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BRPI0409316A - processos para a retirada de água de ácido cianìdrico por destilação e para a hidrocianação de olefinas ou dienos - Google Patents

processos para a retirada de água de ácido cianìdrico por destilação e para a hidrocianação de olefinas ou dienos

Info

Publication number
BRPI0409316A
BRPI0409316A BRPI0409316-0A BRPI0409316A BRPI0409316A BR PI0409316 A BRPI0409316 A BR PI0409316A BR PI0409316 A BRPI0409316 A BR PI0409316A BR PI0409316 A BRPI0409316 A BR PI0409316A
Authority
BR
Brazil
Prior art keywords
distilling
dienes
olefins
acid water
hydrocyanation
Prior art date
Application number
BRPI0409316-0A
Other languages
English (en)
Inventor
Michael Bartsch
Robert Baumann
Gerd Haderlein
Miguel Angel Flores
Tim Jungkamp
Hermann Luyken
Jens Scheidel
Wolfgang Siegel
Dagmar Pascale Kunsmann-Keitel
Peter Bassler
Original Assignee
Basf Ag
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=33154295&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=BRPI0409316(A) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by Basf Ag filed Critical Basf Ag
Publication of BRPI0409316A publication Critical patent/BRPI0409316A/pt
Publication of BRPI0409316B1 publication Critical patent/BRPI0409316B1/pt

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01C—AMMONIA; CYANOGEN; COMPOUNDS THEREOF
    • C01C3/00—Cyanogen; Compounds thereof
    • C01C3/02—Preparation, separation or purification of hydrogen cyanide
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C253/00—Preparation of carboxylic acid nitriles
    • C07C253/08—Preparation of carboxylic acid nitriles by addition of hydrogen cyanide or salts thereof to unsaturated compounds
    • C07C253/10—Preparation of carboxylic acid nitriles by addition of hydrogen cyanide or salts thereof to unsaturated compounds to compounds containing carbon-to-carbon double bonds
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01C—AMMONIA; CYANOGEN; COMPOUNDS THEREOF
    • C01C3/00—Cyanogen; Compounds thereof
    • C01C3/02—Preparation, separation or purification of hydrogen cyanide
    • C01C3/0295—Purification
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01C—AMMONIA; CYANOGEN; COMPOUNDS THEREOF
    • C01C3/00—Cyanogen; Compounds thereof
    • C01C3/06—Stabilisation of hydrogen cyanide
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00105—Controlling the temperature by indirect heating or cooling employing heat exchange fluids part or all of the reactants being heated or cooled outside the reactor while recycling
    • B01J2219/0011—Controlling the temperature by indirect heating or cooling employing heat exchange fluids part or all of the reactants being heated or cooled outside the reactor while recycling involving reactant liquids

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Toxicology (AREA)
  • General Health & Medical Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)

Abstract

"PROCESSOS PARA A RETIRADA DE áGUA DE áCIDO CIANìDRICO POR DESTILAçãO E PARA A HIDROCIANAçãO DE OLEFINAS OU DIENOS". A invenção refere-se a um processo para a retirada de água de ácido cianídrico por destilação, que compreende a destilação de ácido cianídrico bruto contendo de 50 a 99,9% em peso de HCN, de 0,1 a 40% em peso de água, de 0 a 15% em peso de óxidos de carbono e opcionalmente de 0,01 a 1% em peso de um estabilizante não volátil, em uma pressão de 1 bar a 2,5 bar, uma temperatura de fundo de 100<198>C a 130<198>C e uma temperatura de topo de 25<198>C a 54<198>C, na ausência de um estabilizante volátil, em uma coluna de destilação para obter uma corrente de retirada de topo contendo ácido cianídrico anidro purificado e óxidos de carbono e uma corrente de retirada de fundo compreendendo água e, quando apropriado, o estabilizante não volátil.
BRPI0409316-0B1A 2003-04-17 2004-04-15 Processos para a retirada de água de ácido cianídrico por destilação e para a hidrocianação de olefinas ou dienos BRPI0409316B1 (pt)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE10317929A DE10317929A1 (de) 2003-04-17 2003-04-17 Verfahren zur Aufreinigung von Blausäure
PCT/EP2004/003973 WO2004092068A1 (de) 2003-04-17 2004-04-15 Verfahren zur aufreinigung von blausäure

Publications (2)

Publication Number Publication Date
BRPI0409316A true BRPI0409316A (pt) 2006-04-25
BRPI0409316B1 BRPI0409316B1 (pt) 2013-10-15

Family

ID=33154295

Family Applications (1)

Application Number Title Priority Date Filing Date
BRPI0409316-0B1A BRPI0409316B1 (pt) 2003-04-17 2004-04-15 Processos para a retirada de água de ácido cianídrico por destilação e para a hidrocianação de olefinas ou dienos

Country Status (16)

Country Link
US (1) US7462263B2 (pt)
EP (1) EP1618068B1 (pt)
JP (1) JP4406635B2 (pt)
KR (1) KR101093377B1 (pt)
CN (1) CN100340487C (pt)
AR (1) AR044023A1 (pt)
AT (1) ATE336464T1 (pt)
BR (1) BRPI0409316B1 (pt)
CA (1) CA2522520C (pt)
DE (2) DE10317929A1 (pt)
ES (1) ES2270376T3 (pt)
MX (1) MXPA05010572A (pt)
MY (1) MY138553A (pt)
PL (1) PL1618068T3 (pt)
TW (1) TW200505792A (pt)
WO (1) WO2004092068A1 (pt)

Families Citing this family (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102009001699A1 (de) 2008-03-26 2009-10-15 Basf Se Verfahren zur Erhöhung der Verfügbarkeit von Anlagen, in denen Blausäure gehandhabt wird
JP5770279B2 (ja) 2010-07-07 2015-08-26 インヴィスタ テクノロジーズ エスアエルエル ニトリルの製造方法
WO2014099600A1 (en) * 2012-12-18 2014-06-26 Invista North America S.A.R.L. Process for heat recovery from ammonia stripper in adrussow process
JP2016508522A (ja) * 2013-02-28 2016-03-22 ビーエーエスエフ ソシエタス・ヨーロピアＢａｓｆ Ｓｅ Ｓｏ２不含のシアン化水素を使用したｅｄａの製造法
WO2015135971A1 (de) 2014-03-13 2015-09-17 Basf Se Verfahren zur destillativen reinigung von eda
CN104724725B (zh) * 2014-11-21 2017-05-24 重庆紫光化工股份有限公司 氢氰酸气体分离纯化系统及方法
EP3322672B1 (en) * 2015-07-14 2020-05-27 The Chemours Company FC, LLC Method for removing nitriles from hydrogen cyanide
CN105366692B (zh) * 2015-12-04 2018-03-30 中国天辰工程有限公司 一种制取高纯液态氰化氢工艺及系统
CN106365178B (zh) * 2016-08-29 2018-07-27 重庆紫光化工股份有限公司 一种氢氰酸的提纯方法
CN106495186A (zh) * 2016-11-02 2017-03-15 中国天辰工程有限公司 一种高效回收氰化氢的方法
EP3604222A1 (en) * 2018-07-30 2020-02-05 Evonik Operations GmbH Process for the purification of hydrogen cyanide
CN110627091A (zh) * 2019-10-24 2019-12-31 重庆工商大学 一种采用化学法提纯用于制备己二腈的氢氰酸的方法
TW202335966A (zh) 2021-10-29 2023-09-16 德商羅伊姆公司 生產及分離氰化氫之最佳化方法以及將其轉化為甲基丙烯酸（ｍａｓ）及／或甲基丙烯酸烷酯之方法
CN114618181B (zh) * 2022-03-17 2023-12-08 北京道思克矿山装备技术有限公司 一种戊烯腈合成反应中回收氢氰酸的系统和方法

Family Cites Families (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US1934838A (en) * 1930-04-14 1933-11-14 Ig Farbenindustrie Ag Production of hydrocyanic acid
US2571099A (en) * 1950-01-07 1951-10-16 Du Pont Process for hydrocyanation of conjugated diolefinic compounds
NL302210A (pt) * 1963-01-16
FR1377939A (fr) * 1963-01-16 1964-11-06 Knapsack Ag Procédé pour la séparation de l'acrylonitrile et de l'acide cyanhydrique à partir de mélanges par distillation
DE1205064B (de) * 1963-05-04 1965-11-18 Basf Ag Verfahren und Vorrichtung zur Gewinnung von weitgehend wasserfreier Blausaeure durch Destillation von blausaeure- und wasserhaltigen Gasen oder Fluessigkeiten
US3357900A (en) * 1965-05-17 1967-12-12 American Cyanamid Co Series flash distillation for recovery of hcn from aqueous cu-containing slurries
FR2198895B1 (pt) * 1972-09-07 1977-02-25 Du Pont
US3920721A (en) * 1974-09-18 1975-11-18 Du Pont Hydrocyanation of olefins
DE3334321A1 (de) * 1983-09-22 1985-04-11 Lentia GmbH Chem. u. pharm. Erzeugnisse - Industriebedarf, 8000 München Verfahren zur reinigung von rohem acetonitril unter gewinnung von reiner blausaeure
EP0912444A1 (en) * 1996-05-30 1999-05-06 E.I. Du Pont De Nemours And Company An improved process for preparing anhydrous hcn
DE69708431T2 (de) * 1996-09-25 2002-05-02 Mitsubishi Rayon Co., Ltd. Verfahren zur Ammoxydierung in einem Wirbelschichtreaktor
DE19647527C1 (de) * 1996-11-16 1998-03-12 Degussa Verfahren zur Herstellung von Cyanoverbindungen durch Ammonoxidation
DE10034193A1 (de) * 2000-07-13 2002-03-28 Roehm Gmbh Verfahren zur Herstellung von Cyanwasserstoff

Also Published As

Publication number Publication date
KR101093377B1 (ko) 2011-12-14
EP1618068B1 (de) 2006-08-16
EP1618068A1 (de) 2006-01-25
JP2006523590A (ja) 2006-10-19
DE502004001216D1 (de) 2006-09-28
AR044023A1 (es) 2005-08-24
TW200505792A (en) 2005-02-16
MXPA05010572A (es) 2005-11-23
CA2522520A1 (en) 2004-10-28
WO2004092068A1 (de) 2004-10-28
DE10317929A1 (de) 2004-11-11
CA2522520C (en) 2011-11-08
CN1771197A (zh) 2006-05-10
ES2270376T3 (es) 2007-04-01
PL1618068T3 (pl) 2006-12-29
ATE336464T1 (de) 2006-09-15
MY138553A (en) 2009-06-30
US7462263B2 (en) 2008-12-09
US20060201798A1 (en) 2006-09-14
JP4406635B2 (ja) 2010-02-03
KR20050120801A (ko) 2005-12-23
BRPI0409316B1 (pt) 2013-10-15
CN100340487C (zh) 2007-10-03

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Legal Events

Date Code Title Description
B06A Patent application procedure suspended [chapter 6.1 patent gazette]
B06A Patent application procedure suspended [chapter 6.1 patent gazette]
B07A Application suspended after technical examination (opinion) [chapter 7.1 patent gazette]
B09A Decision: intention to grant [chapter 9.1 patent gazette]
B07B Technical examination (opinion): publication cancelled [chapter 7.2 patent gazette]

Free format text: ANULADA A PUBLICACAO DO ITEM 7.1 DA RPI 2222 DE 06/08/2013 POR TER SIDO INDEVIDA.

B16A Patent or certificate of addition of invention granted [chapter 16.1 patent gazette]

Free format text: PRAZO DE VALIDADE: 20 (VINTE) ANOS CONTADOS A PARTIR DE 15/04/2004, OBSERVADAS AS CONDICOES LEGAIS.

B21F Lapse acc. art. 78, item iv - on non-payment of the annual fees in time

Free format text: REFERENTE A 11A ANUIDADE.

B24J Lapse because of non-payment of annual fees (definitively: art 78 iv lpi, resolution 113/2013 art. 12)

Free format text: EM VIRTUDE DA EXTINCAO PUBLICADA NA RPI 2343 DE 01-12-2015 E CONSIDERANDO AUSENCIA DE MANIFESTACAO DENTRO DOS PRAZOS LEGAIS, INFORMO QUE CABE SER MANTIDA A EXTINCAO DA PATENTE E SEUS CERTIFICADOS, CONFORME O DISPOSTO NO ARTIGO 12, DA RESOLUCAO 113/2013.