CN105817479A - A kind of magnesium alloy sheet rolling method - Google Patents
A kind of magnesium alloy sheet rolling method Download PDFInfo
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- CN105817479A CN105817479A CN201610161813.8A CN201610161813A CN105817479A CN 105817479 A CN105817479 A CN 105817479A CN 201610161813 A CN201610161813 A CN 201610161813A CN 105817479 A CN105817479 A CN 105817479A
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- 238000005096 rolling process Methods 0.000 title claims abstract description 68
- 229910000861 Mg alloy Inorganic materials 0.000 title claims abstract description 50
- 238000000034 method Methods 0.000 title claims abstract description 21
- 238000010438 heat treatment Methods 0.000 claims abstract description 30
- 238000003825 pressing Methods 0.000 claims abstract description 6
- 238000010008 shearing Methods 0.000 claims abstract description 5
- 238000000137 annealing Methods 0.000 claims description 9
- 238000005498 polishing Methods 0.000 claims description 7
- 238000005266 casting Methods 0.000 claims 1
- 238000004519 manufacturing process Methods 0.000 abstract description 3
- 238000005336 cracking Methods 0.000 abstract description 2
- 238000004321 preservation Methods 0.000 abstract 1
- 239000000463 material Substances 0.000 description 6
- 229910045601 alloy Inorganic materials 0.000 description 3
- 239000000956 alloy Substances 0.000 description 3
- 238000013016 damping Methods 0.000 description 3
- 229910000838 Al alloy Inorganic materials 0.000 description 2
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 2
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 229910052749 magnesium Inorganic materials 0.000 description 2
- 239000011777 magnesium Substances 0.000 description 2
- 238000002203 pretreatment Methods 0.000 description 2
- 230000008569 process Effects 0.000 description 2
- 239000011701 zinc Substances 0.000 description 2
- 229910052725 zinc Inorganic materials 0.000 description 2
- 229910000831 Steel Inorganic materials 0.000 description 1
- 230000009471 action Effects 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 238000005520 cutting process Methods 0.000 description 1
- 230000005684 electric field Effects 0.000 description 1
- 238000001125 extrusion Methods 0.000 description 1
- 238000005242 forging Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000011056 performance test Methods 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 230000005855 radiation Effects 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
- 238000005728 strengthening Methods 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B21—MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
- B21B—ROLLING OF METAL
- B21B3/00—Rolling materials of special alloys so far as the composition of the alloy requires or permits special rolling methods or sequences ; Rolling of aluminium, copper, zinc or other non-ferrous metals
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B23—MACHINE TOOLS; METAL-WORKING NOT OTHERWISE PROVIDED FOR
- B23P—METAL-WORKING NOT OTHERWISE PROVIDED FOR; COMBINED OPERATIONS; UNIVERSAL MACHINE TOOLS
- B23P15/00—Making specific metal objects by operations not covered by a single other subclass or a group in this subclass
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Abstract
本发明公开了一种AZ33m镁合金薄板轧制方法,该方法包括坯料选取、坯料预处理,坯料预热,升温和保温后进行第一次轧制,后续轧制加热时间为0.5h,每轧一次加热窑温度降低6~10℃,轧辊速度为0.5~0.7m/s,每次下压量为20%~30%,轧制3次后沿轧制方向裁剪板子,回炉加热再沿垂直于上次轧制方向进行轧制,对轧制完毕薄板立即在矫直机上进行矫直,在剪板机上裁去飞边,低温退火,去除氧化物和表面小凹坑,保鲜膜包装。本发明解决了轧制对坯料要求高、生产过程中加热及升温控制繁琐、AZ33m镁合金轧制容易开裂、AZ33m镁合金薄板性能不均匀的问题。
The invention discloses a rolling method of an AZ33m magnesium alloy thin plate. The method includes blank selection, blank pretreatment, blank preheating, heating up and heat preservation, and performing the first rolling. The heating time for the subsequent rolling is 0.5h. The temperature of the heating kiln is lowered by 6-10°C once, the roll speed is 0.5-0.7m/s, and the pressing amount is 20%-30% each time. Carry out rolling in the last rolling direction, straighten the thin plate on the straightening machine immediately after rolling, cut off the flash on the shearing machine, anneal at low temperature, remove oxides and small pits on the surface, and pack in plastic wrap. The invention solves the problems of high requirements on blanks for rolling, cumbersome heating and temperature rise control in the production process, easy cracking of AZ33m magnesium alloy rolling, and uneven performance of AZ33m magnesium alloy thin plates.
Description
技术领域technical field
板轧制方法本发明属于镁合金薄板轧制技术领域,尤其涉及一种一种AZ33m镁合金薄。Plate rolling method The invention belongs to the technical field of magnesium alloy sheet rolling, and in particular relates to an AZ33m magnesium alloy sheet.
背景技术Background technique
目前,镁合金弹性模量低:弹性模量是工程材料重要的性能参数,当镁合金受到外力作用时,应力会均匀分布在材料中,从而避免了镁合金中产生过于强烈的应力集中;镁合金比强度高:比强度的定义为材料断裂时所受的应力除以自身的表观密度,材料的比强度越高表明达到相应强度所用的材料质量越轻;镁合金阻尼性能优良:阻尼是指由于外界或体系自身固有的性征使任何振动系统的振幅有逐渐下降的趋势的特性。较铝合金,镁合金的阻尼特性具有明显的优势;镁合金电磁屏蔽能力强:镁合金具有较强的屏蔽作用,可以通过屏蔽交变电场和磁场来屏蔽电磁波辐射;镁合金加工性好:镁合金的切削速度比起铝合金和钢材等要快很多;镁的晶格结构为hcp(密排六方),镁合金室温塑性变形能力差,室温下塑性成型困难,但在高温时,镁合金会发生滑移和孪晶变形,在两种变形的综合作用下塑性成型能力明显得到提高,考虑到镁合金成型过程中应力状态变和形速率对镁合金加工强化的重要性,目前镁合金成型除少量轧制成型外,其它如挤压和锻作为镁合金塑性成型的主要方式;At present, the elastic modulus of magnesium alloy is low: elastic modulus is an important performance parameter of engineering materials. When magnesium alloy is subjected to external force, the stress will be evenly distributed in the material, thus avoiding too strong stress concentration in magnesium alloy; The specific strength of the alloy is high: the specific strength is defined as the stress suffered by the material when it breaks divided by its own apparent density. The higher the specific strength of the material, the lighter the material used to achieve the corresponding strength; the magnesium alloy has excellent damping performance: the damping is It refers to the characteristic that the amplitude of any vibration system has a tendency to gradually decrease due to the external environment or the inherent characteristics of the system itself. Compared with aluminum alloys, magnesium alloys have obvious advantages in damping characteristics; magnesium alloys have strong electromagnetic shielding ability: magnesium alloys have a strong shielding effect, and can shield electromagnetic wave radiation by shielding alternating electric fields and magnetic fields; magnesium alloys have good processability: magnesium The cutting speed of the alloy is much faster than that of aluminum alloy and steel; the lattice structure of magnesium is hcp (hexagonal close-packed), the plastic deformation ability of the magnesium alloy is poor at room temperature, and the plastic forming is difficult at room temperature, but at high temperature, the magnesium alloy will Slip and twin deformation occur, and the plastic forming ability is significantly improved under the combined action of the two deformations. Considering the importance of stress state change and deformation rate on the processing and strengthening of magnesium alloys during the forming process of magnesium alloys, currently magnesium alloys are formed except Except for a small amount of rolling forming, others such as extrusion and forging are the main methods of plastic forming of magnesium alloys;
目前镁合金轧制存在的主要问题为:轧制温度过高或者过低均容易开裂,温度过高直接影响其强度,而温度过低直接影响其塑性;目前轧制所得板材的性能不均匀,存在各向异性;还没有一套稳定成熟的轧制工艺适用于AZ33m镁合金薄板的生产制备;随着现在镁合金市场需求在扩大,特别是高强高韧镁合金薄板需求迫切。At present, the main problems in magnesium alloy rolling are: the rolling temperature is too high or too low, it is easy to crack, the temperature is too high directly affects its strength, and the temperature is too low directly affects its plasticity; the performance of the rolled plate is not uniform at present, There is anisotropy; there is no stable and mature rolling process suitable for the production and preparation of AZ33m magnesium alloy sheets; as the market demand for magnesium alloys is expanding, especially the demand for high-strength and high-toughness magnesium alloy sheets is urgent.
发明内容Contents of the invention
本发明的目的在于提供一种镁合金薄板轧制方法,旨在解决含锌量高的镁合金轧制时易开裂、镁合金轧制后力学性能低且不均匀的难题。The purpose of the present invention is to provide a magnesium alloy thin plate rolling method, aiming to solve the problems that the magnesium alloy with high zinc content is easy to crack when rolling, and the mechanical properties of the magnesium alloy are low and uneven after rolling.
本发明是这样实现的,一种镁合金薄板轧制方法,该镁合金薄板轧制方法包括以下步骤:The present invention is achieved in this way, a magnesium alloy thin plate rolling method, the magnesium alloy thin plate rolling method comprises the following steps:
坯料选取:选取AZ33m铸造板材或挤压板材;Billet selection: select AZ33m cast plate or extruded plate;
坯料预处理:对铸造板材表面进行铣面,去除氧化物,对仍有少部分裂纹的使用抛光机局部打磨,挤压板材无需处理;Billet pretreatment: Mill the surface of the cast plate to remove oxides, and use a polishing machine to locally polish the surface with a small number of cracks, and the extruded plate does not need to be processed;
坯料预热:开启加热滚道窑,温度设置为330~350℃,坯料随炉加热,轧辊温度设置为(130~180℃);Billet preheating: Turn on the heating roller kiln, set the temperature to 330-350°C, heat the billet with the furnace, and set the roll temperature to (130-180°C);
升温和保温时间共计1.5h后进行第一次轧制,后续每次轧制后加热时间为0.5h,每轧一次加热窑温度降低6~10℃;The first rolling is carried out after heating up and holding time totaling 1.5h, and the heating time after each subsequent rolling is 0.5h, and the temperature of the heating kiln is lowered by 6-10°C for each rolling;
轧辊速度为0.5~0.7m/s,每次下压量为20%~30%;The speed of the roll is 0.5-0.7m/s, and the amount of pressing is 20%-30% each time;
轧制3~6次后沿轧制方向裁剪成400~600mm长的板子,回炉加热再沿垂直于上次轧制方向进行轧制,直至薄板厚度达到目标厚度;After rolling for 3 to 6 times, it is cut into 400-600mm long plates along the rolling direction, returned to the furnace for heating, and then rolled along the direction perpendicular to the previous rolling until the thickness of the thin plate reaches the target thickness;
对轧制完毕薄板立即在矫直机上进行矫直,在剪板机上裁去飞边;Immediately straighten the rolled thin plate on the straightening machine, and cut off the flash on the shearing machine;
低温退火,(100~150℃)1小时Low temperature annealing, (100~150℃) for 1 hour
在抛光机上去除经低温退火后的薄板的氧化物和表面小凹坑,最后保鲜膜包装。Remove oxides and small pits on the surface of the thin plate after low-temperature annealing on a polishing machine, and finally pack it with plastic wrap.
进一步,所述坯料预处理中坯料尺寸为500mm(宽)*10~20mm(厚)*300~1500mm(长度)。Furthermore, the size of the blank in the blank pretreatment is 500mm (width)*10-20mm (thickness)*300-1500mm (length).
进一步,所述坯料预热:开启加热滚道窑,温度设置为330~350℃,坯料随炉加热,轧辊温度设置为130~180℃。Further, the blank is preheated: the heating raceway kiln is turned on, the temperature is set at 330-350°C, the blank is heated with the furnace, and the temperature of the roll is set at 130-180°C.
进一步,所述胚料第一次轧制完毕后,后续轧制,每次轧制完毕后加热时间为0.5h,每轧一次加热窑温度降低6~10℃。Further, after the first rolling of the billet is completed, the subsequent rolling is carried out, and the heating time after each rolling is 0.5h, and the temperature of the heating kiln is lowered by 6-10°C each time rolling.
本发明解决AZ33M镁合金轧制困难的问题,一般轧制镁合金薄板只能选择合金元素低的,特别是锌元素低的,采用的是镁合金挤压板材居多,该发明工艺易于控制,且轧制的薄板性能优良且均匀,没有各向异性;解决了生产过程中加热及升温控制繁琐的问题;解决了AZ33m镁合金轧制容易开裂,成型困难的问题;解决了AZ33m镁合金薄板性能不均匀的问题;提高了AZ33m镁合金薄板性能。目前还没有现有技术方案能达到本发明在轧制AZ33m镁合金薄板的效果;The present invention solves the problem of difficult rolling of AZ33M magnesium alloy. Generally, for rolling magnesium alloy thin plates, only those with low alloy elements, especially those with low zinc elements, are used. Most of the magnesium alloy extruded plates are used. The process of the invention is easy to control, and The rolled sheet has excellent and uniform properties without anisotropy; it solves the cumbersome problem of heating and temperature rise control in the production process; it solves the problem of easy cracking and difficult forming of AZ33m magnesium alloy rolling; it solves the problem of poor performance of AZ33m magnesium alloy sheet Uniformity issue; improved AZ33m magnesium alloy sheet properties. At present, there is no prior art scheme that can reach the effect of the present invention in rolling AZ33m magnesium alloy sheet;
本发明适用于AZ33m镁合金坯料的预处理方式;适用于AZ33m镁合金坯料的加热及温度控制方案;适用于AZ33m镁合金坯料的交换轧制方向的轧制方式;适用于AZ33m镁合金坯料的矫直及最后的低温退火方式。The present invention is applicable to the pretreatment method of AZ33m magnesium alloy billet; to the heating and temperature control scheme of AZ33m magnesium alloy billet; to the rolling mode of exchange rolling direction of AZ33m magnesium alloy billet; Until the final low temperature annealing method.
附图说明Description of drawings
图1是本发明实施例提供的AZ33m镁合金薄板轧制方法流程图。Fig. 1 is a flow chart of the AZ33m magnesium alloy sheet rolling method provided by the embodiment of the present invention.
具体实施方式detailed description
为了使本发明的目的、技术方案及优点更加清楚明白,以下结合实施例,对本发明进行进一步详细说明。应当理解,此处所描述的具体实施例仅仅用以解释本发明,并不用于限定本发明。In order to make the object, technical solution and advantages of the present invention more clear, the present invention will be further described in detail below in conjunction with the examples. It should be understood that the specific embodiments described here are only used to explain the present invention, not to limit the present invention.
实例一Example one
坯料选取:选取AZ33m挤压板材400mm*400mm*10mm胚料;Billet selection: select AZ33m extruded plate 400mm*400mm*10mm blank;
坯料预处理:挤压板材无需处理;Billet pretreatment: extruded sheet does not need to be processed;
坯料预热:开启加热滚道窑,温度设置为340℃,坯料随炉加热,轧辊温度设置为150℃;Billet preheating: turn on the heating raceway kiln, set the temperature to 340°C, heat the billet with the furnace, and set the roll temperature to 150°C;
升温和保温时间共计1.5h后进行第一次轧制,后续每次轧制后回炉加热时间为0.5h,每轧一次加热窑温度降低8℃;The heating and holding time totaled 1.5h before rolling for the first time, and the subsequent heating time after each rolling was 0.5h, and the temperature of the heating kiln was lowered by 8°C every time rolling;
轧辊速度为0.6m/s,每次下压量为板材配料厚度的25%;The speed of the roll is 0.6m/s, and the amount of pressing each time is 25% of the thickness of the sheet material;
轧制3次后沿轧制方向裁剪成400长的板子,回炉加热再沿垂直于上次轧制方向进行轧制,沿此方向轧制4次,每次下压量为25%,最终薄板厚度达到1.33mm。After rolling for 3 times, cut it into 400 long plates along the rolling direction, return to the furnace to heat and then roll along the direction perpendicular to the previous rolling, and roll along this direction 4 times, each time the pressing amount is 25%, and the final thin plate The thickness reaches 1.33mm.
对轧制完毕薄板立即在矫直机上进行矫直,在剪板机上裁去飞边;Immediately straighten the rolled thin plate on the straightening machine, and cut off the flash on the shearing machine;
低温退火,(100~150℃)1小时Low temperature annealing, (100~150℃) for 1 hour
在抛光机上去除经低温退火后的薄板的氧化物和表面小凹坑,最后成品板材尺寸为400mm*1300mm*1.2mm,然后保鲜膜包装。Remove oxides and small pits on the surface of the thin plate after low-temperature annealing on a polishing machine. The final size of the finished plate is 400mm*1300mm*1.2mm, and then packaged with plastic wrap.
实例性能测试Instance performance test
按国标GB/T16865取样上诉实例的薄板材,测试力学性能结果如下:According to the national standard GB/T16865, sample the thin plate of the appeal example, and the test results of mechanical properties are as follows:
本发明适用于AZ33m镁合金坯料的预处理方式;适用于AZ33m镁合金坯料的加热及温度控制方案;适用于AZ33m镁合金坯料的交换轧制方向的轧制方式;适用于AZ33m镁合金坯料的矫直及最后的低温退火方式。The present invention is applicable to the pretreatment method of AZ33m magnesium alloy billet; to the heating and temperature control scheme of AZ33m magnesium alloy billet; to the rolling mode of exchange rolling direction of AZ33m magnesium alloy billet; Until the final low temperature annealing method.
下面结合附图对本发明的应用原理作进一步描述。The application principle of the present invention will be further described below in conjunction with the accompanying drawings.
一种AZ33m镁合金薄板轧制方法,该AZ33m镁合金薄板轧制方法包括以下步骤:A kind of AZ33m magnesium alloy sheet rolling method, this AZ33m magnesium alloy sheet rolling method comprises the following steps:
S101:坯料:AZ33m铸造板材或者挤压板材;S101: Billet: AZ33m cast plate or extruded plate;
S102:坯料预处理:铸造板材需对表面进行铣面,去掉氧化物,如还有少部分裂纹使用抛光机局部稍微打磨即可,挤压板材无需处理,该方案中坯料尺寸为500mm(宽)*10~20mm(厚)*300~1500mm(长度);S102: Billet pretreatment: The cast plate needs to be milled on the surface to remove oxides. If there are still a few cracks, use a polishing machine to polish it locally. Extruded plates do not need to be processed. The size of the billet in this plan is 500mm (width) *10~20mm(thickness)*300~1500mm(length);
S103:坯料预热:开启加热滚道窑,温度设置为330~350℃,坯料随炉加热,轧辊温度设置为(130~180℃);S103: billet preheating: turn on the heating raceway kiln, set the temperature to 330-350°C, heat the billet with the furnace, and set the roll temperature to (130-180°C);
S104:升温和保温时间共计1.5h后进行第一次轧制,后续轧制加热时间为0.5h,每轧一次加热窑温度降低6~10℃;S104: The first rolling is carried out after the total heating and holding time is 1.5 hours, the subsequent rolling heating time is 0.5 hours, and the temperature of the heating kiln is lowered by 6-10°C every time rolling;
S105:轧辊速度为0.5~0.7m/s,每次下压量为20%~30%;S105: The speed of the roll is 0.5-0.7m/s, and the pressing amount is 20%-30% each time;
S106:轧制3~6次过后沿轧制方向裁剪成400~600mm长的板子,回炉加热再沿垂直于上次轧制方向进行轧制,直至薄板厚度达到目标厚度;S106: After rolling for 3 to 6 times, cut it into 400-600 mm long plates along the rolling direction, return to the furnace for heating, and then roll along the direction perpendicular to the previous rolling until the thickness of the thin plate reaches the target thickness;
S107:对轧制完毕薄板立即在矫直机上进行矫直,在剪板机上裁去飞边;S107: Immediately straighten the rolled thin plate on the straightening machine, and cut off the flash on the shearing machine;
S108:低温退火,(100~150℃)1小时;S108: Low temperature annealing, (100-150°C) for 1 hour;
S109:在抛光机上去其氧化物和表面小凹坑,最后保鲜膜包装即成产品。S109: Remove oxides and small pits on the surface on a polishing machine, and finally pack with plastic wrap to complete the product.
以上所述仅为本发明的较佳实施例而已,并不用以限制本发明,凡在本发明的精神和原则之内所作的任何修改、等同替换和改进等,均应包含在本发明的保护范围之内。The above descriptions are only preferred embodiments of the present invention, and are not intended to limit the present invention. Any modifications, equivalent replacements and improvements made within the spirit and principles of the present invention should be included in the protection of the present invention. within range.
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