CA1203115A - Process for the manufacture of a sweetener based on milk and a sweetener manufactured according to the process - Google Patents
Process for the manufacture of a sweetener based on milk and a sweetener manufactured according to the processInfo
- Publication number
- CA1203115A CA1203115A CA000417243A CA417243A CA1203115A CA 1203115 A CA1203115 A CA 1203115A CA 000417243 A CA000417243 A CA 000417243A CA 417243 A CA417243 A CA 417243A CA 1203115 A CA1203115 A CA 1203115A
- Authority
- CA
- Canada
- Prior art keywords
- lactose
- dry matter
- solution
- galactose
- glucose
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 238000000034 method Methods 0.000 title claims abstract description 48
- 235000003599 food sweetener Nutrition 0.000 title claims abstract description 25
- 239000003765 sweetening agent Substances 0.000 title claims abstract description 25
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 7
- 235000013336 milk Nutrition 0.000 title abstract description 6
- 239000008267 milk Substances 0.000 title abstract description 6
- 210000004080 milk Anatomy 0.000 title abstract description 6
- GUBGYTABKSRVRQ-QKKXKWKRSA-N Lactose Natural products OC[C@H]1O[C@@H](O[C@H]2[C@H](O)[C@@H](O)C(O)O[C@@H]2CO)[C@H](O)[C@@H](O)[C@H]1O GUBGYTABKSRVRQ-QKKXKWKRSA-N 0.000 claims abstract description 141
- 239000008101 lactose Substances 0.000 claims abstract description 136
- 150000001768 cations Chemical class 0.000 claims abstract description 37
- 230000007062 hydrolysis Effects 0.000 claims abstract description 35
- 238000006460 hydrolysis reaction Methods 0.000 claims abstract description 35
- 238000004132 cross linking Methods 0.000 claims abstract description 34
- 230000002378 acidificating effect Effects 0.000 claims abstract description 28
- 229930182830 galactose Natural products 0.000 claims abstract description 28
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 claims abstract description 26
- 239000008103 glucose Substances 0.000 claims abstract description 26
- WQZGKKKJIJFFOK-PHYPRBDBSA-N alpha-D-galactose Chemical compound OC[C@H]1O[C@H](O)[C@H](O)[C@@H](O)[C@H]1O WQZGKKKJIJFFOK-PHYPRBDBSA-N 0.000 claims abstract description 25
- WQZGKKKJIJFFOK-VFUOTHLCSA-N beta-D-glucose Chemical compound OC[C@H]1O[C@@H](O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-VFUOTHLCSA-N 0.000 claims abstract description 25
- 230000001131 transforming effect Effects 0.000 claims abstract description 25
- 239000000243 solution Substances 0.000 claims description 52
- 239000000047 product Substances 0.000 claims description 36
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 19
- 239000000203 mixture Substances 0.000 claims description 17
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 12
- 239000005862 Whey Substances 0.000 claims description 10
- 102000007544 Whey Proteins Human genes 0.000 claims description 10
- 108010046377 Whey Proteins Proteins 0.000 claims description 10
- 239000012466 permeate Substances 0.000 claims description 10
- 238000011282 treatment Methods 0.000 claims description 9
- 239000007864 aqueous solution Substances 0.000 claims description 6
- 229940005642 polystyrene sulfonic acid Drugs 0.000 claims description 5
- MIDXCONKKJTLDX-UHFFFAOYSA-N 3,5-dimethylcyclopentane-1,2-dione Chemical compound CC1CC(C)C(=O)C1=O MIDXCONKKJTLDX-UHFFFAOYSA-N 0.000 claims description 4
- 235000013736 caramel Nutrition 0.000 claims description 4
- 238000010438 heat treatment Methods 0.000 claims description 3
- 229920001467 poly(styrenesulfonates) Polymers 0.000 claims description 3
- 238000001816 cooling Methods 0.000 claims description 2
- 238000001704 evaporation Methods 0.000 claims 1
- 230000008020 evaporation Effects 0.000 claims 1
- 238000001914 filtration Methods 0.000 claims 1
- 230000003301 hydrolyzing effect Effects 0.000 abstract description 18
- XDIYNQZUNSSENW-NUVHGKSTSA-N (2r,3s,4s,5r)-2,3,4,5,6-pentahydroxyhexanal;(2r,3s,4r,5r)-2,3,4,5,6-pentahydroxyhexanal Chemical compound OC[C@@H](O)[C@H](O)[C@H](O)[C@@H](O)C=O.OC[C@@H](O)[C@@H](O)[C@H](O)[C@@H](O)C=O XDIYNQZUNSSENW-NUVHGKSTSA-N 0.000 abstract description 5
- 229960001375 lactose Drugs 0.000 description 109
- 150000002500 ions Chemical class 0.000 description 28
- 239000002253 acid Substances 0.000 description 12
- NWUYHJFMYQTDRP-UHFFFAOYSA-N 1,2-bis(ethenyl)benzene;1-ethenyl-2-ethylbenzene;styrene Chemical compound C=CC1=CC=CC=C1.CCC1=CC=CC=C1C=C.C=CC1=CC=CC=C1C=C NWUYHJFMYQTDRP-UHFFFAOYSA-N 0.000 description 8
- 239000003456 ion exchange resin Substances 0.000 description 8
- 229920003303 ion-exchange polymer Polymers 0.000 description 8
- 239000000843 powder Substances 0.000 description 8
- 239000011347 resin Substances 0.000 description 8
- 229920005989 resin Polymers 0.000 description 8
- 235000013351 cheese Nutrition 0.000 description 6
- MYRTYDVEIRVNKP-UHFFFAOYSA-N 1,2-Divinylbenzene Chemical compound C=CC1=CC=CC=C1C=C MYRTYDVEIRVNKP-UHFFFAOYSA-N 0.000 description 5
- 239000000796 flavoring agent Substances 0.000 description 5
- 235000019634 flavors Nutrition 0.000 description 5
- 238000003892 spreading Methods 0.000 description 5
- 235000019605 sweet taste sensations Nutrition 0.000 description 5
- 239000012467 final product Substances 0.000 description 4
- 235000013361 beverage Nutrition 0.000 description 3
- 238000005342 ion exchange Methods 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- 235000013405 beer Nutrition 0.000 description 2
- 238000005336 cracking Methods 0.000 description 2
- 235000013365 dairy product Nutrition 0.000 description 2
- 238000007210 heterogeneous catalysis Methods 0.000 description 2
- 235000015122 lemonade Nutrition 0.000 description 2
- 230000003204 osmotic effect Effects 0.000 description 2
- 230000001172 regenerating effect Effects 0.000 description 2
- 239000007858 starting material Substances 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- GUBGYTABKSRVRQ-XLOQQCSPSA-N Alpha-Lactose Chemical compound O[C@@H]1[C@@H](O)[C@@H](O)[C@@H](CO)O[C@H]1O[C@@H]1[C@@H](CO)O[C@H](O)[C@H](O)[C@H]1O GUBGYTABKSRVRQ-XLOQQCSPSA-N 0.000 description 1
- 240000002129 Malva sylvestris Species 0.000 description 1
- 235000006770 Malva sylvestris Nutrition 0.000 description 1
- 239000004793 Polystyrene Substances 0.000 description 1
- 235000015173 baked goods and baking mixes Nutrition 0.000 description 1
- 102000005936 beta-Galactosidase Human genes 0.000 description 1
- 108010005774 beta-Galactosidase Proteins 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 235000015155 buttermilk Nutrition 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 235000020186 condensed milk Nutrition 0.000 description 1
- 235000009508 confectionery Nutrition 0.000 description 1
- 239000006071 cream Substances 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 238000002425 crystallisation Methods 0.000 description 1
- 230000008025 crystallization Effects 0.000 description 1
- 235000015142 cultured sour cream Nutrition 0.000 description 1
- 230000009089 cytolysis Effects 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 235000015071 dressings Nutrition 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000011010 flushing procedure Methods 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- ZZUFCTLCJUWOSV-UHFFFAOYSA-N furosemide Chemical compound C1=C(Cl)C(S(=O)(=O)N)=CC(C(O)=O)=C1NCC1=CC=CO1 ZZUFCTLCJUWOSV-UHFFFAOYSA-N 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 235000015220 hamburgers Nutrition 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- -1 hydrogen ions Chemical class 0.000 description 1
- 235000015243 ice cream Nutrition 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 235000013372 meat Nutrition 0.000 description 1
- 230000002906 microbiologic effect Effects 0.000 description 1
- 235000012771 pancakes Nutrition 0.000 description 1
- 238000005498 polishing Methods 0.000 description 1
- 229920000172 poly(styrenesulfonic acid) Polymers 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 229920000136 polysorbate Polymers 0.000 description 1
- 229920002223 polystyrene Polymers 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 238000012552 review Methods 0.000 description 1
- 230000000630 rising effect Effects 0.000 description 1
- 229920006395 saturated elastomer Polymers 0.000 description 1
- 235000013580 sausages Nutrition 0.000 description 1
- 235000020183 skimmed milk Nutrition 0.000 description 1
- 235000014347 soups Nutrition 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 230000009466 transformation Effects 0.000 description 1
- 235000008939 whole milk Nutrition 0.000 description 1
- 235000013618 yogurt Nutrition 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13K—SACCHARIDES OBTAINED FROM NATURAL SOURCES OR BY HYDROLYSIS OF NATURALLY OCCURRING DISACCHARIDES, OLIGOSACCHARIDES OR POLYSACCHARIDES
- C13K13/00—Sugars not otherwise provided for in this class
-
- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13K—SACCHARIDES OBTAINED FROM NATURAL SOURCES OR BY HYDROLYSIS OF NATURALLY OCCURRING DISACCHARIDES, OLIGOSACCHARIDES OR POLYSACCHARIDES
- C13K1/00—Glucose; Glucose-containing syrups
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Emergency Medicine (AREA)
- General Health & Medical Sciences (AREA)
- Seasonings (AREA)
- Saccharide Compounds (AREA)
- Dairy Products (AREA)
Applications Claiming Priority (4)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US334,524 | 1981-12-22 | ||
| US33452481A | 1981-12-28 | 1981-12-28 | |
| SE8206009A SE452337B (sv) | 1981-12-28 | 1982-10-22 | Forfarande for framstellning av ett sotningsmedel genom hydrolys av en laktoslosning |
| SE8206009-6 | 1982-10-22 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CA1203115A true CA1203115A (en) | 1986-04-15 |
Family
ID=26658268
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA000417243A Expired CA1203115A (en) | 1981-12-22 | 1982-12-08 | Process for the manufacture of a sweetener based on milk and a sweetener manufactured according to the process |
Country Status (10)
| Country | Link |
|---|---|
| EP (1) | EP0083325B1 (es) |
| AU (1) | AU550326B2 (es) |
| CA (1) | CA1203115A (es) |
| DE (1) | DE3275349D1 (es) |
| ES (1) | ES517877A0 (es) |
| FI (1) | FI72147C (es) |
| IE (1) | IE53762B1 (es) |
| NO (1) | NO157507C (es) |
| NZ (1) | NZ202634A (es) |
| PT (1) | PT75963B (es) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| ES2415905T3 (es) | 2007-02-07 | 2013-07-29 | Kraft Foods R & D, Inc. | Procedimiento para producir suero en polvo modificado |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2592509A (en) * | 1950-07-13 | 1952-04-08 | Borden Co | Noncrystallizing lactose sirup and method of making |
| GB1539278A (en) * | 1977-11-17 | 1979-01-31 | Express Dairy Foods Co Ltd | Production of hydrolysed lactose from whey lactose and its use in brewing or other fermentation process |
| US4266027A (en) * | 1980-03-12 | 1981-05-05 | National Distillers And Chemical Corp. | Process for the hydrolysis of starch and fermentable hydrolysates obtained therefrom |
-
1982
- 1982-11-18 EP EP82850235A patent/EP0083325B1/en not_active Expired
- 1982-11-18 DE DE8282850235T patent/DE3275349D1/de not_active Expired
- 1982-11-22 IE IE2776/82A patent/IE53762B1/en unknown
- 1982-11-26 NZ NZ202634A patent/NZ202634A/en unknown
- 1982-12-02 ES ES82517877A patent/ES517877A0/es active Granted
- 1982-12-08 CA CA000417243A patent/CA1203115A/en not_active Expired
- 1982-12-09 PT PT75963A patent/PT75963B/pt unknown
- 1982-12-21 AU AU91818/82A patent/AU550326B2/en not_active Ceased
- 1982-12-21 NO NO82824301A patent/NO157507C/no unknown
- 1982-12-21 FI FI824400A patent/FI72147C/fi not_active IP Right Cessation
Also Published As
| Publication number | Publication date |
|---|---|
| FI72147C (fi) | 1987-04-13 |
| AU550326B2 (en) | 1986-03-20 |
| NO824301L (no) | 1983-06-23 |
| IE53762B1 (en) | 1989-02-01 |
| EP0083325A3 (en) | 1984-11-28 |
| EP0083325A2 (en) | 1983-07-06 |
| ES8307900A1 (es) | 1983-08-16 |
| DE3275349D1 (en) | 1987-03-12 |
| FI824400L (fi) | 1983-06-29 |
| NO157507C (no) | 1988-04-06 |
| PT75963A (en) | 1983-01-01 |
| ES517877A0 (es) | 1983-08-16 |
| PT75963B (en) | 1985-10-04 |
| NZ202634A (en) | 1986-02-21 |
| EP0083325B1 (en) | 1987-02-04 |
| FI824400A0 (fi) | 1982-12-21 |
| IE822776L (en) | 1983-06-22 |
| NO157507B (no) | 1987-12-21 |
| FI72147B (fi) | 1986-12-31 |
| AU9181882A (en) | 1983-06-30 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| MKEX | Expiry |