CN1073201A - A kind of composition of color flame candle and manufacture method thereof - Google Patents
A kind of composition of color flame candle and manufacture method thereof Download PDFInfo
- Publication number
- CN1073201A CN1073201A CN 91111832 CN91111832A CN1073201A CN 1073201 A CN1073201 A CN 1073201A CN 91111832 CN91111832 CN 91111832 CN 91111832 A CN91111832 A CN 91111832A CN 1073201 A CN1073201 A CN 1073201A
- Authority
- CN
- China
- Prior art keywords
- composition
- manufacture method
- modifying agent
- color flame
- present
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 12
- 239000000203 mixture Substances 0.000 title claims abstract description 11
- 238000000034 method Methods 0.000 title abstract description 7
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 12
- 239000000446 fuel Substances 0.000 claims abstract description 9
- 239000012916 chromogenic reagent Substances 0.000 claims abstract description 6
- 150000003839 salts Chemical class 0.000 claims abstract description 5
- 230000001360 synchronised effect Effects 0.000 claims abstract description 5
- 150000002191 fatty alcohols Chemical class 0.000 claims abstract description 4
- 239000002184 metal Substances 0.000 claims abstract description 4
- 229910044991 metal oxide Inorganic materials 0.000 claims abstract description 4
- 150000004706 metal oxides Chemical class 0.000 claims abstract description 4
- 229910052751 metal Inorganic materials 0.000 claims abstract description 3
- HDDLVZWGOPWKFW-UHFFFAOYSA-N trimethyl 2-hydroxypropane-1,2,3-tricarboxylate Chemical compound COC(=O)CC(O)(C(=O)OC)CC(=O)OC HDDLVZWGOPWKFW-UHFFFAOYSA-N 0.000 claims description 14
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 claims 2
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims 2
- WHXSMMKQMYFTQS-UHFFFAOYSA-N Lithium Chemical compound [Li] WHXSMMKQMYFTQS-UHFFFAOYSA-N 0.000 claims 2
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 claims 2
- 150000001875 compounds Chemical class 0.000 claims 2
- 229910052802 copper Inorganic materials 0.000 claims 2
- 239000010949 copper Substances 0.000 claims 2
- 229910052744 lithium Inorganic materials 0.000 claims 2
- 229910052700 potassium Inorganic materials 0.000 claims 2
- 239000011591 potassium Substances 0.000 claims 2
- 229910052708 sodium Inorganic materials 0.000 claims 2
- 239000011734 sodium Substances 0.000 claims 2
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 claims 1
- 239000002253 acid Substances 0.000 claims 1
- 150000001408 amides Chemical class 0.000 claims 1
- 150000002148 esters Chemical class 0.000 claims 1
- 229910052738 indium Inorganic materials 0.000 claims 1
- APFVFJFRJDLVQX-UHFFFAOYSA-N indium atom Chemical compound [In] APFVFJFRJDLVQX-UHFFFAOYSA-N 0.000 claims 1
- 239000011777 magnesium Substances 0.000 claims 1
- 229910052749 magnesium Inorganic materials 0.000 claims 1
- TZMFJUDUGYTVRY-UHFFFAOYSA-N pentane-2,3-dione Chemical compound CCC(=O)C(C)=O TZMFJUDUGYTVRY-UHFFFAOYSA-N 0.000 claims 1
- 235000014113 dietary fatty acids Nutrition 0.000 abstract description 6
- 229930195729 fatty acid Natural products 0.000 abstract description 6
- 239000000194 fatty acid Substances 0.000 abstract description 6
- 150000004665 fatty acids Chemical class 0.000 abstract description 6
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 abstract description 4
- -1 organic acid ester Chemical class 0.000 abstract description 3
- 230000001932 seasonal effect Effects 0.000 abstract description 3
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 abstract description 2
- 229910052799 carbon Inorganic materials 0.000 abstract description 2
- 239000000567 combustion gas Substances 0.000 abstract description 2
- 150000004696 coordination complex Chemical class 0.000 abstract description 2
- 230000007812 deficiency Effects 0.000 abstract description 2
- TXKMVPPZCYKFAC-UHFFFAOYSA-N disulfur monoxide Inorganic materials O=S=S TXKMVPPZCYKFAC-UHFFFAOYSA-N 0.000 abstract description 2
- 229910052757 nitrogen Inorganic materials 0.000 abstract description 2
- 231100000252 nontoxic Toxicity 0.000 abstract description 2
- 230000003000 nontoxic effect Effects 0.000 abstract description 2
- XTQHKBHJIVJGKJ-UHFFFAOYSA-N sulfur monoxide Chemical compound S=O XTQHKBHJIVJGKJ-UHFFFAOYSA-N 0.000 abstract description 2
- 230000005183 environmental health Effects 0.000 abstract 1
- 235000021355 Stearic acid Nutrition 0.000 description 3
- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 description 3
- OQCDKBAXFALNLD-UHFFFAOYSA-N octadecanoic acid Natural products CCCCCCCC(C)CCCCCCCCC(O)=O OQCDKBAXFALNLD-UHFFFAOYSA-N 0.000 description 3
- 239000008117 stearic acid Substances 0.000 description 3
- JDRMYOQETPMYQX-UHFFFAOYSA-M 4-methoxy-4-oxobutanoate Chemical compound COC(=O)CCC([O-])=O JDRMYOQETPMYQX-UHFFFAOYSA-M 0.000 description 2
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 2
- 238000010521 absorption reaction Methods 0.000 description 2
- JDRMYOQETPMYQX-UHFFFAOYSA-N butanedioic acid monomethyl ester Natural products COC(=O)CCC(O)=O JDRMYOQETPMYQX-UHFFFAOYSA-N 0.000 description 2
- GLDOVTGHNKAZLK-UHFFFAOYSA-N octadecan-1-ol Chemical compound CCCCCCCCCCCCCCCCCCO GLDOVTGHNKAZLK-UHFFFAOYSA-N 0.000 description 2
- 239000002904 solvent Substances 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- FBPFZTCFMRRESA-FSIIMWSLSA-N D-Glucitol Natural products OC[C@H](O)[C@H](O)[C@@H](O)[C@H](O)CO FBPFZTCFMRRESA-FSIIMWSLSA-N 0.000 description 1
- JOYRKODLDBILNP-UHFFFAOYSA-N Ethyl urethane Chemical compound CCOC(N)=O JOYRKODLDBILNP-UHFFFAOYSA-N 0.000 description 1
- 235000009781 Myrtillocactus geometrizans Nutrition 0.000 description 1
- 240000009125 Myrtillocactus geometrizans Species 0.000 description 1
- 235000003140 Panax quinquefolius Nutrition 0.000 description 1
- 240000005373 Panax quinquefolius Species 0.000 description 1
- 244000171022 Peltophorum pterocarpum Species 0.000 description 1
- 229920003171 Poly (ethylene oxide) Polymers 0.000 description 1
- VMHLLURERBWHNL-UHFFFAOYSA-M Sodium acetate Chemical compound [Na+].CC([O-])=O VMHLLURERBWHNL-UHFFFAOYSA-M 0.000 description 1
- 239000012752 auxiliary agent Substances 0.000 description 1
- 238000010923 batch production Methods 0.000 description 1
- 229910021538 borax Inorganic materials 0.000 description 1
- 238000002485 combustion reaction Methods 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- UQGFMSUEHSUPRD-UHFFFAOYSA-N disodium;3,7-dioxido-2,4,6,8,9-pentaoxa-1,3,5,7-tetraborabicyclo[3.3.1]nonane Chemical compound [Na+].[Na+].O1B([O-])OB2OB([O-])OB1O2 UQGFMSUEHSUPRD-UHFFFAOYSA-N 0.000 description 1
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 description 1
- 229940046892 lead acetate Drugs 0.000 description 1
- XIXADJRWDQXREU-UHFFFAOYSA-M lithium acetate Chemical compound [Li+].CC([O-])=O XIXADJRWDQXREU-UHFFFAOYSA-M 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- GOQYKNQRPGWPLP-UHFFFAOYSA-N n-heptadecyl alcohol Natural products CCCCCCCCCCCCCCCCCO GOQYKNQRPGWPLP-UHFFFAOYSA-N 0.000 description 1
- 238000010992 reflux Methods 0.000 description 1
- 239000001632 sodium acetate Substances 0.000 description 1
- 235000017281 sodium acetate Nutrition 0.000 description 1
- 239000004328 sodium tetraborate Substances 0.000 description 1
- 235000010339 sodium tetraborate Nutrition 0.000 description 1
- 239000000600 sorbitol Substances 0.000 description 1
- 238000009423 ventilation Methods 0.000 description 1
Landscapes
- Fats And Perfumes (AREA)
Abstract
The present invention relates to the composition and the manufacture method thereof of candle, particularly relate to a kind of composition and manufacture method thereof of color flame candles.The present invention adopts the poly-basic organic acid ester to make main fuel; Higher fatty acid or high fatty alcohol are made the intensity modifying agent; High fatty acid amide is made releasing agent; Metal oxide or its salt are made the synchronous modifying agent of heart yearn; Metal or its organic salt, metal complex are made chromogenic reagent.The color flame candles of making is beautiful in colour.Softening temperature is higher than 60 ℃, easily lights, and the easy-weathering deliquescence is not nontoxic, and cost is lower, so production and selling is not subject to seasonal restrictions.And carbon in the combustion gas, nitrogen, sulfur oxide content are low, meet the environmental health requirement.So the present invention has overcome the deliquescent deficiency of low, the easy weathering of candle softening temperature in the prior art, can realize in medium and small enterprise.
Description
The present invention relates to the composition and the manufacture method thereof of candle, particularly relate to a kind of composition and manufacture method thereof of color flame candles.
General color flame candles is made up of main fuel, chromogenic reagent and other auxiliary agent, sends the flame of red, yellow, blue, green color when burning.But the color flame candles of Sheng Chaning all existed softening temperature low in the past, easy weathering deliquescence, and heart yearn is asynchronous, makes its production and selling all be subjected to certain restriction.As United States Patent (USP) 2,504,211, adopt sorbitol anhydride to do main fuel, although its softening temperature is higher, flammable poor performance, the moisture absorption easily.According to day disclosure special permission 61,181,899 reports, adopt monomethyl succinate to make main fuel, but the moisture absorption is serious, and the synthetic difficulty of monomethyl succinate is bigger.And for example the Germany patent 1,226, and 234 adopt polyoxyethylene glycol to make main fuel, and its flare is little, is difficult for lighting.Chinese patent 86105053 adopts urethanum to do main fuel, and its shortcoming is low, the easy weathering deliquescence of softening temperature, difficult point combustion etc.
Task of the present invention provides a kind of composition and manufacture method thereof of new type colorful flame candle.Make its performance be better than prior art, and cost is lower.The present invention adopts trimethyl citrate to do main fuel; Higher fatty acid or high fatty alcohol are made the intensity modifying agent; High fatty acid amide is made releasing agent; Metal and metal oxide or its salt are made the synchronous modifying agent of heart yearn; Metal or its organic salt, metal complex are made chromogenic reagent.Its concrete percentage composition is as follows:
Trimethyl citrate 60-90
Higher fatty acid 1-10
(perhaps high fatty alcohol)
High fatty acid amide 0-5
The synchronous modifying agent 0-5 of heart yearn
Chromogenic reagent 1-5
Oil-soluble colourant are an amount of
By above-mentioned percentage composition, in the container that has agitator, thermometer and reflux condensate device, add main fuel, intensity modifying agent and releasing agent earlier, be heated to 80 ℃-90 ℃, under constantly stirring, add chromogenic reagent, continue to stir 10-25 minute, transfer to required color with oil-soluble colourant then, castable is treated the fully cooling back demoulding, gets product.
Color flame candles made in accordance with the present invention, softening temperature is higher than 60 ℃, has good burning performance, and lights easily, and the easy-weathering deliquescence is not nontoxic, and cost is lower than prior art significantly.Because softening temperature is higher, is not subject to seasonal restrictions so produce, and the problem that has existed since the color flame candles production midium or long term is resolved.Carbon in the combustion gas, nitrogen, sulfur oxide content are lower, meet sanitary requirement.
One embodiment of the present of invention are:
1, blushed flame candle:
Trimethyl citrate 96%
Stearyl alcohol 2%
Lithium acetate 2%
Wax is red an amount of
2, green flame candle:
Trimethyl citrate 91%
Stearic acid 2%
Lead acetate 2%
Sodium tetraborate 5%
Solvent green is an amount of
3, blue flame candle:
Trimethyl citrate 93%
Stearic acid 2%
Ventilation breather 5%
Solvent blue is an amount of
4, yellow flame candle:
Trimethyl citrate 97%
Stearic acid 2%
Sodium acetate 1%
Oil Yellow is an amount of
Below only be an embodiment, in concrete batch process the in batches, can also adjust percentage composition.Because it is higher that the color flame candles made from the present invention has softening temperature, produce and be not subject to seasonal restrictions, be convenient to transportation and store; Easily light, advantage such as heart yearn is synchronous has overcome the deficiency of prior art, has possessed the condition of industrialized mass production, can realize in medium and small enterprise.
Claims (1)
- A kind of composition and making method of manufacturing color flame candles is characterized in that:A, main fuel are trimethyl citrate, and its consumption accounts for the 60-99% of total score;B, intensity modifying agent are C 10-C 30Lipid acid or Fatty Alcohol(C12-C14 and C12-C18), its consumption accounts for the 1-10% of total score;C, releasing agent are C 10-C 30Fatty amide, its consumption is the 0-5% of total score;D, the synchronous modifying agent of heart yearn are metal, metal oxide or its salt, and its consumption is the 0-5% of total score;E, chromogenic reagent are that the wire and the heart yearn of lithium, sodium, potassium, magnesium, copper, indium is compound, perhaps the complex compound of the methyl ethyl diketone of lithium, sodium, potassium, copper, acetylacetic ester.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 91111832 CN1030466C (en) | 1991-12-12 | 1991-12-12 | Composition of colour flame candle and its making method |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 91111832 CN1030466C (en) | 1991-12-12 | 1991-12-12 | Composition of colour flame candle and its making method |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1073201A true CN1073201A (en) | 1993-06-16 |
| CN1030466C CN1030466C (en) | 1995-12-06 |
Family
ID=4910892
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 91111832 Expired - Fee Related CN1030466C (en) | 1991-12-12 | 1991-12-12 | Composition of colour flame candle and its making method |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN1030466C (en) |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1047400C (en) * | 1995-09-07 | 1999-12-15 | 王明凤 | Prodn process of color-flame candle |
| EP1380638A1 (en) | 2002-07-12 | 2004-01-14 | Xin Lu | Colored flame candle and manufacture thereof |
| EP1752523A1 (en) | 2005-08-08 | 2007-02-14 | Jiande Jiaxuan Articles Co., Ltd. | Candle body composition for colored flame candles and use thereof |
| CN100455648C (en) * | 2006-05-10 | 2009-01-28 | 尧开梅 | Filling candle and process for preparing same |
| CN101451091B (en) * | 2007-12-04 | 2011-07-20 | 湖南株洲高新技术产业开发区五星科技发展有限公司 | Color-flame candle and its preparing process |
| WO2011110085A2 (en) | 2010-03-08 | 2011-09-15 | 建德市嘉轩工艺品有限公司 | Colored flame candle and manufacturing method thereof |
| CN102559397A (en) * | 2011-12-27 | 2012-07-11 | 中南大学 | Method for making color flame candle |
-
1991
- 1991-12-12 CN CN 91111832 patent/CN1030466C/en not_active Expired - Fee Related
Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1047400C (en) * | 1995-09-07 | 1999-12-15 | 王明凤 | Prodn process of color-flame candle |
| EP1380638A1 (en) | 2002-07-12 | 2004-01-14 | Xin Lu | Colored flame candle and manufacture thereof |
| US6712865B2 (en) | 2002-07-12 | 2004-03-30 | Xin Lu | Colored flame candle and manufacture thereof |
| EP1752523A1 (en) | 2005-08-08 | 2007-02-14 | Jiande Jiaxuan Articles Co., Ltd. | Candle body composition for colored flame candles and use thereof |
| CN100455648C (en) * | 2006-05-10 | 2009-01-28 | 尧开梅 | Filling candle and process for preparing same |
| CN101451091B (en) * | 2007-12-04 | 2011-07-20 | 湖南株洲高新技术产业开发区五星科技发展有限公司 | Color-flame candle and its preparing process |
| WO2011110085A2 (en) | 2010-03-08 | 2011-09-15 | 建德市嘉轩工艺品有限公司 | Colored flame candle and manufacturing method thereof |
| US9212337B2 (en) | 2010-03-08 | 2015-12-15 | Jiande Jiaxuan Articles Co., Ltd. | Colored flame candle and manufacture thereof |
| CN102559397A (en) * | 2011-12-27 | 2012-07-11 | 中南大学 | Method for making color flame candle |
Also Published As
| Publication number | Publication date |
|---|---|
| CN1030466C (en) | 1995-12-06 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| C19 | Lapse of patent right due to non-payment of the annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |