legal Events
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| C06 | Publication | ||
| PB01 | Publication | ||
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