CN106876256A - SiC double flute UMOSFET devices and preparation method thereof - Google Patents
SiC double flute UMOSFET devices and preparation method thereof Download PDFInfo
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Abstract
本发明涉及一种SiC双槽UMOSFET器件的制备方法,其特征在于,包括:选取SiC衬底;在所述SiC衬底连续表面生长漂移层、外延层及源区层;对所述源区层、所述外延层及所述漂移层进行刻蚀形成栅槽;对所述栅槽进行离子注入形成栅介质保护区;对所述源区层、所述外延层及所述漂移层进行刻蚀形成源槽;对所述源槽进行离子注入形成源槽拐角保护区;在所述栅槽内生长栅介质层及栅极层以形成栅极;钝化处理并制备电极以形成所述SiC双槽UMOSFET器件。本发明通过在源极和漂移层及外延层的界面形成肖特基接触,在保证不引起体二极管的“通电劣化”问题的同时,减少了额外的肖特基二极管,提高了器件的可靠性并降低了器件设计的复杂性和成本。
The invention relates to a method for preparing a SiC double-slot UMOSFET device, which is characterized in that it comprises: selecting a SiC substrate; growing a drift layer, an epitaxial layer and a source layer on the continuous surface of the SiC substrate; 1. Etching the epitaxial layer and the drift layer to form a gate groove; performing ion implantation on the gate groove to form a gate dielectric protection area; etching the source region layer, the epitaxial layer and the drift layer Forming a source trench; performing ion implantation on the source trench to form a source trench corner protection area; growing a gate dielectric layer and a gate layer in the gate trench to form a gate; passivation treatment and preparing electrodes to form the SiC double slot UMOSFET devices. The present invention forms a Schottky contact at the interface between the source electrode and the drift layer and the epitaxial layer, while ensuring that the problem of "power-on degradation" of the body diode is not caused, additional Schottky diodes are reduced, and the reliability of the device is improved. And reduce the complexity and cost of device design.
Description
技术领域technical field
本发明涉及集成电路技术领域,特别涉及一种SiC双槽UMOSFET器件及其制备方法。The invention relates to the technical field of integrated circuits, in particular to a SiC double-slot UMOSFET device and a preparation method thereof.
背景技术Background technique
宽带隙半导体材料SiC具有较大的禁带宽度,较高的临界击穿电场,高热导率和高电子饱和漂移速度等优良物理和化学特性,适合制作高温、高压、大功率、抗辐照的半导体器件。在功率电子领域中,功率MOSFET已被广泛应用,它具有栅极驱动简单,开关时间短等特点。垂直结构的UMOSFET相对于横向结构的MOSFET,具有导通电阻小,元胞尺寸小的优点,具有广阔的应用前景。The wide bandgap semiconductor material SiC has excellent physical and chemical properties such as large bandgap width, high critical breakdown electric field, high thermal conductivity and high electron saturation drift velocity, and is suitable for making high temperature, high pressure, high power, radiation resistant Semiconductor device. In the field of power electronics, power MOSFET has been widely used, it has the characteristics of simple gate drive and short switching time. Compared with the horizontal structure MOSFET, the vertical structure UMOSFET has the advantages of small on-resistance and small cell size, and has broad application prospects.
但在UMOSFET中,槽栅拐角处的电场集中很容易导致该处氧化层被提前击穿,对于SiC材料来说这一现象更为严重。通过在栅槽的底部设计一层P+型掺杂区域即P+栅介质保护区,使槽底的尖峰电场从栅氧化层上转移到P+栅介质保护区与N-漂移层所构成的PN结上,进而缓解了栅氧电场带来的可靠性问题。并且双槽结构的UMOSFET,通过在源极刻槽,该区域深入N-漂移层的深度要大于栅氧在N-漂移层中的深度,利用这点,氧化层处的电场因为源槽的存在而转移到源槽拐角处,进一步改善器件的击穿特性。同时MOSFET在变流器中作为功率开关,当其体二极管作为续流通路持续流过正向电流时,会发生“通电劣化”现象,使导通电阻和二极管的正向导通压降增大,并引起可靠性问题。However, in UMOSFET, the electric field concentration at the corner of the trench gate can easily lead to premature breakdown of the oxide layer, and this phenomenon is more serious for SiC materials. By designing a layer of P+ doped region, namely P+ gate dielectric protection region, at the bottom of the gate groove, the peak electric field at the bottom of the groove is transferred from the gate oxide layer to the PN junction formed by the P+ gate dielectric protection region and the N-drift layer. , thereby alleviating the reliability problem caused by the gate oxide electric field. And for the UMOSFET with double-groove structure, by carving a groove on the source, the depth of this region into the N-drift layer is greater than the depth of the gate oxide in the N-drift layer. Using this, the electric field at the oxide layer is due to the existence of the source groove And transferred to the corner of the source trench, further improving the breakdown characteristics of the device. At the same time, the MOSFET is used as a power switch in the converter. When its body diode continues to flow forward current as a freewheeling path, the phenomenon of "power-on deterioration" will occur, which will increase the on-resistance and the forward conduction voltage drop of the diode. and cause reliability issues.
因此在实际的应用中,通常采用在器件源漏极两端并联一个开启电压小于体二极管的肖特基二极管的方法来提供续流通路。显然这种方法极大地增加了电路设计的复杂性和成本费用。Therefore, in practical applications, a Schottky diode whose turn-on voltage is lower than that of the body diode is usually connected in parallel across the source and drain of the device to provide a freewheeling path. Obviously, this method greatly increases the complexity and cost of circuit design.
发明内容Contents of the invention
因此,为解决现有技术存在的技术缺陷和不足,本发明提出一种SiC双槽UMOSFET器件的制备方法。Therefore, in order to solve the technical defects and deficiencies existing in the prior art, the present invention proposes a method for preparing a SiC double-slot UMOSFET device.
具体地,本发明一个实施例提出的一种SiC双槽UMOSFET器件的制备方法,包括:Specifically, a method for preparing a SiC double-slot UMOSFET device proposed by an embodiment of the present invention includes:
步骤1、选取SiC衬底;Step 1. Select the SiC substrate;
步骤2、在所述SiC衬底连续表面生长漂移层、外延层及源区层;Step 2, growing a drift layer, an epitaxial layer and a source region layer on the continuous surface of the SiC substrate;
步骤3、对所述源区层、所述外延层及所述漂移层进行刻蚀形成栅槽;Step 3, etching the source region layer, the epitaxial layer and the drift layer to form gate grooves;
步骤4、对所述栅槽进行离子注入形成栅介质保护区;Step 4, performing ion implantation on the gate groove to form a gate dielectric protection area;
步骤5、对所述源区层、所述外延层及所述漂移层进行刻蚀形成源槽;Step 5. Etching the source region layer, the epitaxial layer and the drift layer to form source trenches;
步骤6、对所述源槽进行离子注入形成源槽拐角保护区;Step 6, performing ion implantation on the source groove to form a corner protection area of the source groove;
步骤7、在所述栅槽内生长栅介质层及栅极层以形成栅极;Step 7, growing a gate dielectric layer and a gate layer in the gate groove to form a gate;
步骤8、钝化处理并制备电极以形成所述SiC双槽UMOSFET器件。Step 8, passivating and preparing electrodes to form the SiC double-slot UMOSFET device.
在本发明的一个实施例中,步骤2包括:In one embodiment of the invention, step 2 includes:
步骤21、利用外延生长工艺,在所述SiC衬底表面生长所述漂移层;Step 21, using an epitaxial growth process to grow the drift layer on the surface of the SiC substrate;
步骤22、利用外延生长工艺,在所述漂移层表面生长所述外延层;Step 22, using an epitaxial growth process to grow the epitaxial layer on the surface of the drift layer;
步骤23、利用外延生长工艺,在所述外延层表面外延生长所述源区层。Step 23 , epitaxially growing the source region layer on the surface of the epitaxial layer by using an epitaxial growth process.
在本发明的一个实施例中,步骤3包括:In one embodiment of the present invention, step 3 includes:
利用ICP刻蚀工艺,采用第一掩膜版,对所述源区层表面进行刻蚀,在所述源区层、所述外延层及所述漂移层中形成所述栅槽。The surface of the source region layer is etched by using the first mask plate by using an ICP etching process, and the gate groove is formed in the source region layer, the epitaxial layer and the drift layer.
在本发明的一个实施例中,步骤4包括:In one embodiment of the present invention, step 4 includes:
利用自对准注入工艺,采用第一掩膜版,对所述栅槽进行Al离子注入在所述漂移层内形成所述栅介质保护区。Using a self-aligned implantation process and using a first mask plate, Al ion implantation is performed on the gate groove to form the gate dielectric protection region in the drift layer.
在本发明的一个实施例中,步骤5包括:In one embodiment of the present invention, step 5 includes:
利用ICP刻蚀工艺,采用第二掩膜版,对所述源区层表面进行刻蚀,在所述源区层、所述外延层及所述漂移层中形成所述源槽。The surface of the source region layer is etched by using a second mask plate by using an ICP etching process, and the source groove is formed in the source region layer, the epitaxial layer and the drift layer.
在本发明的一个实施例中,步骤6包括:In one embodiment of the present invention, step 6 includes:
利用自对准注入工艺,采用第二掩膜版,对所述源槽进行Al离子注入在所述漂移层内形成所述源槽拐角保护区。Using a self-aligned implantation process and using a second mask plate, Al ion implantation is performed on the source trench to form a corner protection area of the source trench in the drift layer.
在本发明的一个实施例中,对所述源槽进行Al离子注入,包括:In one embodiment of the present invention, performing Al ion implantation on the source groove includes:
采用450keV的注入能量、7.97×1013cm-2的注入剂量,对所述源槽进行第一次Al离子注入;Using an implantation energy of 450keV and an implantation dose of 7.97×10 13 cm -2 , perform the first Al ion implantation on the source groove;
采用300keV的注入能量、4.69×1013cm-2的注入剂量,对所述源槽进行第二次Al离子注入;Using an implant energy of 300keV and an implant dose of 4.69×10 13 cm -2 , perform a second Al ion implantation on the source groove;
采用200keV的注入能量、3.27×1013cm-2的注入剂量,对所述源槽进行第三次Al离子注入;Using an implant energy of 200keV and an implant dose of 3.27×10 13 cm -2 , perform a third Al ion implantation on the source groove;
采用120keV的注入能量、2.97×1013cm-2的注入剂量,对所述源槽进行第四次Al离子注入。The fourth Al ion implantation was performed on the source trench by using an implantation energy of 120keV and an implantation dose of 2.97×10 13 cm −2 .
在本发明的一个实施例中,步骤7包括:In one embodiment of the present invention, step 7 includes:
利用干氧工艺,在所述栅槽内生长SiO2材料以形成所述栅介质层;Using a dry oxygen process, growing SiO2 material in the gate trench to form the gate dielectric layer;
利用HWLPCVD工艺,在所述栅槽内生长多晶Si材料以形成所述栅极层;growing a polycrystalline Si material in the gate groove by using a HWLPCVD process to form the gate layer;
在本发明的一个实施例中,步骤8包括:In one embodiment of the present invention, step 8 includes:
在包括所述栅极的衬底上表面生长钝化层;growing a passivation layer on the surface of the substrate including the gate;
利用刻蚀工艺,对所述栅极表面的所述钝化层进行刻蚀形成电极接触孔;Etching the passivation layer on the surface of the gate by an etching process to form an electrode contact hole;
利用电子束蒸发工艺,在所述源槽和所述电极接触孔内生长金属材料形成源电极和栅电极;Using an electron beam evaporation process, growing a metal material in the source groove and the electrode contact hole to form a source electrode and a gate electrode;
利用电子束蒸发工艺,在衬底下表面生长金属材料形成漏电极以最终形成所述SiC双槽UMOSFET器件。Using an electron beam evaporation process, a metal material is grown on the lower surface of the substrate to form a drain electrode to finally form the SiC double-groove UMOSFET device.
本发明另一个实施例提出的一种SiC双槽UMOSFET器件,由上述实施例提供的方法制备形成。A SiC double-slot UMOSFET device proposed in another embodiment of the present invention is prepared by the method provided in the above embodiment.
上述实施例,通过在源极和N-漂移层及外延层的界面形成肖特基接触,替代外接的肖特基二极管作为续流通路,在保证不引起体二极管的“通电劣化”问题的同时,减少了额外的肖特基二极管,提高了器件的可靠性并降低了器件设计的复杂性和成本。另外,本发明利用双槽UMSFET自带的双槽结构,通过离子自对准工艺,无需光刻,形成P+栅介质保护区和P+源槽拐角保护区,进一步地改善了器件的击穿特性,以较小的工艺代价实现了更好的器件性能。In the above embodiment, by forming a Schottky contact at the interface between the source electrode and the N-drift layer and the epitaxial layer, the external Schottky diode is replaced as a freewheeling path, while ensuring that the problem of "conduction degradation" of the body diode is not caused , reducing additional Schottky diodes, improving device reliability and reducing device design complexity and cost. In addition, the present invention uses the double-slot structure of the double-slot UMSFET to form a P+ gate dielectric protection area and a P+ source slot corner protection area through an ion self-alignment process without photolithography, which further improves the breakdown characteristics of the device. Better device performance is achieved with a smaller process cost.
通过以下参考附图的详细说明,本发明的其它方面和特征变得明显。但是应当知道,该附图仅仅为解释的目的设计,而不是作为本发明的范围的限定,这是因为其应当参考附加的权利要求。还应当知道,除非另外指出,不必要依比例绘制附图,它们仅仅力图概念地说明此处描述的结构和流程。Other aspects and features of the present invention will become apparent from the following detailed description with reference to the accompanying drawings. It should be understood, however, that the drawings are designed for purposes of illustration only and not as a limitation of the scope of the invention since reference should be made to the appended claims. It should also be understood that, unless otherwise indicated, the drawings are not necessarily drawn to scale and are merely intended to conceptually illustrate the structures and processes described herein.
附图说明Description of drawings
下面将结合附图,对本发明的具体实施方式进行详细的说明。The specific implementation manners of the present invention will be described in detail below in conjunction with the accompanying drawings.
图1为本发明实施例提供的一种SiC双槽UMOSFET器件的结构示意图;FIG. 1 is a schematic structural diagram of a SiC double-slot UMOSFET device provided by an embodiment of the present invention;
图2为本发明实施例提供的一种SiC双槽UMOSFET器件制备方法的示意图;2 is a schematic diagram of a method for preparing a SiC double-slot UMOSFET device provided by an embodiment of the present invention;
图3a-图3k为本发明实施例提供的一种SiC双槽UMOSFET器件的工艺示意图。3a-3k are process schematic diagrams of a SiC double-slot UMOSFET device provided by an embodiment of the present invention.
具体实施方式detailed description
为使本发明的上述目的、特征和优点能够更加明显易懂,下面结合附图对本发明的具体实施方式做详细的说明。In order to make the above objects, features and advantages of the present invention more comprehensible, specific implementations of the present invention will be described in detail below in conjunction with the accompanying drawings.
实施例一Embodiment one
请参见图1,图1为本发明实施例提供的一种SiC双槽UMOSFET器件的结构示意图。本发明SiC双槽UMOSFET器件包括漏极11、N+衬底1、N-漂移层2、P-外延层3、N+源区层4、源极10、P+源槽拐角保护区6、槽栅介质7、多晶硅8、P+栅介质保护区5、栅电极9。Please refer to FIG. 1 , which is a schematic structural diagram of a SiC double-slot UMOSFET device provided by an embodiment of the present invention. The SiC double-slot UMOSFET device of the present invention includes a drain 11, an N+ substrate 1, an N-drift layer 2, a P-epitaxy layer 3, an N+ source region layer 4, a source 10, a P+ source groove corner protection region 6, and a groove gate dielectric 7. Polysilicon 8, P+ gate dielectric protection area 5, gate electrode 9.
优选地,源槽的深度大于栅槽的深度,且源槽的宽度等于P+源槽拐角保护区6的宽度;栅槽的宽度等于P+栅介质保护区5的宽度,所述源极10与N-漂移层2和P-外延层3之间的界面为肖特基接触,其余为欧姆接触。Preferably, the depth of the source groove is greater than the depth of the gate groove, and the width of the source groove is equal to the width of the P+ source groove corner protection area 6; the width of the gate groove is equal to the width of the P+ gate dielectric protection area 5, and the source 10 and N - The interface between the drift layer 2 and the P-epitaxial layer 3 is a Schottky contact, the rest are ohmic contacts.
可选地,源槽深度为3μm,栅槽深度为2.5μm,通过感应耦合等离子体(inductivelycowpled plasmas,简称ICP)刻蚀形成。源槽和P+源槽拐角保护区6的宽度分别为1μm,栅槽和P+栅介质保护区5的宽度分别为1.5μm。Optionally, the depth of the source trench is 3 μm, and the depth of the gate trench is 2.5 μm, which are formed by inductively coupled plasma (ICP for short) etching. The widths of the source groove and the P+ source groove corner protection region 6 are 1 μm respectively, and the widths of the gate groove and the P+ gate dielectric protection region 5 are 1.5 μm respectively.
可选地,N+衬底1是厚度为200μm~500μm,氮离子掺杂浓度为5×1018cm-3~1×1020cm-3的N型SiC衬底1。N-漂移层2是厚度为10μm~20μm,氮离子掺杂浓度为1×1015cm-3~6×1015cm-3的N型SiC外延层。Optionally, the N+ substrate 1 is an N-type SiC substrate 1 with a thickness of 200 μm-500 μm and a nitrogen ion doping concentration of 5×10 18 cm −3 to 1×10 20 cm −3 . The N-drift layer 2 is an N-type SiC epitaxial layer with a thickness of 10 μm to 20 μm and a nitrogen ion doping concentration of 1×10 15 cm −3 to 6×10 15 cm −3 .
可选地,所述P+源槽拐角保护区6厚度为0.5μm,Al离子掺杂浓度为3×1018cm-3。P+栅介质保护区5厚度为0.5μm,Al离子掺杂浓度为3×1018cm-3。Optionally, the P+ source groove corner protection region 6 has a thickness of 0.5 μm, and an Al ion doping concentration of 3×10 18 cm −3 . The P+ gate dielectric protection region 5 has a thickness of 0.5 μm and an Al ion doping concentration of 3×10 18 cm −3 .
可选地,所述P-外延层3是厚度为1μm~1.5μm,Al离子掺杂浓度为1×1017cm-3的P型SiC外延层。N+源区层4是厚度为0.5μm,氮离子掺杂浓度为5×1018cm-3的N型SiC外延层。Optionally, the P- epitaxial layer 3 is a P-type SiC epitaxial layer with a thickness of 1 μm˜1.5 μm and an Al ion doping concentration of 1×10 17 cm −3 . The N+ source region layer 4 is an N-type SiC epitaxial layer with a thickness of 0.5 μm and a nitrogen ion doping concentration of 5×10 18 cm −3 .
可选地,所述槽栅介质7是厚度为100nm的二氧化硅,通过干氧工艺形成。多晶硅8为poly Si,其深度为2.4μm,宽度为1.3μm,通过淀积填充整个栅槽结构。淀积场氧化层或者Si3N4层作为钝化层,腐蚀钝化层开电极孔。栅电极9,漏极11和源极10及其肖特基接触通过电子束蒸发金属形成。Optionally, the trench gate dielectric 7 is silicon dioxide with a thickness of 100 nm, formed by a dry oxygen process. The polysilicon 8 is poly Si with a depth of 2.4 μm and a width of 1.3 μm, and is deposited to fill the entire gate groove structure. A field oxide layer or Si 3 N 4 layer is deposited as a passivation layer, and the passivation layer is etched to open electrode holes. The gate electrode 9, drain 11 and source 10 and their Schottky contacts are formed by electron beam evaporation of metals.
本发明实施例,本发明通过在源槽引入肖特基二极管,替代外接的肖特基二极管作为续流通路,在保证不引起体二极管的“通电劣化”问题的同时,减少了额外的肖特基二极管,提高了器件的可靠性并降低了器件设计的复杂性和成本。In the embodiment of the present invention, the present invention replaces the externally connected Schottky diode as a freewheeling path by introducing a Schottky diode into the source tank, reducing the additional Schottky diode while ensuring that the problem of "power-on degradation" of the body diode is not caused. The base diode improves the reliability of the device and reduces the complexity and cost of device design.
需要说明的是,本发明中涉及的栅极,是指包括栅介质层和栅材料层构成的整体结构,例如栅极为栅氧材料和多晶硅材料构成的整体结构。本发明涉及的栅电极,是指为了金属化互连而在本发明的栅极表面淀积的金属材料,同样类似表述例如源电极和漏电极。It should be noted that the gate involved in the present invention refers to an integral structure including a gate dielectric layer and a gate material layer, for example, the gate is an integral structure formed of gate oxide material and polysilicon material. The gate electrode in the present invention refers to the metal material deposited on the surface of the gate in the present invention for the purpose of metallizing interconnection, and similar expressions such as source electrode and drain electrode are also used.
实施例二Embodiment two
请参见图2,图2为本发明实施例提供的一种SiC双槽UMOSFET器件制备方法的示意图。该制备方法可以包括如下步骤:Please refer to FIG. 2 . FIG. 2 is a schematic diagram of a method for fabricating a SiC double-slot UMOSFET device provided by an embodiment of the present invention. The preparation method may comprise the steps of:
步骤1、选取SiC衬底;Step 1. Select the SiC substrate;
步骤2、在所述SiC衬底连续表面生长漂移层、外延层及源区层;Step 2, growing a drift layer, an epitaxial layer and a source region layer on the continuous surface of the SiC substrate;
步骤3、对所述源区层、所述外延层及所述漂移层进行刻蚀形成栅槽;Step 3, etching the source region layer, the epitaxial layer and the drift layer to form gate grooves;
步骤4、对所述栅槽进行离子注入形成栅介质保护区;Step 4, performing ion implantation on the gate groove to form a gate dielectric protection area;
步骤5、对所述源区层、所述外延层及所述漂移层进行刻蚀形成源槽;Step 5. Etching the source region layer, the epitaxial layer and the drift layer to form source trenches;
步骤6、对所述源槽进行离子注入形成源槽拐角保护区;Step 6, performing ion implantation on the source groove to form a corner protection area of the source groove;
步骤7、在所述栅槽内生长栅介质层及栅极层以形成栅极;Step 7, growing a gate dielectric layer and a gate layer in the gate groove to form a gate;
步骤8、钝化处理并制备电极以形成所述SiC双槽UMOSFET器件。Step 8, passivating and preparing electrodes to form the SiC double-slot UMOSFET device.
可选地,对于步骤2,可以包括:Optionally, for step 2, may include:
步骤21、利用外延生长工艺,在所述SiC衬底表面生长所述漂移层;Step 21, using an epitaxial growth process to grow the drift layer on the surface of the SiC substrate;
步骤22、利用外延生长工艺,在所述漂移层表面生长所述外延层;Step 22, using an epitaxial growth process to grow the epitaxial layer on the surface of the drift layer;
步骤23、利用外延生长工艺,在所述外延层表面外延生长所述源区层。Step 23 , epitaxially growing the source region layer on the surface of the epitaxial layer by using an epitaxial growth process.
具体地,对于步骤21,包括:Specifically, for step 21, including:
在N型SiC衬底上生长10μm~20μm氮离子掺杂的漂移层,掺杂浓度为1×1015cm-3~6×1015cm-3,外延温度为1600℃,压力为100mbar,反应气体是硅烷和丙烷,载运气体为纯氢气,杂质源为液态氮气;A drift layer doped with nitrogen ions of 10 μm to 20 μm is grown on an N-type SiC substrate, the doping concentration is 1×10 15 cm -3 to 6×10 15 cm -3 , the epitaxy temperature is 1600°C, the pressure is 100mbar, and the reaction The gas is silane and propane, the carrier gas is pure hydrogen, and the impurity source is liquid nitrogen;
具体地,对于步骤22,包括:Specifically, for step 22, including:
在氮离子掺杂的漂移层上生长1μm~1.5μmAl离子掺杂的外延层,掺杂浓度为1×1017cm-3~1×1018cm-3,外延温度为1600℃,压力为100mbar,反应气体是硅烷和丙烷,载运气体为纯氢气,杂质源为三基甲铝;A 1μm-1.5μm Al ion-doped epitaxial layer is grown on the nitrogen ion-doped drift layer, the doping concentration is 1×10 17 cm -3 ~1×10 18 cm -3 , the epitaxy temperature is 1600°C, and the pressure is 100mbar , the reaction gas is silane and propane, the carrier gas is pure hydrogen, and the impurity source is trimethylaluminum;
具体地,对于步骤23,包括:Specifically, for step 23, including:
在外延层上生长为0.5μm氮离子掺杂的源区层,掺杂浓度为5×1018cm-3,外延温度为1600℃,压力为100mbar,反应气体是硅烷和丙烷,载运气体为纯氢气,杂质源为液态氮气;A source region layer doped with 0.5 μm nitrogen ions is grown on the epitaxial layer, the doping concentration is 5×10 18 cm -3 , the epitaxial temperature is 1600°C, the pressure is 100 mbar, the reaction gas is silane and propane, and the carrier gas is pure Hydrogen, the impurity source is liquid nitrogen;
可选地,对于步骤3,可以包括:Optionally, for step 3, may include:
利用ICP刻蚀工艺,采用第一掩膜版,对所述源区层表面进行刻蚀,在所述源区层、所述外延层及所述漂移层中形成所述栅槽。The surface of the source region layer is etched by using the first mask plate by using an ICP etching process, and the gate groove is formed in the source region layer, the epitaxial layer and the drift layer.
具体地,对于步骤3,包括:Specifically, for step 3, include:
利用ICP工艺,刻蚀形成栅槽,宽度为1.5μm,深度为2.5μm,其中,ICP线圈功率850W,源功率100W,反应气体SF6和O2分别为48sccm和12sccm;Using the ICP process, etch to form a gate groove with a width of 1.5 μm and a depth of 2.5 μm, of which, the ICP coil power is 850W, the source power is 100W, and the reaction gas SF 6 and O 2 are 48 sccm and 12 sccm respectively;
可选地,对于步骤4,可以包括:Optionally, for step 4, may include:
利用自对准注入工艺,采用第一掩膜版,对所述栅槽进行Al离子注入在所述漂移层内形成所述栅介质保护区。Using a self-aligned implantation process and using a first mask plate, Al ion implantation is performed on the gate groove to form the gate dielectric protection region in the drift layer.
具体地,对于步骤4,包括:Specifically, for step 4, include:
利用栅槽的刻蚀掩膜在漂移层进行多次Al离子自对准注入,形成深度为0.5μm,浓度为3×1018cm-3的栅介质保护区,注入温度为650℃。Al ion self-aligned implantation was performed multiple times in the drift layer by using the etching mask of the gate trench to form a gate dielectric protection area with a depth of 0.5 μm and a concentration of 3×10 18 cm -3 , and the implantation temperature was 650°C.
可选地,对于步骤5,可以包括:Optionally, for step 5, may include:
利用ICP刻蚀工艺,采用第二掩膜版,对所述源区层表面进行刻蚀,在所述源区层、所述外延层及所述漂移层中形成所述源槽。The surface of the source region layer is etched by using a second mask plate by using an ICP etching process, and the source groove is formed in the source region layer, the epitaxial layer and the drift layer.
具体地,对于步骤5,包括:Specifically, for step 5, include:
利用ICP工艺刻蚀形成源槽,宽度为1μm,深度为3μm,ICP线圈功率850W,源功率100W,反应气体SF6和O2分别为48sccm和12sccm;The source groove is formed by etching by ICP process, the width is 1μm, the depth is 3μm, the ICP coil power is 850W, the source power is 100W, and the reaction gas SF6 and O2 are 48sccm and 12sccm respectively;
可选地,对于步骤6,可以包括:Optionally, for step 6, may include:
利用自对准注入工艺,采用第二掩膜版,对所述源槽进行Al离子注入在所述漂移层内形成所述源槽拐角保护区。Using a self-aligned implantation process and using a second mask plate, Al ion implantation is performed on the source trench to form a corner protection area of the source trench in the drift layer.
其中,对所述源槽进行Al离子注入,包括:Wherein, performing Al ion implantation on the source tank includes:
采用450keV的注入能量、7.97×1013cm-2的注入剂量,对所述栅槽进行第一次Al离子注入;Using implant energy of 450keV and implant dose of 7.97×10 13 cm -2 , perform the first Al ion implantation on the gate groove;
采用300keV的注入能量、4.69×1013cm-2的注入剂量,对所述栅槽进行第二次Al离子注入;Using an implant energy of 300keV and an implant dose of 4.69×10 13 cm -2 , perform a second Al ion implantation on the gate groove;
采用200keV的注入能量、3.27×1013cm-2的注入剂量,对所述栅槽进行第三次Al离子注入;Using an implant energy of 200keV and an implant dose of 3.27×10 13 cm -2 , perform Al ion implantation on the gate groove for the third time;
采用120keV的注入能量、2.97×1013cm-2的注入剂量,对所述栅槽进行第四次Al离子注入。A fourth Al ion implantation is performed on the gate trench by using an implantation energy of 120keV and an implantation dose of 2.97×10 13 cm −2 .
具体地,对于步骤6,包括:Specifically, for step 6, include:
利用源槽的刻蚀掩膜在漂移层进行多次Al离子自对准注入,形成深度为0.5μm,浓度为3×1018cm-3的源槽拐角保护区,注入温度为650℃;Using the etch mask of the source trench to carry out self-aligned implantation of Al ions multiple times in the drift layer to form a protection area at the corner of the source trench with a depth of 0.5 μm and a concentration of 3×10 18 cm -3 , and the implantation temperature is 650°C;
可选地,对于步骤7,可以包括:Optionally, for step 7, may include:
利用干氧工艺,在所述栅槽内生长SiO2材料以形成所述栅介质层;Using a dry oxygen process, growing SiO2 material in the gate trench to form the gate dielectric layer;
利用热壁低压化学汽相淀积(hot wall low pressure chemical vapourdeposition,简称HWLPCVD)工艺,在所述栅槽内生长多晶Si材料以形成所述栅极层;Using a hot wall low pressure chemical vapor deposition (hot wall low pressure chemical vapor deposition, HWLPCVD for short) process, growing polycrystalline Si material in the gate trench to form the gate layer;
具体地,步骤7包括:Specifically, step 7 includes:
采用干氧工艺在1150℃下制备SiO2栅介质层,厚度为100nm,然后在1050℃,NO氛围下进行退火,降低SiO2薄膜表面的粗糙度;Prepare the SiO 2 gate dielectric layer at 1150°C by dry oxygen process with a thickness of 100nm, and then anneal at 1050°C in NO atmosphere to reduce the roughness of the SiO 2 film surface;
采用HWLPCVD工艺生长poly Si填满栅槽,淀积温度为600~650℃,淀积压强为60~80Pa,反应气体为硅烷和磷化氢,载运气体为氦气;The HWLPCVD process is used to grow poly Si to fill the gate groove, the deposition temperature is 600-650°C, the deposition pressure is 60-80Pa, the reaction gas is silane and phosphine, and the carrier gas is helium;
可选地,对于步骤8,可以包括:Optionally, for step 8, may include:
在包括栅极的衬底上表面生长钝化层;growing a passivation layer on the surface of the substrate including the gate;
利用刻蚀工艺,对所述栅极表面的所述钝化层进行刻蚀形成电极接触孔;Etching the passivation layer on the surface of the gate by an etching process to form an electrode contact hole;
利用电子束蒸发工艺,在所述源槽和所述电极接触孔内生长金属材料形成源电极和栅电极9;Using an electron beam evaporation process, growing a metal material in the source groove and the electrode contact hole to form a source electrode and a gate electrode 9;
利用电子束蒸发工艺,在衬底下表面生长金属材料形成漏电极以最终形成所述SiC双槽UMOSFET器件。Using an electron beam evaporation process, a metal material is grown on the lower surface of the substrate to form a drain electrode to finally form the SiC double-groove UMOSFET device.
具体地,步骤8包括:Specifically, step 8 includes:
在器件表面淀积一层场氧或者Si3N4层,再开电极接触孔;Deposit a layer of field oxygen or Si 3 N 4 on the surface of the device, and then open electrode contact holes;
电子束蒸发Ti/Ni/Au,制备电极,最后在Ar气氛中快速退火3min,温度为1050℃。因为漂移层和外延层掺杂浓度较低,在源极与漂移层和外延层界面形成肖特基接触,其他界面形成欧姆接触。Ti/Ni/Au was evaporated by electron beam to prepare electrodes, and finally annealed rapidly in Ar atmosphere for 3min at a temperature of 1050°C. Because the doping concentration of the drift layer and the epitaxial layer is low, a Schottky contact is formed at the interface between the source electrode and the drift layer and the epitaxial layer, and ohmic contacts are formed at other interfaces.
本发明实施例,本发明通过在源槽引入肖特基二极管,替代外接的肖特基二极管作为续流通路,在保证不引起体二极管的“通电劣化”问题的同时,减少了额外的肖特基二极管,提高了器件的可靠性并降低了器件设计的复杂性和成本。另外,本发明实施例利用双槽UMSFET自带的双槽结构,通过离子自对准工艺,无需光刻,形成栅介质保护区和源槽拐角保护区,进一步地改善了器件的击穿特性,以较小的工艺代价实现了更好的器件性能。In the embodiment of the present invention, the present invention replaces the externally connected Schottky diode as a freewheeling path by introducing a Schottky diode into the source tank, reducing the additional Schottky diode while ensuring that the problem of "power-on degradation" of the body diode is not caused. The base diode improves the reliability of the device and reduces the complexity and cost of device design. In addition, the embodiment of the present invention utilizes the double-groove structure of the dual-groove UMSFET to form the gate dielectric protection area and the source groove corner protection area through the ion self-alignment process without photolithography, which further improves the breakdown characteristics of the device. Better device performance is achieved with a smaller process cost.
实施例二Embodiment two
请参见图3,图3为本实施例提供了另一种SiC双槽UMOSFET器件制备方法,该制备方法包括如下步骤:Please refer to FIG. 3. FIG. 3 provides another SiC double-slot UMOSFET device preparation method for this embodiment. The preparation method includes the following steps:
步骤a,在N型SiC衬底1上外延生长N-漂移层2,如图3a所示。In step a, an N-drift layer 2 is epitaxially grown on an N-type SiC substrate 1, as shown in FIG. 3a.
先对厚度为200μm,氮离子掺杂浓度为5×1018cm-3的N型SiC衬底进行RCA标准清洗,然后在整个SiC衬底1上外延生长厚度为10μm,氮离子掺杂浓度为1×1015cm-3的N-漂移层2。其工艺条件是:温度为1600℃,压力为100mbar,反应气体是硅烷和丙烷,载运气体为纯氢气,杂质源为液态氮气。RCA standard cleaning was performed on the N-type SiC substrate with a thickness of 200 μm and a nitrogen ion doping concentration of 5×10 18 cm -3 , and then epitaxial growth was performed on the entire SiC substrate 1 with a thickness of 10 μm and a nitrogen ion doping concentration of 1×10 15 cm −3 of N-drift layer 2. The process conditions are as follows: temperature is 1600°C, pressure is 100mbar, reaction gas is silane and propane, carrier gas is pure hydrogen, and impurity source is liquid nitrogen.
步骤b,外延生长P-外延层3,如图3b所示。Step b, epitaxially growing the P- epitaxial layer 3, as shown in FIG. 3b.
在N-漂移层2上生长一层厚度为1μm,Al离子掺杂浓度为1×1017cm-3的P-外延层3。其工艺条件是:温度为1600℃,压力为100mbar,反应气体是硅烷和丙烷,载运气体为纯氢气,杂质源为三基甲铝。A P-epitaxial layer 3 with a thickness of 1 μm and an Al ion doping concentration of 1×10 17 cm −3 is grown on the N-drift layer 2 . The process conditions are as follows: the temperature is 1600°C, the pressure is 100mbar, the reaction gas is silane and propane, the carrier gas is pure hydrogen, and the impurity source is trimethylaluminum.
步骤c,外延生长N+源区层4,如图3c所示。Step c, epitaxially growing the N+ source region layer 4, as shown in FIG. 3c.
在P-外延层3上生长一层厚度为0.5μm,氮离子掺杂浓度为5×1018cm-3的N+源区层4。其工艺条件是:温度为1600℃,压力为100mbar,反应气体是硅烷和丙烷,载运气体为纯氢气,杂质源为液态氮气。An N+ source region layer 4 with a thickness of 0.5 μm and a nitrogen ion doping concentration of 5×10 18 cm −3 is grown on the P − epitaxial layer 3 . The process conditions are as follows: temperature is 1600°C, pressure is 100mbar, reaction gas is silane and propane, carrier gas is pure hydrogen, and impurity source is liquid nitrogen.
步骤d,刻蚀形成栅槽,如图3d所示。In step d, gate grooves are formed by etching, as shown in FIG. 3d.
首先磁控溅射一层的Ti膜作为ICP刻蚀掩膜,然后涂胶光刻,进行ICP刻蚀,刻蚀出槽的宽度为1.5μm,深度为2.5μm,最后去胶,去刻蚀掩膜,清洗成光片。其工艺条件为:ICP线圈功率850W,源功率100W,反应气体SF6和O2分别为48sccm和12sccm。First magnetron sputtering a layer The Ti film is used as an ICP etching mask, and then coated with photolithography, and ICP etching is performed. The width of the etched groove is 1.5 μm, and the depth is 2.5 μm. Finally, the glue is removed, the etching mask is removed, and it is cleaned into a light sheet . The process conditions are: ICP coil power 850W, source power 100W, reaction gas SF6 and O2 are 48sccm and 12sccm respectively.
步骤e,利用栅槽的刻蚀掩膜在N-漂移层2进行多次Al离子自对准注入,如图3e所示。In step e, self-aligned implantation of Al ions is performed multiple times in the N-drift layer 2 by using the etching mask of the gate groove, as shown in FIG. 3e.
先后采用450keV、300keV、200keV和120keV的注入能量,将注入剂量为7.97×1013cm-2、4.69×1013cm-2、3.27×1013cm-2和2.97×1013cm-2的Al离子,分四次注入到N-漂移层2的注入区,形成深度为0.5μm,浓度为3×1018cm-3的P+栅介质保护区5,注入温度为650℃。The implantation energies of 450keV , 300keV , 200keV and 120keV were adopted successively , and Al Ions are implanted into the implantation region of the N-drift layer 2 in four times to form a P+ gate dielectric protection region 5 with a depth of 0.5 μm and a concentration of 3×10 18 cm −3 , and the implantation temperature is 650° C.
步骤f,刻蚀形成源槽,如图3f所示。In step f, source grooves are formed by etching, as shown in FIG. 3f.
首先磁控溅射一层的Ti膜作为ICP刻蚀掩膜,然后涂胶光刻,进行ICP刻蚀,刻蚀出槽的宽度为1μm,深度为3μm,最后去胶,去刻蚀掩膜,清洗成光片。其工艺条件为:ICP线圈功率850W,源功率100W,反应气体SF6和O2分别为48sccm和12sccm。First magnetron sputtering a layer The Ti film is used as an ICP etching mask, and then glued to photolithography, and ICP etching is performed, and the width of the etched groove is 1 μm, and the depth is 3 μm. Finally, the glue is removed, the etching mask is removed, and a light sheet is cleaned. The process conditions are: ICP coil power 850W, source power 100W, reaction gas SF6 and O2 are 48sccm and 12sccm respectively.
步骤g,利用源槽的刻蚀掩膜在N-漂移层2进行多次Al离子自对准注入,如图3g所示。In step g, self-aligned implantation of Al ions is performed on the N-drift layer 2 for multiple times by using the etching mask of the source trench, as shown in FIG. 3g.
首先先后采用450keV、300keV、200keV和120keV的注入能量,将注入剂量为7.97×1013cm-2、4.69×1013cm-2、3.27×1013cm-2和2.97×1013cm-2的Al离子,分四次注入到N-漂移层2的注入区,形成深度为0.5μm,浓度为3×1018cm-3的P+源槽拐角保护区6,注入温度为650℃。Firstly, the implantation energies of 450keV, 300keV, 200keV and 120keV were adopted successively, and the implant doses were 7.97×10 13 cm -2 , 4.69×10 13 cm -2 , 3.27×10 13 cm -2 and 2.97×10 13 cm -2 Al ions are implanted into the implantation region of the N-drift layer 2 in four times to form a P+ source groove corner protection region 6 with a depth of 0.5 μm and a concentration of 3×10 18 cm -3 , and the implantation temperature is 650°C.
再采用RCA清洗标准对SiC表面进行清洗,烘干后制作C膜保护,然后在1700~1750℃氩气氛围中进行离子激活退火10min。Then use the RCA cleaning standard to clean the SiC surface, make a C film protection after drying, and then perform ion activation annealing in an argon atmosphere at 1700-1750 ° C for 10 minutes.
步骤h,制备槽栅介质7,所用材料为SiO2,如图3h所示。In step h, trench gate dielectric 7 is prepared, and the material used is SiO 2 , as shown in FIG. 3h.
采用干氧工艺在1150℃下制备SiO2栅介质层,厚度为100nm,然后在1050℃,NO氛围下进行退火,降低SiO2薄膜表面的粗糙度。The SiO 2 gate dielectric layer was prepared at 1150°C by dry oxygen process with a thickness of 100nm, and then annealed at 1050°C in NO atmosphere to reduce the roughness of the SiO 2 film surface.
步骤i,制备poly Si栅,如图3i所示。Step i, preparing a poly Si gate, as shown in Figure 3i.
采用低压热壁化学汽相淀积法生长poly Si填满栅槽,淀积温度为600~650℃,淀积压强为60~80Pa,反应气体为硅烷和磷化氢,载运气体为氦气,然后涂胶光刻,刻蚀polySi层,形成多晶硅栅,最后去胶,清洗。Poly Si is grown by low-pressure hot-wall chemical vapor deposition to fill the gate groove, the deposition temperature is 600-650°C, the deposition pressure is 60-80Pa, the reaction gas is silane and phosphine, and the carrier gas is helium. Then glue photolithography, etch the polySi layer to form a polysilicon gate, and finally remove the glue and clean.
步骤j,制备钝化层,如图3j所示。Step j, preparing a passivation layer, as shown in Figure 3j.
在器件表面淀积一层场氧或者Si3N4层,然后涂胶光刻,腐蚀钝化层开电极接触孔,最后去胶,清洗。Deposit a layer of field oxygen or Si 3 N 4 on the surface of the device, then apply glue for photolithography, etch the passivation layer to open electrode contact holes, and finally remove the glue and clean.
步骤k,制备电极,如图3k所示。In step k, an electrode is prepared, as shown in FIG. 3k.
先在正面电子束蒸发Ti/Ni/Au制作栅,源电极,然后涂胶光刻,腐蚀金属形成栅,源电极,去胶,清洗。First, the front electron beam evaporates Ti/Ni/Au to make the gate and source electrode, then apply glue and photolithography, corrode the metal to form the gate, source electrode, remove the glue, and clean.
再在背面电子束蒸发Ti/Ni/Au制作漏电极,最后在Ar气氛中快速退火3min,温度为1050℃。因为N-漂移层2和P-外延层3掺杂浓度较低,在源极10与和N-漂移层2和P-外延层3界面形成肖特基接触,其他界面形成欧姆接触。Then Ti/Ni/Au is evaporated by electron beam on the back side to make the drain electrode, and finally annealed rapidly in Ar atmosphere for 3min at a temperature of 1050°C. Because the doping concentration of the N-drift layer 2 and the P-epitaxial layer 3 is relatively low, a Schottky contact is formed at the interface between the source electrode 10 and the N-drift layer 2 and the P-epitaxial layer 3 , and ohmic contacts are formed at other interfaces.
实施例三Embodiment three
请参见图3,图3为本实施例提供了另一种SiC双槽UMOSFET器件制备方法,该制备方法包括如下步骤:Please refer to FIG. 3. FIG. 3 provides another SiC double-slot UMOSFET device preparation method for this embodiment. The preparation method includes the following steps:
步骤a,在N型SiC衬底1上外延生长N-漂移层2,如图3a所示。In step a, an N-drift layer 2 is epitaxially grown on an N-type SiC substrate 1, as shown in FIG. 3a.
先对厚度为500μm,氮离子掺杂浓度为1×1020cm-3的N型SiC衬底1进行RCA标准清洗,然后在整个SiC衬底1上外延生长厚度为20μm,氮离子掺杂浓度为3×1015cm-3的N-漂移层2。其工艺条件是:温度为1600℃,压力为100mbar,反应气体是硅烷和丙烷,载运气体为纯氢气,杂质源为液态氮气。RCA standard cleaning is performed on the N-type SiC substrate 1 with a thickness of 500 μm and a nitrogen ion doping concentration of 1×10 20 cm -3 , and then epitaxial growth on the entire SiC substrate 1 with a thickness of 20 μm and a nitrogen ion doping concentration of The N-drift layer 2 is 3×10 15 cm -3 . The process conditions are as follows: temperature is 1600°C, pressure is 100mbar, reaction gas is silane and propane, carrier gas is pure hydrogen, and impurity source is liquid nitrogen.
步骤b,外延生长P-外延层3,如图3b所示。Step b, epitaxially growing the P- epitaxial layer 3, as shown in FIG. 3b.
在N-漂移层2上生长一层厚度为1.5μm,Al离子掺杂浓度为1×1017cm-3的P-外延层3。其工艺条件是:温度为1600℃,压力为100mbar,反应气体是硅烷和丙烷,载运气体为纯氢气,杂质源为三基甲铝。A P-epitaxial layer 3 with a thickness of 1.5 μm and an Al ion doping concentration of 1×10 17 cm −3 is grown on the N-drift layer 2 . The process conditions are as follows: the temperature is 1600°C, the pressure is 100mbar, the reaction gas is silane and propane, the carrier gas is pure hydrogen, and the impurity source is trimethylaluminum.
步骤c,外延生长N+源区层4,如图3c所示。Step c, epitaxially growing the N+ source region layer 4, as shown in FIG. 3c.
在P-外延层3上生长一层厚度为0.5μm,氮离子掺杂浓度为5×1018cm-3的N+源区层4。其工艺条件是:温度为1600℃,压力为100mbar,反应气体是硅烷和丙烷,载运气体为纯氢气,杂质源为液态氮气。An N+ source region layer 4 with a thickness of 0.5 μm and a nitrogen ion doping concentration of 5×10 18 cm −3 is grown on the P − epitaxial layer 3 . The process conditions are as follows: temperature is 1600°C, pressure is 100mbar, reaction gas is silane and propane, carrier gas is pure hydrogen, and impurity source is liquid nitrogen.
步骤d,刻蚀形成栅槽,如图3d所示。In step d, gate grooves are formed by etching, as shown in FIG. 3d.
首先磁控溅射一层的Ti膜作为ICP刻蚀掩膜,然后涂胶光刻,进行ICP刻蚀,刻蚀出槽的宽度为1.5μm,深度为2.5μm,最后去胶,去刻蚀掩膜,清洗成光片。其工艺条件为:ICP线圈功率850W,源功率100W,反应气体SF6和O2分别为48sccm和12sccm。First magnetron sputtering a layer The Ti film is used as an ICP etching mask, and then coated with photolithography, and ICP etching is performed. The width of the etched groove is 1.5 μm, and the depth is 2.5 μm. Finally, the glue is removed, the etching mask is removed, and it is cleaned into a light sheet . The process conditions are: ICP coil power 850W, source power 100W, reaction gas SF6 and O2 are 48sccm and 12sccm respectively.
步骤e,利用栅槽的刻蚀掩膜在N-漂移层2进行多次Al离子自对准注入,如图3e所示。In step e, self-aligned implantation of Al ions is performed multiple times in the N-drift layer 2 by using the etching mask of the gate groove, as shown in FIG. 3e.
先后采用450keV、300keV、200keV和120keV的注入能量,将注入剂量为7.97×1013cm-2、4.69×1013cm-2、3.27×1013cm-2和2.97×1013cm-2的Al离子,分四次注入到N-漂移层2的注入区,形成深度为0.5μm,浓度为3×1018cm-3的P+栅介质保护区5,注入温度为650℃。The implantation energies of 450keV , 300keV , 200keV and 120keV were adopted successively , and Al Ions are implanted into the implantation region of the N-drift layer 2 in four times to form a P+ gate dielectric protection region 5 with a depth of 0.5 μm and a concentration of 3×10 18 cm −3 , and the implantation temperature is 650° C.
步骤f,刻蚀形成源槽,如图3f所示。In step f, source grooves are formed by etching, as shown in FIG. 3f.
首先磁控溅射一层的Ti膜作为ICP刻蚀掩膜,然后涂胶光刻,进行ICP刻蚀,刻蚀出槽的宽度为1μm,深度为3μm,最后去胶,去刻蚀掩膜,清洗成光片。其工艺条件为:ICP线圈功率850W,源功率100W,反应气体SF6和O2分别为48sccm和12sccm。First magnetron sputtering a layer The Ti film is used as an ICP etching mask, and then glued to photolithography, and ICP etching is performed, and the width of the etched groove is 1 μm, and the depth is 3 μm. Finally, the glue is removed, the etching mask is removed, and a light sheet is cleaned. The process conditions are: ICP coil power 850W, source power 100W, reaction gas SF6 and O2 are 48sccm and 12sccm respectively.
步骤g,利用源槽的刻蚀掩膜在N-漂移层2进行多次Al离子自对准注入,如图3g所示。In step g, self-aligned implantation of Al ions is performed on the N-drift layer 2 for multiple times by using the etching mask of the source trench, as shown in FIG. 3g.
首先先后采用450keV、300keV、200keV和120keV的注入能量,将注入剂量为7.97×1013cm-2、4.69×1013cm-2、3.27×1013cm-2和2.97×1013cm-2的Al离子,分四次注入到N-漂移层2的注入区,形成深度为0.5μm,浓度为3×1018cm-3的P+源槽拐角保护区6,注入温度为650℃。Firstly, the implantation energies of 450keV, 300keV, 200keV and 120keV were adopted successively, and the implant doses were 7.97×10 13 cm -2 , 4.69×10 13 cm -2 , 3.27×10 13 cm -2 and 2.97×10 13 cm -2 Al ions are implanted into the implantation region of the N-drift layer 2 in four times to form a P+ source groove corner protection region 6 with a depth of 0.5 μm and a concentration of 3×10 18 cm -3 , and the implantation temperature is 650°C.
再采用RCA清洗标准对SiC表面进行清洗,烘干后制作C膜保护,然后在1700~1750℃氩气氛围中进行离子激活退火10min。Then use the RCA cleaning standard to clean the SiC surface, make a C film protection after drying, and then perform ion activation annealing in an argon atmosphere at 1700-1750 ° C for 10 minutes.
步骤h,制备槽栅介质7,所用材料为SiO2,如图3h所示。In step h, trench gate dielectric 7 is prepared, and the material used is SiO 2 , as shown in FIG. 3h.
采用干氧工艺在1150℃下制备SiO2栅介质层,厚度为100nm,然后在1050℃,NO氛围下进行退火,降低SiO2薄膜表面的粗糙度。The SiO 2 gate dielectric layer was prepared at 1150°C by dry oxygen process with a thickness of 100nm, and then annealed at 1050°C in NO atmosphere to reduce the roughness of the SiO 2 film surface.
步骤i,制备poly Si栅,如图3i所示。Step i, preparing a poly Si gate, as shown in Figure 3i.
采用低压热壁化学汽相淀积法生长poly Si填满栅槽,淀积温度为600~650℃,淀积压强为60~80Pa,反应气体为硅烷和磷化氢,载运气体为氦气,然后涂胶光刻,刻蚀polySi层,形成多晶硅栅,最后去胶,清洗。Poly Si is grown by low-pressure hot-wall chemical vapor deposition to fill the gate groove, the deposition temperature is 600-650°C, the deposition pressure is 60-80Pa, the reaction gas is silane and phosphine, and the carrier gas is helium. Then glue photolithography, etch the polySi layer to form a polysilicon gate, and finally remove the glue and clean.
步骤j,制备钝化层,如图3j所示。Step j, preparing a passivation layer, as shown in Figure 3j.
在器件表面淀积一层场氧或者Si3N4层,然后涂胶光刻,腐蚀钝化层开电极接触孔,最后去胶,清洗。Deposit a layer of field oxygen or Si 3 N 4 on the surface of the device, then apply glue for photolithography, etch the passivation layer to open electrode contact holes, and finally remove the glue and clean.
步骤k,制备电极,如图3k所示。In step k, an electrode is prepared, as shown in FIG. 3k.
先在正面电子束蒸发Ti/Ni/Au制作栅,源电极,然后涂胶光刻,腐蚀金属形成栅,源电极,去胶,清洗。First, the front electron beam evaporates Ti/Ni/Au to make the gate and source electrode, then apply glue and photolithography, corrode the metal to form the gate, source electrode, remove the glue, and clean.
再在背面电子束蒸发Ti/Ni/Au制作漏电极,最后在Ar气氛中快速退火3min,温度为1050℃。因为N-漂移层2和P-外延层3掺杂浓度较低,在源极10与和N-漂移层2和P-外延层3界面形成肖特基接触,其他界面形成欧姆接触。Then Ti/Ni/Au is evaporated by electron beam on the back side to make the drain electrode, and finally annealed rapidly in Ar atmosphere for 3min at a temperature of 1050°C. Because the doping concentration of the N-drift layer 2 and the P-epitaxial layer 3 is relatively low, a Schottky contact is formed at the interface between the source electrode 10 and the N-drift layer 2 and the P-epitaxial layer 3 , and ohmic contacts are formed at other interfaces.
实施例四Embodiment four
请参见图3,图3为本实施例提供了另一种SiC双槽UMOSFET器件制备方法,该制备方法包括如下步骤:Please refer to FIG. 3. FIG. 3 provides another SiC double-slot UMOSFET device preparation method for this embodiment. The preparation method includes the following steps:
步骤a,在N型Si衬底1上外延生长N-漂移层2,如图3a所示。In step a, an N-drift layer 2 is epitaxially grown on an N-type Si substrate 1, as shown in FIG. 3a.
先对厚度为300μm,氮离子掺杂浓度为1×1019cm-3的N型SiC衬底进行RCA标准清洗,然后在整个SiC衬底1上外延生长厚度为15μm,氮离子掺杂浓度为6×1015cm-3的N-漂移层2。其工艺条件是:温度为1600℃,压力为100mbar,反应气体是硅烷和丙烷,载运气体为纯氢气,杂质源为液态氮气。RCA standard cleaning was performed on the N-type SiC substrate with a thickness of 300 μm and a nitrogen ion doping concentration of 1×10 19 cm -3 , and then epitaxial growth was performed on the entire SiC substrate 1 with a thickness of 15 μm and a nitrogen ion doping concentration of N-drift layer 2 of 6×10 15 cm −3 . The process conditions are as follows: temperature is 1600°C, pressure is 100mbar, reaction gas is silane and propane, carrier gas is pure hydrogen, and impurity source is liquid nitrogen.
步骤b,外延生长P-外延层3,如图3b所示。Step b, epitaxially growing the P- epitaxial layer 3, as shown in FIG. 3b.
在N-漂移层2上生长一层厚度为1.3μm,Al离子掺杂浓度为1×1017cm-3的P-外延层3。其工艺条件是:温度为1600℃,压力为100mbar,反应气体是硅烷和丙烷,载运气体为纯氢气,杂质源为三基甲铝。A P-epitaxial layer 3 with a thickness of 1.3 μm and an Al ion doping concentration of 1×10 17 cm −3 is grown on the N-drift layer 2 . The process conditions are as follows: the temperature is 1600°C, the pressure is 100mbar, the reaction gas is silane and propane, the carrier gas is pure hydrogen, and the impurity source is trimethylaluminum.
步骤c,外延生长N+源区层4,如图3c所示。Step c, epitaxially growing the N+ source region layer 4, as shown in FIG. 3c.
在P-外延层3上生长一层厚度为0.5μm,氮离子掺杂浓度为5×1018cm-3的N+源区层4。An N+ source region layer 4 with a thickness of 0.5 μm and a nitrogen ion doping concentration of 5×10 18 cm −3 is grown on the P − epitaxial layer 3 .
其工艺条件是:温度为1600℃,压力为100mbar,反应气体是硅烷和丙烷,载运气体为纯氢气,杂质源为液态氮气。The process conditions are as follows: temperature is 1600°C, pressure is 100mbar, reaction gas is silane and propane, carrier gas is pure hydrogen, and impurity source is liquid nitrogen.
步骤d,刻蚀形成栅槽,如图3d所示。In step d, gate grooves are formed by etching, as shown in FIG. 3d.
首先磁控溅射一层的Ti膜作为ICP刻蚀掩膜,然后涂胶光刻,进行ICP刻蚀,刻蚀出槽的宽度为1.5μm,深度为2.5μm,最后去胶,去刻蚀掩膜,清洗成光片。其工艺条件为:ICP线圈功率850W,源功率100W,反应气体SF6和O2分别为48sccm和12sccm。First magnetron sputtering a layer The Ti film is used as an ICP etching mask, and then coated with photolithography, and ICP etching is performed. The width of the etched groove is 1.5 μm, and the depth is 2.5 μm. Finally, the glue is removed, the etching mask is removed, and it is cleaned into a light sheet . The process conditions are: ICP coil power 850W, source power 100W, reaction gas SF6 and O2 are 48sccm and 12sccm respectively.
步骤e,利用栅槽的刻蚀掩膜在N-漂移层2进行多次Al离子自对准注入,如图3e所示。In step e, self-aligned implantation of Al ions is performed multiple times in the N-drift layer 2 by using the etching mask of the gate groove, as shown in FIG. 3e.
先后采用450keV、300keV、200keV和120keV的注入能量,将注入剂量为7.97×1013cm-2、4.69×1013cm-2、3.27×1013cm-2和2.97×1013cm-2的Al离子,分四次注入到N-漂移层2的注入区,形成深度为0.5μm,浓度为3×1018cm-3的P+栅介质保护区5,注入温度为650℃。The implantation energies of 450keV , 300keV , 200keV and 120keV were adopted successively , and Al Ions are implanted into the implantation region of the N-drift layer 2 in four times to form a P+ gate dielectric protection region 5 with a depth of 0.5 μm and a concentration of 3×10 18 cm −3 , and the implantation temperature is 650° C.
步骤f,刻蚀形成源槽,如图3f所示。In step f, source grooves are formed by etching, as shown in FIG. 3f.
首先磁控溅射一层的Ti膜作为ICP刻蚀掩膜,然后涂胶光刻,进行ICP刻蚀,刻蚀出槽的宽度为1μm,深度为3μm,最后去胶,去刻蚀掩膜,清洗成光片。其工艺条件为:ICP线圈功率850W,源功率100W,反应气体SF6和O2分别为48sccm和12sccm。First magnetron sputtering a layer The Ti film is used as an ICP etching mask, and then glued to photolithography, and ICP etching is performed, and the width of the etched groove is 1 μm, and the depth is 3 μm. Finally, the glue is removed, the etching mask is removed, and a light sheet is cleaned. The process conditions are: ICP coil power 850W, source power 100W, reaction gas SF6 and O2 are 48sccm and 12sccm respectively.
步骤g,利用源槽的刻蚀掩膜在N-漂移层2进行多次Al离子自对准注入,如图3g所示。In step g, self-aligned implantation of Al ions is performed on the N-drift layer 2 for multiple times by using the etching mask of the source trench, as shown in FIG. 3g.
首先先后采用450keV、300keV、200keV和120keV的注入能量,将注入剂量为7.97×1013cm-2、4.69×1013cm-2、3.27×1013cm-2和2.97×1013cm-2的Al离子,分四次注入到N-漂移层2的注入区,形成深度为0.5μm,浓度为3×1018cm-3的P+源槽拐角保护区6,注入温度为650℃。Firstly, the implantation energies of 450keV, 300keV, 200keV and 120keV were adopted successively, and the implant doses were 7.97×10 13 cm -2 , 4.69×10 13 cm -2 , 3.27×10 13 cm -2 and 2.97×10 13 cm -2 Al ions are implanted into the implantation region of the N-drift layer 2 in four times to form a P+ source groove corner protection region 6 with a depth of 0.5 μm and a concentration of 3×10 18 cm -3 , and the implantation temperature is 650°C.
再采用RCA清洗标准对SiC表面进行清洗,烘干后制作C膜保护,然后在1700~1750℃氩气氛围中进行离子激活退火10min。Then use the RCA cleaning standard to clean the SiC surface, make a C film protection after drying, and then perform ion activation annealing in an argon atmosphere at 1700-1750 ° C for 10 minutes.
步骤h,制备槽栅介质7,所用材料为SiO2,如图3h所示。In step h, trench gate dielectric 7 is prepared, and the material used is SiO 2 , as shown in FIG. 3h.
采用干氧工艺在1150℃下制备SiO2栅介质层,厚度为100nm,然后在1050℃,NO氛围下进行退火,降低SiO2薄膜表面的粗糙度。The SiO 2 gate dielectric layer was prepared at 1150°C by dry oxygen process with a thickness of 100nm, and then annealed at 1050°C in NO atmosphere to reduce the roughness of the SiO 2 film surface.
步骤i,制备poly Si栅,如图3i所示。Step i, preparing a poly Si gate, as shown in Figure 3i.
采用低压热壁化学汽相淀积法生长poly Si填满栅槽,淀积温度为600~650℃,淀积压强为60~80Pa,反应气体为硅烷和磷化氢,载运气体为氦气,然后涂胶光刻,刻蚀polySi层,形成多晶硅栅,最后去胶,清洗。Poly Si is grown by low-pressure hot-wall chemical vapor deposition to fill the gate groove, the deposition temperature is 600-650°C, the deposition pressure is 60-80Pa, the reaction gas is silane and phosphine, and the carrier gas is helium. Then apply glue for photolithography, etch the polySi layer to form a polysilicon gate, and finally remove the glue and clean.
步骤j,制备钝化层,如图3j所示。Step j, preparing a passivation layer, as shown in Figure 3j.
在器件表面淀积一层场氧或者Si3N4层,然后涂胶光刻,腐蚀钝化层开电极接触孔,最后去胶,清洗。Deposit a layer of field oxygen or Si 3 N 4 on the surface of the device, then apply glue for photolithography, etch the passivation layer to open electrode contact holes, and finally remove the glue and clean.
步骤k,制备电极,如图3k所示。In step k, an electrode is prepared, as shown in FIG. 3k.
先在正面电子束蒸发Ti/Ni/Au制作栅,源电极,然后涂胶光刻,腐蚀金属形成栅,源电极,去胶,清洗。First, the front electron beam evaporates Ti/Ni/Au to make the gate and source electrode, then apply glue and photolithography, corrode the metal to form the gate, source electrode, remove the glue, and clean.
再在背面电子束蒸发Ti/Ni/Au制作漏电极,最后在Ar气氛中快速退火3min,温度为1050℃。因为N-漂移层2和P-外延层3掺杂浓度较低,在源极10与和N-漂移层2和P-外延层3界面形成肖特基接触,其他界面形成欧姆接触。Then Ti/Ni/Au is evaporated by electron beam on the back side to make the drain electrode, and finally annealed rapidly in Ar atmosphere for 3min at a temperature of 1050°C. Because the doping concentration of the N-drift layer 2 and the P-epitaxial layer 3 is relatively low, a Schottky contact is formed at the interface between the source electrode 10 and the N-drift layer 2 and the P-epitaxial layer 3 , and ohmic contacts are formed at other interfaces.
综上所述,本文中应用了具体个例对本发明本发明实施例提供的一种SiC双槽UMOSFET器件及其制备方法的实施方式进行了阐述,以上实施例的说明只是用于帮助理解本发明的方法及其核心思想;同时,对于本领域的一般技术人员,依据本发明的思想,在具体实施方式及应用范围上均会有改变之处,综上所述,本说明书内容不应理解为对本发明的限制,本发明的保护范围应以所附的权利要求为准。In summary, this paper uses specific examples to illustrate the implementation of a SiC double-slot UMOSFET device and its manufacturing method provided by the embodiment of the present invention. The description of the above embodiment is only used to help understand the present invention method and its core idea; at the same time, for those of ordinary skill in the art, according to the idea of the present invention, there will be changes in the specific implementation and scope of application. In summary, the content of this specification should not be understood as For the limitation of the present invention, the scope of protection of the present invention should be based on the appended claims.
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