BR9811450A - Processos para a condensação fracionada de uma mistura gasosa e para a preparação de ácido acrìlico ou ácido metacrìlico - Google Patents
Processos para a condensação fracionada de uma mistura gasosa e para a preparação de ácido acrìlico ou ácido metacrìlicoInfo
- Publication number
- BR9811450A BR9811450A BR9811450-6A BR9811450A BR9811450A BR 9811450 A BR9811450 A BR 9811450A BR 9811450 A BR9811450 A BR 9811450A BR 9811450 A BR9811450 A BR 9811450A
- Authority
- BR
- Brazil
- Prior art keywords
- gas mixture
- processes
- preparation
- fractional condensation
- acrylic acid
- Prior art date
Links
- NIXOWILDQLNWCW-UHFFFAOYSA-N 2-Propenoic acid Natural products OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 title abstract 4
- 238000000034 method Methods 0.000 title abstract 4
- 239000000203 mixture Substances 0.000 title abstract 4
- 238000009833 condensation Methods 0.000 title abstract 3
- 230000005494 condensation Effects 0.000 title abstract 3
- SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 title abstract 2
- CERQOIWHTDAKMF-UHFFFAOYSA-N Methacrylic acid Chemical compound CC(=C)C(O)=O CERQOIWHTDAKMF-UHFFFAOYSA-N 0.000 title abstract 2
- 238000002360 preparation method Methods 0.000 title abstract 2
- 239000000470 constituent Substances 0.000 abstract 3
- 238000001816 cooling Methods 0.000 abstract 1
- 150000002735 metacrylic acids Chemical class 0.000 abstract 1
- 238000000926 separation method Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C57/00—Unsaturated compounds having carboxyl groups bound to acyclic carbon atoms
- C07C57/02—Unsaturated compounds having carboxyl groups bound to acyclic carbon atoms with only carbon-to-carbon double bonds as unsaturation
- C07C57/03—Monocarboxylic acids
- C07C57/04—Acrylic acid; Methacrylic acid
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D5/00—Condensation of vapours; Recovering volatile solvents by condensation
- B01D5/0027—Condensation of vapours; Recovering volatile solvents by condensation by direct contact between vapours or gases and the cooling medium
- B01D5/003—Condensation of vapours; Recovering volatile solvents by condensation by direct contact between vapours or gases and the cooling medium within column(s)
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/42—Separation; Purification; Stabilisation; Use of additives
- C07C51/43—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
- C07C51/44—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation by distillation
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Crystallography & Structural Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Connection Of Motors, Electrical Generators, Mechanical Devices, And The Like (AREA)
Abstract
"PROCESSOS PARA A CONDENSAçãO FRACIONADA DE UMA MISTURA GASOSA E PARA A PREPARAçãO DE áCIDO ACRìLICO OU áCIDO METACRìLICO" A invenção refere-se a um processo para a condensação fracionada de uma mistura gasosa, que contém pelo menos um outro constituinte condensável, em adição ao ácido acrílico ou ácido metacrílico, e que possui também uma alta proporção de um ou mais constituintes não condensáveis. De acordo com o referido processo, a mistura gasosa é passada através de um coluna com chicanas eficientes para a separação e os constituintes condensáveis são condensados por resfriamento.
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19740253.4 | 1997-09-12 | ||
| DE19740253A DE19740253A1 (de) | 1997-09-12 | 1997-09-12 | Verfahren zur fraktionierten Kondensation eines heißen Gasgemisches mit einem hohen Anteil nicht kondensierbarer Komponenten |
| PCT/EP1998/005779 WO1999014182A1 (de) | 1997-09-12 | 1998-09-10 | Verfahren zur fraktionierten kondensation eines acrylsäure oder methacrylsäure enthaltenden heissen gasgemisches mit einem hohen anteil nicht kondensierbarer komponenten |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| BR9811450A true BR9811450A (pt) | 2000-08-15 |
| BR9811450B1 BR9811450B1 (pt) | 2011-06-28 |
Family
ID=7842221
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| BRPI9811450-6A BR9811450B1 (pt) | 1997-09-12 | 1998-09-10 | processo para a preparação de ácido acrìlico ou ácido metacrìlico por oxidação catalìtica em fase gasosa. |
Country Status (14)
| Country | Link |
|---|---|
| US (1) | US6646161B1 (pt) |
| EP (1) | EP1015411B1 (pt) |
| JP (1) | JP4215388B2 (pt) |
| KR (1) | KR100603875B1 (pt) |
| CN (1) | CN1092636C (pt) |
| AU (1) | AU9624998A (pt) |
| BR (1) | BR9811450B1 (pt) |
| CA (1) | CA2303373A1 (pt) |
| CZ (1) | CZ297503B6 (pt) |
| DE (2) | DE19740253A1 (pt) |
| ES (1) | ES2201539T3 (pt) |
| MY (1) | MY119650A (pt) |
| TW (1) | TW431905B (pt) |
| WO (1) | WO1999014182A1 (pt) |
Families Citing this family (63)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE19814375A1 (de) * | 1998-03-31 | 1999-10-07 | Basf Ag | Verfahren zur Herstellung von Acrylsäure und Acrylsäureestern |
| DE19814387A1 (de) * | 1998-03-31 | 1999-10-07 | Basf Ag | Verfahren zur Herstellung von Acrylsäure und Acrylsäureestern |
| US6498272B1 (en) | 1999-03-06 | 2002-12-24 | Basf Aktiengesellschaft | Method for producing acrylic acid |
| MY122671A (en) | 1999-03-06 | 2006-04-29 | Basf Ag | Fractional condensation of a product gas mixture containing acrylic acid |
| DE60133473T2 (de) | 2001-12-14 | 2009-05-20 | Evonik Stockhausen Gmbh | Verfahren zur Herstellung von Acrylsäure |
| MY135762A (en) * | 2002-01-09 | 2008-06-30 | Basf Ag | Method for producing acrylic acid |
| DE10220494A1 (de) | 2002-05-07 | 2003-11-20 | Basf Ag | Verfahren zur Herstellung einer wässrigen Alkaliacrylat-Lösung |
| BRPI0413297B1 (pt) | 2003-08-06 | 2014-01-21 | Processo para operar uma oxidação parcial contínua em fase gasosa catalisada de maneira heterogênea de pelo menos um composto orgânico | |
| JP2005234834A (ja) * | 2004-02-19 | 2005-09-02 | Hitachi Ltd | 論理ボリュームの再配置方法 |
| DE102004021764A1 (de) * | 2004-04-30 | 2005-06-02 | Basf Ag | Verfahren zur Herstellung von Acrylsäure durch heterogen katalysierte Gasphasenpartialoxidation wenigstens einer C3-Kohlenwasserstoffvorläuferverbindung |
| US7592483B2 (en) | 2004-07-01 | 2009-09-22 | Basf Aktiengesellschaft | Preparation of acrolein or acrylic acid or a mixture thereof by heterogeneously catalyzed partial gas phase oxidation of propylene |
| DE102004055765A1 (de) * | 2004-11-18 | 2006-05-24 | Basf Ag | Verfahren zur Herstellung wasserabsorbierender Polymere |
| US7601866B2 (en) | 2005-03-01 | 2009-10-13 | Basf Aktiengesellschaft | Process for removing methacrolein from liquid phase comprising acrylic acid as a main constituent and target product, and methacrolein as a secondary component |
| US7705181B2 (en) | 2005-03-01 | 2010-04-27 | Basf Akiengesellschaft | Process for removing methacrylic acid from liquid phase comprising acrylic acid as a main constituent and target product, and methacrylic acid as a secondary component |
| DE102005018702A1 (de) | 2005-04-21 | 2006-10-26 | Basf Ag | Verfahren zur Regelung einer hydraulischen Waschkolonne |
| DE102005019911A1 (de) | 2005-04-27 | 2006-11-02 | Basf Ag | Verfahren der rektifikativen Auftrennung einer Acrylsäure und/oder Methacrylsäure enthaltenden Flüssigkeit |
| KR100999428B1 (ko) * | 2006-01-20 | 2010-12-09 | 니폰 쇼쿠바이 컴파니 리미티드 | (메타)아크릴산의 제조 방법 |
| JP5368673B2 (ja) * | 2006-01-20 | 2013-12-18 | 株式会社日本触媒 | (メタ)アクリル酸の製造方法 |
| WO2008033687A2 (en) | 2006-09-15 | 2008-03-20 | Dow Global Technologies Inc. | Process for producing acrylic acid |
| DE102007055086A1 (de) | 2007-11-16 | 2009-05-20 | Basf Se | Verfahren zur Herstellung von Acrylsäure |
| JP5489726B2 (ja) * | 2007-01-26 | 2014-05-14 | ビーエーエスエフ ソシエタス・ヨーロピア | アクリル酸の製造方法 |
| WO2008090190A1 (de) * | 2007-01-26 | 2008-07-31 | Basf Se | Verfahren zur herstellung von acrylsäure |
| DE102007004960A1 (de) | 2007-01-26 | 2008-07-31 | Basf Se | Verfahren zur Herstellung von Acrylsäure |
| DE102007043758A1 (de) | 2007-09-13 | 2008-10-23 | Basf Se | Verfahren zum Betreiben einer kontinuierlichen Abtrennung eines Zielproduktes X in Form von feinteiligem Kristallisat des Zielproduktes X |
| BE1018537A3 (fr) | 2007-09-13 | 2011-03-01 | Basf Se | Procede d'exploitation d'une separation en continu d'un produit cible x sous la forme d'un cristallisat finement divise. |
| DE102007043748A1 (de) | 2007-09-13 | 2008-09-11 | Basf Se | Verfahren zur kontinuierlichen Abtrennung eines Zielproduktes X in Form von feinteiligem Kristallisat |
| JP5380434B2 (ja) | 2008-04-27 | 2014-01-08 | 株式会社日本触媒 | アクリル酸の製造方法ならびにその製造方法を用いた親水性樹脂の製造方法および吸水性樹脂の製造方法 |
| JP5507111B2 (ja) * | 2008-05-30 | 2014-05-28 | ローム アンド ハース カンパニー | 水性(メタ)アクリル酸の製造方法 |
| EP2135656A1 (en) * | 2008-05-30 | 2009-12-23 | Rohm and Haas Company | Method for production of purified (Meth)acrylic acid |
| EP2334631B1 (de) | 2008-07-28 | 2017-03-01 | Basf Se | Verfahren zur auftrennung von in einem produktgasgemisch einer partiellen heterogen katalysierten gasphasenoxidation einer c3-vorläuferverbinding der acrylsäure als hauptbestandteil enthaltener acrylsäure und als nebenprodukt enthaltenem glyoxal |
| DE102008040799A1 (de) | 2008-07-28 | 2008-12-11 | Basf Se | Verfahren zur Auftrennung von in einem Produktgasgemisch einer partiellen heterogen katalysierten Gasphasenoxidation einer C3-Vorläuferverbindung der Acrylsäure als Hauptbestandteil enthaltener Acrylsäure und als Nebenprodukt enthaltenem Glyoxal |
| DE102008041573A1 (de) | 2008-08-26 | 2010-03-04 | Basf Se | Verfahren zur Auftrennung von in einem Produktgasgemisch einer partiellen heterogen katalysierten Gasphasenoxidation einer C3-Vorläuferverbindung der Acrylsäure als Hauptbestandteil enhaltener Acrylsäure und als Nebenprodukt enthaltenem Glyoxal |
| KR101994630B1 (ko) | 2008-10-01 | 2019-07-02 | 알케마 인코포레이티드 | 온라인 근적외선 분석을 이용한 (메트)아크릴산 정제 방법의 제어 |
| WO2011017172A2 (en) * | 2009-07-28 | 2011-02-10 | Joule Unlimited, Inc. | Fractional condensation processes, apparatuses and systems |
| DE102010042216A1 (de) | 2010-10-08 | 2011-06-09 | Basf Se | Verfahren zur Hemmung der unerwünschten radikalischen Polymerisation von in einer flüssigen Phase P befindlicher Acrylsäure |
| DE102011076931A1 (de) | 2011-06-03 | 2012-12-06 | Basf Se | Wässrige Lösung, enthaltend Acrylsäure und deren konjugierte Base |
| CA2781246A1 (en) * | 2011-07-14 | 2013-01-14 | Rohm And Haas Company | Method for removal of organic compounds from waste water streams in a process for production of (meth)acrylic acid |
| DE102012204436A1 (de) | 2012-03-20 | 2012-10-04 | Basf Se | Thermisches Trennverfahren |
| CN104350034B (zh) | 2012-06-08 | 2018-07-31 | Cj 第一制糖株式会社 | 可再生丙烯酸生产和自其制备的产物 |
| FR3017617B1 (fr) * | 2014-02-19 | 2016-02-12 | Arkema France | Procede de production d'acide acrylique bio-source |
| JP6703950B2 (ja) | 2014-02-20 | 2020-06-03 | アーケマ・インコーポレイテッド | アクリル酸を生成するための方法及びシステム |
| DE102014215438A1 (de) | 2014-08-05 | 2016-02-11 | Basf Se | Kolonne zur thermischen Behandlung von fluiden Gemischen |
| DE102014215437A1 (de) | 2014-08-05 | 2015-11-05 | Basf Se | Kolonne zur thermischen Behandlung eines Fluids |
| DE102014215436A1 (de) | 2014-08-05 | 2015-10-15 | Basf Se | Kolonne zur thermischen Behandlung von fluiden Gemischen, insbesondere solchen, die (Meth)acrylmonomere enthalten |
| DE102015213493A1 (de) | 2015-07-17 | 2016-09-15 | Basf Se | Kolonne zur thermischen Behandlung von fluiden Gemischen, insbesondere solchen, die (Meth)acrylmonomere enthalten |
| DE102015213490A1 (de) | 2015-07-17 | 2016-09-15 | Basf Se | Kolonne zur thermischen Behandlung von fluiden Gemischen, insbesondere solchen, die (Meth)acrylmonomere enthalten |
| DE102015122209A1 (de) | 2015-12-18 | 2017-02-16 | Basf Se | Kolonne zur thermischen Behandlung von fluiden Gemischen |
| FR3049601B1 (fr) * | 2016-03-29 | 2018-03-09 | Arkema France | Procede ameliore de production d'acide (meth)acrylique |
| US11447439B2 (en) | 2018-07-26 | 2022-09-20 | Basf Se | Method for inhibiting unwanted radical polymerisation of acrylic acid present in a liquid phase P |
| CN115335354A (zh) | 2020-03-26 | 2022-11-11 | 巴斯夫欧洲公司 | 抑制存在于液相p中的丙烯酸的不期望的自由基聚合的方法 |
| KR20230165803A (ko) | 2021-03-31 | 2023-12-05 | 바스프 에스이 | 중합 경향을 갖는 화합물의 혼합물을 열 처리하기 위한 컬럼 |
| WO2023006503A1 (de) | 2021-07-28 | 2023-02-02 | Basf Se | Verfahren zur herstellung von acrylsäure |
| FR3147566A1 (fr) | 2023-04-05 | 2024-10-11 | Arkema France | PROCEDE DE FABRICATION D’ACIDES CARBOXYLIQUES α-β INSATURES BIOSOURCES A PARTIR DE POLY(3-HYDROXYALCANOATE) |
| FR3147564A1 (fr) | 2023-04-05 | 2024-10-11 | Arkema France | PROCEDE DE FABRICATION D’ACIDES CARBOXYLIQUES α-β INSATURES BIOSOURCES A PARTIR DE POLY(3-HYDROXYALCANOATE) CONTENU DANS DE LA BIOMASSE |
| FR3147565A1 (fr) | 2023-04-05 | 2024-10-11 | Arkema France | PROCEDE DE FABRICATION D’ACIDES CARBOXYLIQUES α-β INSATURES BIOSOURCES A PARTIR DE POLY(3-HYDROXYALCANOATE) CONTENU DANS DE LA BIOMASSE |
| WO2024246367A1 (de) | 2023-06-02 | 2024-12-05 | Basf Se | Verfahren und vorrichtung zur gewinnung von acrylsäure |
| WO2025078224A1 (de) | 2023-10-11 | 2025-04-17 | Basf Se | Verfahren zur aufreinigung von acrylsäure durch kreisgasrückführung |
| WO2025078225A1 (de) | 2023-10-11 | 2025-04-17 | Basf Se | Verfahren zur aufreinigung von acrylsäure durch muttersäurerückführung |
| WO2025114418A1 (en) | 2023-11-28 | 2025-06-05 | Basf Se | Process for the distillation of acrylic acid with split-dosing of polymerization inhibitor |
| WO2025172146A1 (de) | 2024-02-15 | 2025-08-21 | Basf Se | Verfahren zur herstellung von acrylsäure |
| WO2025219135A1 (en) | 2024-04-17 | 2025-10-23 | Basf Se | Process for utilizing high calorific acrylic acid production waste streams |
| WO2025219136A1 (en) | 2024-04-17 | 2025-10-23 | Basf Se | Process for utilizing acrylic acid production waste streams |
| WO2025219137A1 (en) | 2024-04-17 | 2025-10-23 | Basf Se | Process for utilizing acrylic acid production waste streams by gasification and fermentation |
Family Cites Families (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| AR206439A1 (es) * | 1974-10-07 | 1976-07-23 | Celanese Corp | Un metodo para la recuperacion de un acido acrilico crudo |
| JPS6054939B2 (ja) * | 1977-08-04 | 1985-12-03 | 住友化学工業株式会社 | 粗製アクリル酸の精製方法 |
| JPS6013739A (ja) * | 1983-07-04 | 1985-01-24 | Sumitomo Chem Co Ltd | アクリル酸の精製方法 |
| US4599144A (en) * | 1984-06-25 | 1986-07-08 | Standard Oil Company (Indiana) | Process for recovery of methacrylic acid |
| US4999452A (en) * | 1989-05-15 | 1991-03-12 | Union Carbide Chemicals And Plastics Company Inc. | Process for producing acrylic ester |
| JP3289303B2 (ja) * | 1992-03-06 | 2002-06-04 | 住友化学工業株式会社 | アクロレインの製造方法 |
| DE4308087C2 (de) * | 1993-03-13 | 1997-02-06 | Basf Ag | Verfahren zur Abtrennung von Acrylsäure aus den Reaktionsgasen der katalytischen Oxidation von Propylen und/oder Acrolein |
| DE59602040D1 (de) * | 1995-03-10 | 1999-07-08 | Basf Ag | Verfahren der kontinuierlich betriebenen heterogen katalysierten Gasphasenoxidation von Propylen zu Acrolein, Acrylsäure oder deren Gemisch |
| FR2735989B1 (fr) * | 1995-06-29 | 1997-08-14 | Rhone Poulenc Nutrition Animal | Procede et installation de purification d'un flux gazeux contenant de l'acroleine |
-
1997
- 1997-09-12 DE DE19740253A patent/DE19740253A1/de not_active Withdrawn
-
1998
- 1998-09-10 DE DE59808713T patent/DE59808713D1/de not_active Expired - Lifetime
- 1998-09-10 AU AU96249/98A patent/AU9624998A/en not_active Abandoned
- 1998-09-10 EP EP98950022A patent/EP1015411B1/de not_active Expired - Lifetime
- 1998-09-10 BR BRPI9811450-6A patent/BR9811450B1/pt not_active IP Right Cessation
- 1998-09-10 CN CN98808971A patent/CN1092636C/zh not_active Expired - Lifetime
- 1998-09-10 KR KR1020007002599A patent/KR100603875B1/ko not_active Expired - Lifetime
- 1998-09-10 TW TW087115041A patent/TW431905B/zh not_active IP Right Cessation
- 1998-09-10 CA CA002303373A patent/CA2303373A1/en not_active Abandoned
- 1998-09-10 JP JP2000511736A patent/JP4215388B2/ja not_active Expired - Lifetime
- 1998-09-10 WO PCT/EP1998/005779 patent/WO1999014182A1/de not_active Ceased
- 1998-09-10 CZ CZ20000898A patent/CZ297503B6/cs not_active IP Right Cessation
- 1998-09-10 ES ES98950022T patent/ES2201539T3/es not_active Expired - Lifetime
- 1998-09-10 US US09/508,077 patent/US6646161B1/en not_active Expired - Lifetime
- 1998-09-11 MY MYPI98004175A patent/MY119650A/en unknown
Also Published As
| Publication number | Publication date |
|---|---|
| TW431905B (en) | 2001-05-01 |
| US6646161B1 (en) | 2003-11-11 |
| CZ297503B6 (cs) | 2007-01-03 |
| CA2303373A1 (en) | 1999-03-25 |
| JP4215388B2 (ja) | 2009-01-28 |
| MY119650A (en) | 2005-06-30 |
| EP1015411A1 (de) | 2000-07-05 |
| BR9811450B1 (pt) | 2011-06-28 |
| CZ2000898A3 (cs) | 2000-06-14 |
| AU9624998A (en) | 1999-04-05 |
| KR100603875B1 (ko) | 2006-07-25 |
| ES2201539T3 (es) | 2004-03-16 |
| DE19740253A1 (de) | 1999-03-18 |
| DE59808713D1 (de) | 2003-07-17 |
| KR20010023911A (ko) | 2001-03-26 |
| WO1999014182A1 (de) | 1999-03-25 |
| JP2001516737A (ja) | 2001-10-02 |
| EP1015411B1 (de) | 2003-06-11 |
| CN1269779A (zh) | 2000-10-11 |
| CN1092636C (zh) | 2002-10-16 |
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