BR9714567A - Método para preparar etilenodiamino-n, n'-disuccinato dissódico. - Google Patents
Método para preparar etilenodiamino-n, n'-disuccinato dissódico.Info
- Publication number
- BR9714567A BR9714567A BR9714567-0A BR9714567A BR9714567A BR 9714567 A BR9714567 A BR 9714567A BR 9714567 A BR9714567 A BR 9714567A BR 9714567 A BR9714567 A BR 9714567A
- Authority
- BR
- Brazil
- Prior art keywords
- disuccinate
- disodium ethylenediamine
- preparing disodium
- ethylenediamine
- preparing
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C227/00—Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton
- C07C227/38—Separation; Purification; Stabilisation; Use of additives
- C07C227/40—Separation; Purification
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C227/00—Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton
- C07C227/04—Formation of amino groups in compounds containing carboxyl groups
- C07C227/06—Formation of amino groups in compounds containing carboxyl groups by addition or substitution reactions, without increasing the number of carbon atoms in the carbon skeleton of the acid
- C07C227/08—Formation of amino groups in compounds containing carboxyl groups by addition or substitution reactions, without increasing the number of carbon atoms in the carbon skeleton of the acid by reaction of ammonia or amines with acids containing functional groups
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
"MéTODO PARA PREPARAR ETILENODIAMINO-N, N' - DISSUCCINATO DISSóDICO". é revelado um prodesso para isolar o sal dissódico de uma mistura de isómeros mesos e racêmicos de sais de sódio do ácido N, N' - etilenodiamina dissuccínico, a partir de soluções aquosas alcalinas, ajustados-se o pH da solução alcalina entre 5 a 10 por adição de um ácido, seguido pela recuperação de um sal dissódico sólido. A mistura de isómeros pode ser preparada pela reação do maleato de sódio com etilenodiamina em uma solução aquosa alcalina. Esse método é particularmente apropriado para preparar o sal dissódico tetraidatado e evitar a formação de ácido livre. O produto final biodegrada mais rapidamente que o ácido N, N, N', N' - etilenodiaminotetracético (EDTA).
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US08/832,555 US5731468A (en) | 1997-04-03 | 1997-04-03 | Preparation of disodium ethylenediamine-N,N'-disuccinate |
| PCT/US1997/020828 WO1998043944A1 (en) | 1997-04-03 | 1997-11-17 | Preparation of disodium ethylenediamine-n,n'-disuccinate |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| BR9714567A true BR9714567A (pt) | 2000-02-15 |
Family
ID=25261999
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| BR9714567-0A BR9714567A (pt) | 1997-04-03 | 1997-11-17 | Método para preparar etilenodiamino-n, n'-disuccinato dissódico. |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US5731468A (pt) |
| EP (1) | EP1021395B1 (pt) |
| JP (1) | JP2002508744A (pt) |
| AT (1) | ATE207877T1 (pt) |
| BR (1) | BR9714567A (pt) |
| DE (1) | DE69707928T2 (pt) |
| WO (1) | WO1998043944A1 (pt) |
Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB9507659D0 (en) * | 1995-04-13 | 1995-05-31 | Ass Octel | Alkylation process |
| DE19800437A1 (de) * | 1998-01-08 | 1999-07-15 | Basf Ag | Verfahren zur Herstellung von (S,S)-N,N'-Ethylendiamindibernsteinsäure, analogen Verbindungen oder Salzen davon |
| EP0997531B1 (en) * | 1998-04-17 | 2007-10-31 | Mitsubishi Rayon Co., Ltd. | Process for producing alkali metal s,s-ethylenediamine-n,n'-disuccinates |
| DE102009027164A1 (de) * | 2009-06-24 | 2010-12-30 | Henkel Ag & Co. Kgaa | Maschinelles Geschirrspülmittel |
| DE102009027160A1 (de) * | 2009-06-24 | 2010-12-30 | Henkel Ag & Co. Kgaa | Maschinelles Geschirrspülmittel |
Family Cites Families (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3158635A (en) * | 1959-03-18 | 1964-11-24 | Stauffer Chemical Co | Bis-adduction products and methods of preparing same |
| US5569443A (en) * | 1994-11-18 | 1996-10-29 | The Dow Chemical Company | Method for removing hydrogen sulfide from a gas using polyamino disuccinic acid |
| GB9322648D0 (en) * | 1993-11-03 | 1993-12-22 | Ass Octel | Process for the production of s.s.e.d.d.s |
| EP0687950A1 (en) * | 1994-05-27 | 1995-12-20 | Konica Corporation | Granular and tablet-shape processing composition for processing a silver halide photographic light-sensitive material |
| US5466867A (en) * | 1994-07-11 | 1995-11-14 | Albemarle Corporation | Method for producing [S,S]-ethylenediamine-N,N'-disuccinic acid from its calcium salt |
| US5587512A (en) * | 1994-07-11 | 1996-12-24 | Albemarle Corporation | Process for obtaining [S,S]-ethylenediamine-n,n'-disuccinic acid from a salt solution of such acid and l-aspartic acid |
| US5554791A (en) * | 1994-07-11 | 1996-09-10 | Albemarle Corporation | Process for producing [S,S]-ethylenediamine-N,N'-disuccinic acid |
-
1997
- 1997-04-03 US US08/832,555 patent/US5731468A/en not_active Expired - Lifetime
- 1997-11-17 JP JP54159398A patent/JP2002508744A/ja active Pending
- 1997-11-17 DE DE69707928T patent/DE69707928T2/de not_active Expired - Lifetime
- 1997-11-17 WO PCT/US1997/020828 patent/WO1998043944A1/en not_active Ceased
- 1997-11-17 AT AT97946939T patent/ATE207877T1/de not_active IP Right Cessation
- 1997-11-17 EP EP97946939A patent/EP1021395B1/en not_active Expired - Lifetime
- 1997-11-17 BR BR9714567-0A patent/BR9714567A/pt not_active IP Right Cessation
Also Published As
| Publication number | Publication date |
|---|---|
| DE69707928T2 (de) | 2002-04-11 |
| JP2002508744A (ja) | 2002-03-19 |
| EP1021395A1 (en) | 2000-07-26 |
| EP1021395B1 (en) | 2001-10-31 |
| US5731468A (en) | 1998-03-24 |
| WO1998043944A1 (en) | 1998-10-08 |
| ATE207877T1 (de) | 2001-11-15 |
| DE69707928D1 (de) | 2001-12-06 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| B25A | Requested transfer of rights approved |
Free format text: DOW GLOBAL TECHNOLOGIES INC (US) |
|
| B06A | Patent application procedure suspended [chapter 6.1 patent gazette] | ||
| B09A | Decision: intention to grant [chapter 9.1 patent gazette] | ||
| B16A | Patent or certificate of addition of invention granted [chapter 16.1 patent gazette] |
Free format text: PRAZO DE VALIDADE: 10 (DEZ) ANOS CONTADOS A PARTIR DE 04/11/2008, OBSERVADAS AS CONDICOES LEGAIS. |
|
| B21F | Lapse acc. art. 78, item iv - on non-payment of the annual fees in time | ||
| B24J | Lapse because of non-payment of annual fees (definitively: art 78 iv lpi, resolution 113/2013 art. 12) |