BRPI0618068A2 - método de cloração de sacarose-6-éster para produzir 6' , 4, 1' -tricloro-sacarose-6-ésteres - Google Patents
método de cloração de sacarose-6-éster para produzir 6' , 4, 1' -tricloro-sacarose-6-ésteresInfo
- Publication number
- BRPI0618068A2 BRPI0618068A2 BRPI0618068A BRPI0618068A BRPI0618068A2 BR PI0618068 A2 BRPI0618068 A2 BR PI0618068A2 BR PI0618068 A BRPI0618068 A BR PI0618068A BR PI0618068 A BRPI0618068 A BR PI0618068A BR PI0618068 A2 BRPI0618068 A2 BR PI0618068A2
- Authority
- BR
- Brazil
- Prior art keywords
- sucrose
- trichloro
- esters
- produce
- chlorination method
- Prior art date
Links
- 238000005660 chlorination reaction Methods 0.000 title 1
- 238000000034 method Methods 0.000 title 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
- C07H13/00—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids
- C07H13/02—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids by carboxylic acids
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
- C07H13/00—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
- C07H13/00—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids
- C07H13/02—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids by carboxylic acids
- C07H13/04—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids by carboxylic acids having the esterifying carboxyl radicals attached to acyclic carbon atoms
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Biochemistry (AREA)
- Biotechnology (AREA)
- General Health & Medical Sciences (AREA)
- Genetics & Genomics (AREA)
- Molecular Biology (AREA)
- Saccharide Compounds (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US73242105P | 2005-10-31 | 2005-10-31 | |
| US11/554,398 US20070100139A1 (en) | 2005-10-31 | 2006-10-30 | Methods for chlorinating sucrose-6-ester |
| PCT/US2006/042448 WO2007053604A2 (en) | 2005-10-31 | 2006-10-31 | Methods for chlorinating sucrose-6-ester |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| BRPI0618068A2 true BRPI0618068A2 (pt) | 2016-09-13 |
Family
ID=38007056
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| BRPI0618068A BRPI0618068A2 (pt) | 2005-10-31 | 2006-10-31 | método de cloração de sacarose-6-éster para produzir 6' , 4, 1' -tricloro-sacarose-6-ésteres |
Country Status (9)
| Country | Link |
|---|---|
| US (1) | US20070100139A1 (pt) |
| EP (1) | EP1945707A2 (pt) |
| JP (1) | JP2009513673A (pt) |
| KR (1) | KR20080064885A (pt) |
| CN (1) | CN101331181A (pt) |
| AU (1) | AU2006308897A1 (pt) |
| BR (1) | BRPI0618068A2 (pt) |
| CA (1) | CA2627416A1 (pt) |
| WO (1) | WO2007053604A2 (pt) |
Families Citing this family (24)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20080300401A1 (en) * | 2007-06-04 | 2008-12-04 | Polymed Therapeutics, Inc. | Novel chlorination process for preparing sucralose |
| AR070082A1 (es) * | 2008-01-04 | 2010-03-10 | Tate & Lyle Technology Ltd | Metodo para la produccion de sucralosa |
| WO2009117317A1 (en) * | 2008-03-20 | 2009-09-24 | Tate & Lyle Technology Ltd | Removal of acids from tertiary amide solvents |
| US8436157B2 (en) | 2008-03-26 | 2013-05-07 | Tate & Lyle Technology Limited | Method for the production of sucralose |
| US8497367B2 (en) * | 2008-04-03 | 2013-07-30 | Tate & Lyle Technology Limited | Sucralose purification process |
| WO2009124113A1 (en) * | 2008-04-03 | 2009-10-08 | Tate & Lyle Technology Ltd. | Extraction of less polar impurities from sucralose containing aqueous feed streams |
| US8212022B2 (en) * | 2008-04-03 | 2012-07-03 | Tate & Lyle Technology Limited | Effect of carbohydrate concentration on sucralose extraction efficiency |
| AR071134A1 (es) * | 2008-04-03 | 2010-05-26 | Tate & Lyle Technology Ltd | Cristalizacion de sucralosa a partir de chorros que contienen sucralosa |
| GB2468936B (en) | 2009-03-27 | 2011-09-07 | Mohamad Rami Radwan Jaber | Chlorination of sucrose-6-esters |
| GB2469157B (en) | 2009-03-30 | 2011-07-06 | John Kerr | Process for removing dimethylamine during sucralose production |
| GB2469158B (en) | 2009-03-31 | 2011-09-28 | Peter J Seaberg | Base-assisted formation of tin-sucrose adducts |
| GB2471348B (en) | 2009-06-22 | 2011-12-14 | Tate & Lyle Technology Ltd | A method for producing sucralose-6-acylate |
| GB2474310B (en) | 2009-10-12 | 2012-02-29 | Tate & Lyle Technology Ltd | Process for the production of sucrose-6-ester |
| GB2474311B (en) * | 2009-10-12 | 2012-10-17 | Tate & Lyle Technology Ltd | Low temperature, single solvent process for the production of sucrose-6-ester |
| CN103298824B (zh) | 2010-11-23 | 2016-10-12 | 列克星敦制药实验室 | 碳水化合物的低温氯化 |
| GB201110520D0 (en) | 2011-05-10 | 2011-08-03 | Tate & Lyle Technology Ltd | Extraction of carboxylic acids with tin compounds |
| HUE027876T2 (en) | 2011-10-14 | 2016-10-28 | Lexington Pharmaceuticals Laboratories Llc | Carbohydrate chlorination and carbohydrate derivatives |
| CN105829332B (zh) | 2013-12-16 | 2018-10-02 | 塔特和莱利技术有限公司 | 蔗糖-6-酯的氯化 |
| CN105273095A (zh) * | 2014-05-28 | 2016-01-27 | 四川海思科制药有限公司 | 一种舒更葡糖钠及其中间体的制备方法 |
| GB2544217B (en) | 2014-08-08 | 2020-03-25 | Tate & Lyle Tech Ltd | Chlorination of sucrose-6-esters |
| GB2536480B (en) | 2015-03-17 | 2019-09-04 | Tate & Lyle Tech Ltd | DMF Distillation |
| CN105131050B (zh) * | 2015-07-22 | 2018-07-31 | 青岛科技大学 | 一种氯化剂的制备方法及其制备三氯蔗糖的方法 |
| GB2551591B (en) | 2016-06-23 | 2019-08-07 | Tate & Lyle Tech Ltd | Liquid-liquid extraction of DMF |
| CN114146673A (zh) * | 2021-12-20 | 2022-03-08 | 安徽金禾实业股份有限公司 | 一种三氯蔗糖生产中连续中和的装置及方法 |
Family Cites Families (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4117224A (en) * | 1974-10-15 | 1978-09-26 | Tate & Lyle Limited | Preparation of sucrose 6,6'-dichloro hexa-acetate |
| US4435440A (en) * | 1976-01-08 | 1984-03-06 | Tate & Lyle Limited | Sweeteners |
| ATE732T1 (de) * | 1978-10-18 | 1982-03-15 | Tate & Lyle Patent Holdings Limited | Verfahren zur herstellung von 2-chlor-2-deoxy-sacchariden und einige 2-chlor-2-deoxy-saccharide. |
| US4324888A (en) * | 1979-03-09 | 1982-04-13 | Talres Development (N.A.) N.V. | Process for the preparation of chlorodeoxysugars |
| EP0031651B1 (en) * | 1979-12-20 | 1983-03-23 | TATE & LYLE PUBLIC LIMITED COMPANY | Process for the preparation of 4,1',6'-trichloro-4,1',6'-trideoxy-galactosucrose |
| US4291158A (en) * | 1980-01-28 | 1981-09-22 | Velsicol Chemical Corporation | Sucrose ester of 2-methoxy-3,6-dichlorobenzoic acid |
| EP0043649B1 (en) * | 1980-07-08 | 1984-09-12 | TATE & LYLE PUBLIC LIMITED COMPANY | Process for the preparation of 4, 1',6'-trichloro-4,1',6'-trideoxygalactosucrose (tgs) |
| CA1183133A (en) * | 1980-10-28 | 1985-02-26 | Tate & Lyle Public Limited Company | Sweet chlorine-substituted disaccharides |
| CA1213887A (en) * | 1982-09-13 | 1986-11-12 | Riaz A. Khan | Sucrose derivative |
| US4439596A (en) * | 1983-03-21 | 1984-03-27 | E. I. Du Pont De Nemours And Company | Chlorination of hydroquinone |
| GB8316790D0 (en) * | 1983-06-21 | 1983-07-27 | Tate & Lyle Plc | Chemical process |
| US4980463A (en) * | 1989-07-18 | 1990-12-25 | Noramco, Inc. | Sucrose-6-ester chlorination |
| US5136031A (en) * | 1990-07-09 | 1992-08-04 | Tate & Lyle Public Limited Company | Chlorination of sugars |
| US5498709A (en) * | 1994-10-17 | 1996-03-12 | Mcneil-Ppc, Inc. | Production of sucralose without intermediate isolation of crystalline sucralose-6-ester |
| US20060276639A1 (en) * | 2005-06-01 | 2006-12-07 | Healthy Brands, Llc | Conversion of sucralose-6-ester to sucralose |
-
2006
- 2006-10-30 US US11/554,398 patent/US20070100139A1/en not_active Abandoned
- 2006-10-31 BR BRPI0618068A patent/BRPI0618068A2/pt not_active IP Right Cessation
- 2006-10-31 CN CNA2006800401072A patent/CN101331181A/zh active Pending
- 2006-10-31 WO PCT/US2006/042448 patent/WO2007053604A2/en not_active Ceased
- 2006-10-31 CA CA002627416A patent/CA2627416A1/en not_active Abandoned
- 2006-10-31 JP JP2008538104A patent/JP2009513673A/ja not_active Withdrawn
- 2006-10-31 AU AU2006308897A patent/AU2006308897A1/en not_active Abandoned
- 2006-10-31 EP EP06827156A patent/EP1945707A2/en not_active Withdrawn
- 2006-10-31 KR KR1020087012285A patent/KR20080064885A/ko not_active Withdrawn
Also Published As
| Publication number | Publication date |
|---|---|
| WO2007053604A3 (en) | 2007-11-29 |
| KR20080064885A (ko) | 2008-07-09 |
| JP2009513673A (ja) | 2009-04-02 |
| CN101331181A (zh) | 2008-12-24 |
| AU2006308897A1 (en) | 2007-05-10 |
| US20070100139A1 (en) | 2007-05-03 |
| CA2627416A1 (en) | 2007-05-10 |
| EP1945707A2 (en) | 2008-07-23 |
| WO2007053604A2 (en) | 2007-05-10 |
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Legal Events
| Date | Code | Title | Description |
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| B06G | Technical and formal requirements: other requirements [chapter 6.7 patent gazette] |
Free format text: SOLICITA-SE A REGULARIZACAO DA PROCURACAO, UMA VEZ QUE BASEADO NO ARTIGO 216 PAR 1O DA LPI, O DOCUMENTO DE PROCURACAO DEVE SER APRESENTADO NO ORIGINAL, TRASLADO OU FOTOCOPIA AUTENTICADA. |
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| B11Z | Dismissal: petition dismissal - article 216, par 2 of industrial property law |
Free format text: REFERENTE A PETICAO NO 20080064056/RJ DE 29/04/2008. |
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| B11M | Decision cancelled [chapter 11.13 patent gazette] |
Free format text: O DESPACHO 11.6.1 ESTA SENDO ANULADO TENDO POR BASE A DETERMINACAO DO DIRETOR DE PATENTES, A QUAL E CALCADA NO PARECER NO 0003-2014 AGU/PGF/PFE/INPI/COOPHI-LBC-1.0. |
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| B06H | Technical and formal requirements: requirement cancelled [chapter 6.8 patent gazette] |
Free format text: O DESPACHO 6.7 ESTA SENDO ANULADO TENDO POR BASE A DETERMINACAO DO DIRETOR DE PATENTES, A QUAL E CALCADA NO PARECER NO 0003-2014 AGU/PGF/PFE/INPI/COOPHI-LBC-1.0. |
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| B08F | Application dismissed because of non-payment of annual fees [chapter 8.6 patent gazette] |
Free format text: REFERENTE AS 6A, 7A, 8A, 9A E 10A ANUIDADES. |
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| B08K | Patent lapsed as no evidence of payment of the annual fee has been furnished to inpi [chapter 8.11 patent gazette] |