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BR9811450A - Processos para a condensação fracionada de uma mistura gasosa e para a preparação de ácido acrìlico ou ácido metacrìlico - Google Patents

Processos para a condensação fracionada de uma mistura gasosa e para a preparação de ácido acrìlico ou ácido metacrìlico

Info

Publication number
BR9811450A
BR9811450A BR9811450-6A BR9811450A BR9811450A BR 9811450 A BR9811450 A BR 9811450A BR 9811450 A BR9811450 A BR 9811450A BR 9811450 A BR9811450 A BR 9811450A
Authority
BR
Brazil
Prior art keywords
gas mixture
processes
preparation
fractional condensation
acrylic acid
Prior art date
Application number
BR9811450-6A
Other languages
English (en)
Other versions
BR9811450B1 (pt
Inventor
Bernd Eck
Otto Machhammer
Theo Proll
Volker Schliephake
Joachim Thiel
Klaus Br Llos
Original Assignee
Basf Ag
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Basf Ag filed Critical Basf Ag
Publication of BR9811450A publication Critical patent/BR9811450A/pt
Publication of BR9811450B1 publication Critical patent/BR9811450B1/pt

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C57/00Unsaturated compounds having carboxyl groups bound to acyclic carbon atoms
    • C07C57/02Unsaturated compounds having carboxyl groups bound to acyclic carbon atoms with only carbon-to-carbon double bonds as unsaturation
    • C07C57/03Monocarboxylic acids
    • C07C57/04Acrylic acid; Methacrylic acid
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D5/00Condensation of vapours; Recovering volatile solvents by condensation
    • B01D5/0027Condensation of vapours; Recovering volatile solvents by condensation by direct contact between vapours or gases and the cooling medium
    • B01D5/003Condensation of vapours; Recovering volatile solvents by condensation by direct contact between vapours or gases and the cooling medium within column(s)
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42Separation; Purification; Stabilisation; Use of additives
    • C07C51/43Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
    • C07C51/44Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation by distillation

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Connection Of Motors, Electrical Generators, Mechanical Devices, And The Like (AREA)

Abstract

"PROCESSOS PARA A CONDENSAçãO FRACIONADA DE UMA MISTURA GASOSA E PARA A PREPARAçãO DE áCIDO ACRìLICO OU áCIDO METACRìLICO" A invenção refere-se a um processo para a condensação fracionada de uma mistura gasosa, que contém pelo menos um outro constituinte condensável, em adição ao ácido acrílico ou ácido metacrílico, e que possui também uma alta proporção de um ou mais constituintes não condensáveis. De acordo com o referido processo, a mistura gasosa é passada através de um coluna com chicanas eficientes para a separação e os constituintes condensáveis são condensados por resfriamento.
BRPI9811450-6A 1997-09-12 1998-09-10 processo para a preparação de ácido acrìlico ou ácido metacrìlico por oxidação catalìtica em fase gasosa. BR9811450B1 (pt)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
DE19740253.4 1997-09-12
DE19740253A DE19740253A1 (de) 1997-09-12 1997-09-12 Verfahren zur fraktionierten Kondensation eines heißen Gasgemisches mit einem hohen Anteil nicht kondensierbarer Komponenten
PCT/EP1998/005779 WO1999014182A1 (de) 1997-09-12 1998-09-10 Verfahren zur fraktionierten kondensation eines acrylsäure oder methacrylsäure enthaltenden heissen gasgemisches mit einem hohen anteil nicht kondensierbarer komponenten

Publications (2)

Publication Number Publication Date
BR9811450A true BR9811450A (pt) 2000-08-15
BR9811450B1 BR9811450B1 (pt) 2011-06-28

Family

ID=7842221

Family Applications (1)

Application Number Title Priority Date Filing Date
BRPI9811450-6A BR9811450B1 (pt) 1997-09-12 1998-09-10 processo para a preparação de ácido acrìlico ou ácido metacrìlico por oxidação catalìtica em fase gasosa.

Country Status (14)

Country Link
US (1) US6646161B1 (pt)
EP (1) EP1015411B1 (pt)
JP (1) JP4215388B2 (pt)
KR (1) KR100603875B1 (pt)
CN (1) CN1092636C (pt)
AU (1) AU9624998A (pt)
BR (1) BR9811450B1 (pt)
CA (1) CA2303373A1 (pt)
CZ (1) CZ297503B6 (pt)
DE (2) DE19740253A1 (pt)
ES (1) ES2201539T3 (pt)
MY (1) MY119650A (pt)
TW (1) TW431905B (pt)
WO (1) WO1999014182A1 (pt)

Families Citing this family (63)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE19814375A1 (de) * 1998-03-31 1999-10-07 Basf Ag Verfahren zur Herstellung von Acrylsäure und Acrylsäureestern
DE19814387A1 (de) * 1998-03-31 1999-10-07 Basf Ag Verfahren zur Herstellung von Acrylsäure und Acrylsäureestern
US6498272B1 (en) 1999-03-06 2002-12-24 Basf Aktiengesellschaft Method for producing acrylic acid
MY122671A (en) 1999-03-06 2006-04-29 Basf Ag Fractional condensation of a product gas mixture containing acrylic acid
DE60133473T2 (de) 2001-12-14 2009-05-20 Evonik Stockhausen Gmbh Verfahren zur Herstellung von Acrylsäure
MY135762A (en) * 2002-01-09 2008-06-30 Basf Ag Method for producing acrylic acid
DE10220494A1 (de) 2002-05-07 2003-11-20 Basf Ag Verfahren zur Herstellung einer wässrigen Alkaliacrylat-Lösung
BRPI0413297B1 (pt) 2003-08-06 2014-01-21 Processo para operar uma oxidação parcial contínua em fase gasosa catalisada de maneira heterogênea de pelo menos um composto orgânico
JP2005234834A (ja) * 2004-02-19 2005-09-02 Hitachi Ltd 論理ボリュームの再配置方法
DE102004021764A1 (de) * 2004-04-30 2005-06-02 Basf Ag Verfahren zur Herstellung von Acrylsäure durch heterogen katalysierte Gasphasenpartialoxidation wenigstens einer C3-Kohlenwasserstoffvorläuferverbindung
US7592483B2 (en) 2004-07-01 2009-09-22 Basf Aktiengesellschaft Preparation of acrolein or acrylic acid or a mixture thereof by heterogeneously catalyzed partial gas phase oxidation of propylene
DE102004055765A1 (de) * 2004-11-18 2006-05-24 Basf Ag Verfahren zur Herstellung wasserabsorbierender Polymere
US7601866B2 (en) 2005-03-01 2009-10-13 Basf Aktiengesellschaft Process for removing methacrolein from liquid phase comprising acrylic acid as a main constituent and target product, and methacrolein as a secondary component
US7705181B2 (en) 2005-03-01 2010-04-27 Basf Akiengesellschaft Process for removing methacrylic acid from liquid phase comprising acrylic acid as a main constituent and target product, and methacrylic acid as a secondary component
DE102005018702A1 (de) 2005-04-21 2006-10-26 Basf Ag Verfahren zur Regelung einer hydraulischen Waschkolonne
DE102005019911A1 (de) 2005-04-27 2006-11-02 Basf Ag Verfahren der rektifikativen Auftrennung einer Acrylsäure und/oder Methacrylsäure enthaltenden Flüssigkeit
KR100999428B1 (ko) * 2006-01-20 2010-12-09 니폰 쇼쿠바이 컴파니 리미티드 (메타)아크릴산의 제조 방법
JP5368673B2 (ja) * 2006-01-20 2013-12-18 株式会社日本触媒 (メタ)アクリル酸の製造方法
WO2008033687A2 (en) 2006-09-15 2008-03-20 Dow Global Technologies Inc. Process for producing acrylic acid
DE102007055086A1 (de) 2007-11-16 2009-05-20 Basf Se Verfahren zur Herstellung von Acrylsäure
JP5489726B2 (ja) * 2007-01-26 2014-05-14 ビーエーエスエフ ソシエタス・ヨーロピア アクリル酸の製造方法
WO2008090190A1 (de) * 2007-01-26 2008-07-31 Basf Se Verfahren zur herstellung von acrylsäure
DE102007004960A1 (de) 2007-01-26 2008-07-31 Basf Se Verfahren zur Herstellung von Acrylsäure
DE102007043758A1 (de) 2007-09-13 2008-10-23 Basf Se Verfahren zum Betreiben einer kontinuierlichen Abtrennung eines Zielproduktes X in Form von feinteiligem Kristallisat des Zielproduktes X
BE1018537A3 (fr) 2007-09-13 2011-03-01 Basf Se Procede d'exploitation d'une separation en continu d'un produit cible x sous la forme d'un cristallisat finement divise.
DE102007043748A1 (de) 2007-09-13 2008-09-11 Basf Se Verfahren zur kontinuierlichen Abtrennung eines Zielproduktes X in Form von feinteiligem Kristallisat
JP5380434B2 (ja) 2008-04-27 2014-01-08 株式会社日本触媒 アクリル酸の製造方法ならびにその製造方法を用いた親水性樹脂の製造方法および吸水性樹脂の製造方法
JP5507111B2 (ja) * 2008-05-30 2014-05-28 ローム アンド ハース カンパニー 水性(メタ)アクリル酸の製造方法
EP2135656A1 (en) * 2008-05-30 2009-12-23 Rohm and Haas Company Method for production of purified (Meth)acrylic acid
EP2334631B1 (de) 2008-07-28 2017-03-01 Basf Se Verfahren zur auftrennung von in einem produktgasgemisch einer partiellen heterogen katalysierten gasphasenoxidation einer c3-vorläuferverbinding der acrylsäure als hauptbestandteil enthaltener acrylsäure und als nebenprodukt enthaltenem glyoxal
DE102008040799A1 (de) 2008-07-28 2008-12-11 Basf Se Verfahren zur Auftrennung von in einem Produktgasgemisch einer partiellen heterogen katalysierten Gasphasenoxidation einer C3-Vorläuferverbindung der Acrylsäure als Hauptbestandteil enthaltener Acrylsäure und als Nebenprodukt enthaltenem Glyoxal
DE102008041573A1 (de) 2008-08-26 2010-03-04 Basf Se Verfahren zur Auftrennung von in einem Produktgasgemisch einer partiellen heterogen katalysierten Gasphasenoxidation einer C3-Vorläuferverbindung der Acrylsäure als Hauptbestandteil enhaltener Acrylsäure und als Nebenprodukt enthaltenem Glyoxal
KR101994630B1 (ko) 2008-10-01 2019-07-02 알케마 인코포레이티드 온라인 근적외선 분석을 이용한 (메트)아크릴산 정제 방법의 제어
WO2011017172A2 (en) * 2009-07-28 2011-02-10 Joule Unlimited, Inc. Fractional condensation processes, apparatuses and systems
DE102010042216A1 (de) 2010-10-08 2011-06-09 Basf Se Verfahren zur Hemmung der unerwünschten radikalischen Polymerisation von in einer flüssigen Phase P befindlicher Acrylsäure
DE102011076931A1 (de) 2011-06-03 2012-12-06 Basf Se Wässrige Lösung, enthaltend Acrylsäure und deren konjugierte Base
CA2781246A1 (en) * 2011-07-14 2013-01-14 Rohm And Haas Company Method for removal of organic compounds from waste water streams in a process for production of (meth)acrylic acid
DE102012204436A1 (de) 2012-03-20 2012-10-04 Basf Se Thermisches Trennverfahren
CN104350034B (zh) 2012-06-08 2018-07-31 Cj 第一制糖株式会社 可再生丙烯酸生产和自其制备的产物
FR3017617B1 (fr) * 2014-02-19 2016-02-12 Arkema France Procede de production d'acide acrylique bio-source
JP6703950B2 (ja) 2014-02-20 2020-06-03 アーケマ・インコーポレイテッド アクリル酸を生成するための方法及びシステム
DE102014215438A1 (de) 2014-08-05 2016-02-11 Basf Se Kolonne zur thermischen Behandlung von fluiden Gemischen
DE102014215437A1 (de) 2014-08-05 2015-11-05 Basf Se Kolonne zur thermischen Behandlung eines Fluids
DE102014215436A1 (de) 2014-08-05 2015-10-15 Basf Se Kolonne zur thermischen Behandlung von fluiden Gemischen, insbesondere solchen, die (Meth)acrylmonomere enthalten
DE102015213493A1 (de) 2015-07-17 2016-09-15 Basf Se Kolonne zur thermischen Behandlung von fluiden Gemischen, insbesondere solchen, die (Meth)acrylmonomere enthalten
DE102015213490A1 (de) 2015-07-17 2016-09-15 Basf Se Kolonne zur thermischen Behandlung von fluiden Gemischen, insbesondere solchen, die (Meth)acrylmonomere enthalten
DE102015122209A1 (de) 2015-12-18 2017-02-16 Basf Se Kolonne zur thermischen Behandlung von fluiden Gemischen
FR3049601B1 (fr) * 2016-03-29 2018-03-09 Arkema France Procede ameliore de production d'acide (meth)acrylique
US11447439B2 (en) 2018-07-26 2022-09-20 Basf Se Method for inhibiting unwanted radical polymerisation of acrylic acid present in a liquid phase P
CN115335354A (zh) 2020-03-26 2022-11-11 巴斯夫欧洲公司 抑制存在于液相p中的丙烯酸的不期望的自由基聚合的方法
KR20230165803A (ko) 2021-03-31 2023-12-05 바스프 에스이 중합 경향을 갖는 화합물의 혼합물을 열 처리하기 위한 컬럼
WO2023006503A1 (de) 2021-07-28 2023-02-02 Basf Se Verfahren zur herstellung von acrylsäure
FR3147566A1 (fr) 2023-04-05 2024-10-11 Arkema France PROCEDE DE FABRICATION D’ACIDES CARBOXYLIQUES α-β INSATURES BIOSOURCES A PARTIR DE POLY(3-HYDROXYALCANOATE)
FR3147564A1 (fr) 2023-04-05 2024-10-11 Arkema France PROCEDE DE FABRICATION D’ACIDES CARBOXYLIQUES α-β INSATURES BIOSOURCES A PARTIR DE POLY(3-HYDROXYALCANOATE) CONTENU DANS DE LA BIOMASSE
FR3147565A1 (fr) 2023-04-05 2024-10-11 Arkema France PROCEDE DE FABRICATION D’ACIDES CARBOXYLIQUES α-β INSATURES BIOSOURCES A PARTIR DE POLY(3-HYDROXYALCANOATE) CONTENU DANS DE LA BIOMASSE
WO2024246367A1 (de) 2023-06-02 2024-12-05 Basf Se Verfahren und vorrichtung zur gewinnung von acrylsäure
WO2025078224A1 (de) 2023-10-11 2025-04-17 Basf Se Verfahren zur aufreinigung von acrylsäure durch kreisgasrückführung
WO2025078225A1 (de) 2023-10-11 2025-04-17 Basf Se Verfahren zur aufreinigung von acrylsäure durch muttersäurerückführung
WO2025114418A1 (en) 2023-11-28 2025-06-05 Basf Se Process for the distillation of acrylic acid with split-dosing of polymerization inhibitor
WO2025172146A1 (de) 2024-02-15 2025-08-21 Basf Se Verfahren zur herstellung von acrylsäure
WO2025219135A1 (en) 2024-04-17 2025-10-23 Basf Se Process for utilizing high calorific acrylic acid production waste streams
WO2025219136A1 (en) 2024-04-17 2025-10-23 Basf Se Process for utilizing acrylic acid production waste streams
WO2025219137A1 (en) 2024-04-17 2025-10-23 Basf Se Process for utilizing acrylic acid production waste streams by gasification and fermentation

Family Cites Families (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
AR206439A1 (es) * 1974-10-07 1976-07-23 Celanese Corp Un metodo para la recuperacion de un acido acrilico crudo
JPS6054939B2 (ja) * 1977-08-04 1985-12-03 住友化学工業株式会社 粗製アクリル酸の精製方法
JPS6013739A (ja) * 1983-07-04 1985-01-24 Sumitomo Chem Co Ltd アクリル酸の精製方法
US4599144A (en) * 1984-06-25 1986-07-08 Standard Oil Company (Indiana) Process for recovery of methacrylic acid
US4999452A (en) * 1989-05-15 1991-03-12 Union Carbide Chemicals And Plastics Company Inc. Process for producing acrylic ester
JP3289303B2 (ja) * 1992-03-06 2002-06-04 住友化学工業株式会社 アクロレインの製造方法
DE4308087C2 (de) * 1993-03-13 1997-02-06 Basf Ag Verfahren zur Abtrennung von Acrylsäure aus den Reaktionsgasen der katalytischen Oxidation von Propylen und/oder Acrolein
DE59602040D1 (de) * 1995-03-10 1999-07-08 Basf Ag Verfahren der kontinuierlich betriebenen heterogen katalysierten Gasphasenoxidation von Propylen zu Acrolein, Acrylsäure oder deren Gemisch
FR2735989B1 (fr) * 1995-06-29 1997-08-14 Rhone Poulenc Nutrition Animal Procede et installation de purification d'un flux gazeux contenant de l'acroleine

Also Published As

Publication number Publication date
TW431905B (en) 2001-05-01
US6646161B1 (en) 2003-11-11
CZ297503B6 (cs) 2007-01-03
CA2303373A1 (en) 1999-03-25
JP4215388B2 (ja) 2009-01-28
MY119650A (en) 2005-06-30
EP1015411A1 (de) 2000-07-05
BR9811450B1 (pt) 2011-06-28
CZ2000898A3 (cs) 2000-06-14
AU9624998A (en) 1999-04-05
KR100603875B1 (ko) 2006-07-25
ES2201539T3 (es) 2004-03-16
DE19740253A1 (de) 1999-03-18
DE59808713D1 (de) 2003-07-17
KR20010023911A (ko) 2001-03-26
WO1999014182A1 (de) 1999-03-25
JP2001516737A (ja) 2001-10-02
EP1015411B1 (de) 2003-06-11
CN1269779A (zh) 2000-10-11
CN1092636C (zh) 2002-10-16

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Legal Events

Date Code Title Description
B07A Application suspended after technical examination (opinion) [chapter 7.1 patent gazette]
B15K Others concerning applications: alteration of classification

Free format text: ALTERADA DE INT.CL: C07C 57/07, B01D 5/00, C07C 51/44

Ipc: C07C 57/07 (2008.04)

B09B Patent application refused [chapter 9.2 patent gazette]

Free format text: INDEFIRO O PEDIDO DE PATENTE COM BASE NOS ARTIGOS 8O, E 13 DA LPI NO 9.279 DE 14/05/1.996

B12B Appeal against refusal [chapter 12.2 patent gazette]
B16A Patent or certificate of addition of invention granted [chapter 16.1 patent gazette]

Free format text: PRAZO DE VALIDADE: 10 (DEZ) ANOS CONTADOS A PARTIR DE 28/06/2011, OBSERVADAS AS CONDICOES LEGAIS.

B25D Requested change of name of applicant approved

Owner name: BASF SE (DE)

B21A Patent or certificate of addition expired [chapter 21.1 patent gazette]

Free format text: PATENTE EXTINTA EM 28.06.2021