BG110975A - Food supplement containing terpenoids and flavonoids from essential oil raw materials - extracts of pine twigs and juniper fruit - Google Patents
Food supplement containing terpenoids and flavonoids from essential oil raw materials - extracts of pine twigs and juniper fruit Download PDFInfo
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- BG110975A BG110975A BG10110975A BG11097511A BG110975A BG 110975 A BG110975 A BG 110975A BG 10110975 A BG10110975 A BG 10110975A BG 11097511 A BG11097511 A BG 11097511A BG 110975 A BG110975 A BG 110975A
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- flavonoids
- ethanol
- terpenoids
- extracts
- pine
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- 241000721662 Juniperus Species 0.000 title claims abstract description 15
- 229930003935 flavonoid Natural products 0.000 title claims abstract description 11
- 150000002215 flavonoids Chemical class 0.000 title claims abstract description 11
- 235000017173 flavonoids Nutrition 0.000 title claims abstract description 11
- 235000013399 edible fruits Nutrition 0.000 title claims abstract description 10
- 150000003505 terpenes Chemical class 0.000 title claims abstract description 10
- 239000000284 extract Substances 0.000 title abstract description 14
- 235000015872 dietary supplement Nutrition 0.000 title abstract description 8
- 235000011613 Pinus brutia Nutrition 0.000 title abstract description 7
- 235000008331 Pinus X rigitaeda Nutrition 0.000 title abstract description 6
- 241000018646 Pinus brutia Species 0.000 title abstract description 6
- 239000000341 volatile oil Substances 0.000 title description 3
- 239000002994 raw material Substances 0.000 title 1
- 239000000203 mixture Substances 0.000 claims abstract description 6
- ZOXJGFHDIHLPTG-UHFFFAOYSA-N Boron Chemical compound [B] ZOXJGFHDIHLPTG-UHFFFAOYSA-N 0.000 claims description 9
- 229910052796 boron Inorganic materials 0.000 claims description 9
- 125000003118 aryl group Chemical group 0.000 claims description 8
- UXTMROKLAAOEQO-UHFFFAOYSA-N chloroform;ethanol Chemical compound CCO.ClC(Cl)Cl UXTMROKLAAOEQO-UHFFFAOYSA-N 0.000 claims description 6
- 239000000469 ethanolic extract Substances 0.000 claims description 5
- 235000013373 food additive Nutrition 0.000 claims description 5
- 239000002778 food additive Substances 0.000 claims description 5
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 abstract description 22
- HEDRZPFGACZZDS-UHFFFAOYSA-N Chloroform Chemical compound ClC(Cl)Cl HEDRZPFGACZZDS-UHFFFAOYSA-N 0.000 abstract description 10
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 abstract description 9
- 239000012141 concentrate Substances 0.000 abstract description 9
- 239000000243 solution Substances 0.000 abstract description 8
- 238000004519 manufacturing process Methods 0.000 abstract description 6
- 239000012670 alkaline solution Substances 0.000 abstract description 5
- 235000009508 confectionery Nutrition 0.000 abstract description 4
- 235000012970 cakes Nutrition 0.000 abstract description 3
- YZSJUQIFYHUSKU-UHFFFAOYSA-N ethanol;propane-1,2-diol Chemical compound CCO.CC(O)CO YZSJUQIFYHUSKU-UHFFFAOYSA-N 0.000 abstract description 3
- 235000015243 ice cream Nutrition 0.000 abstract description 3
- 235000013334 alcoholic beverage Nutrition 0.000 abstract description 2
- 239000003995 emulsifying agent Substances 0.000 abstract description 2
- 241000218641 Pinaceae Species 0.000 abstract 1
- 239000013543 active substance Substances 0.000 abstract 1
- 230000001225 therapeutic effect Effects 0.000 abstract 1
- 235000008504 concentrate Nutrition 0.000 description 7
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 4
- 238000001704 evaporation Methods 0.000 description 4
- 230000008020 evaporation Effects 0.000 description 4
- 238000000605 extraction Methods 0.000 description 4
- 239000002904 solvent Substances 0.000 description 4
- 230000000694 effects Effects 0.000 description 3
- 239000003921 oil Substances 0.000 description 3
- UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 description 2
- FEWJPZIEWOKRBE-UHFFFAOYSA-N Tartaric acid Natural products [H+].[H+].[O-]C(=O)C(O)C(O)C([O-])=O FEWJPZIEWOKRBE-UHFFFAOYSA-N 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- 150000007513 acids Chemical class 0.000 description 2
- 230000001152 anti-nicotinic effect Effects 0.000 description 2
- 235000013361 beverage Nutrition 0.000 description 2
- 239000000839 emulsion Substances 0.000 description 2
- 235000011187 glycerol Nutrition 0.000 description 2
- 230000035876 healing Effects 0.000 description 2
- 238000002156 mixing Methods 0.000 description 2
- 235000016709 nutrition Nutrition 0.000 description 2
- 230000020477 pH reduction Effects 0.000 description 2
- 235000002906 tartaric acid Nutrition 0.000 description 2
- 239000011975 tartaric acid Substances 0.000 description 2
- LNAZSHAWQACDHT-XIYTZBAFSA-N (2r,3r,4s,5r,6s)-4,5-dimethoxy-2-(methoxymethyl)-3-[(2s,3r,4s,5r,6r)-3,4,5-trimethoxy-6-(methoxymethyl)oxan-2-yl]oxy-6-[(2r,3r,4s,5r,6r)-4,5,6-trimethoxy-2-(methoxymethyl)oxan-3-yl]oxyoxane Chemical compound CO[C@@H]1[C@@H](OC)[C@H](OC)[C@@H](COC)O[C@H]1O[C@H]1[C@H](OC)[C@@H](OC)[C@H](O[C@H]2[C@@H]([C@@H](OC)[C@H](OC)O[C@@H]2COC)OC)O[C@@H]1COC LNAZSHAWQACDHT-XIYTZBAFSA-N 0.000 description 1
- 241000218631 Coniferophyta Species 0.000 description 1
- 206010020772 Hypertension Diseases 0.000 description 1
- 206010028980 Neoplasm Diseases 0.000 description 1
- CWEZAWNPTYBADX-UHFFFAOYSA-N Procyanidin Natural products OC1C(OC2C(O)C(Oc3c2c(O)cc(O)c3C4C(O)C(Oc5cc(O)cc(O)c45)c6ccc(O)c(O)c6)c7ccc(O)c(O)c7)c8c(O)cc(O)cc8OC1c9ccc(O)c(O)c9 CWEZAWNPTYBADX-UHFFFAOYSA-N 0.000 description 1
- 229930182448 Prodelphinidin Natural products 0.000 description 1
- 229920000124 Prodelphinidin Polymers 0.000 description 1
- 241001006211 Silvius Species 0.000 description 1
- -1 acidification Substances 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 229940126675 alternative medicines Drugs 0.000 description 1
- 230000003266 anti-allergic effect Effects 0.000 description 1
- 230000003110 anti-inflammatory effect Effects 0.000 description 1
- 230000000840 anti-viral effect Effects 0.000 description 1
- 230000001764 biostimulatory effect Effects 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 235000012174 carbonated soft drink Nutrition 0.000 description 1
- 230000003177 cardiotonic effect Effects 0.000 description 1
- 235000019504 cigarettes Nutrition 0.000 description 1
- 230000001804 emulsifying effect Effects 0.000 description 1
- 239000000686 essence Substances 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 239000012676 herbal extract Substances 0.000 description 1
- 239000002035 hexane extract Substances 0.000 description 1
- 230000001506 immunosuppresive effect Effects 0.000 description 1
- 235000021579 juice concentrates Nutrition 0.000 description 1
- 239000000453 juniperus communis l. leaf oil Substances 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 229920000609 methyl cellulose Polymers 0.000 description 1
- 239000001923 methylcellulose Substances 0.000 description 1
- 235000010981 methylcellulose Nutrition 0.000 description 1
- 235000019520 non-alcoholic beverage Nutrition 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 239000000546 pharmaceutical excipient Substances 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 239000003755 preservative agent Substances 0.000 description 1
- 230000002335 preservative effect Effects 0.000 description 1
- 229920002414 procyanidin Polymers 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 229910000030 sodium bicarbonate Inorganic materials 0.000 description 1
- 235000017557 sodium bicarbonate Nutrition 0.000 description 1
- 235000002639 sodium chloride Nutrition 0.000 description 1
- 235000014214 soft drink Nutrition 0.000 description 1
- 238000000935 solvent evaporation Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 235000020357 syrup Nutrition 0.000 description 1
- 239000006188 syrup Substances 0.000 description 1
- 235000013343 vitamin Nutrition 0.000 description 1
- 229940088594 vitamin Drugs 0.000 description 1
- 229930003231 vitamin Natural products 0.000 description 1
- 239000011782 vitamin Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Landscapes
- Coloring Foods And Improving Nutritive Qualities (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Abstract
Description
Описание на изобретениетоDescription of the invention
1.Наименование на изобретението1. Name of the invention
Хранителна добавка , съдържаща терпеноиди и флавоноиди от етеричномаслени суровини - екстракти от борова вършина и плод хвойнаNutritional Supplement containing Terpenoids and Flavonoids from Essential Oils - Pine and Juniper Extracts
2.0бласт на приложение - изобретението се отнася до хранителна добавка - концентрат, съдържаща терпеноиди и флавоноиди на екстракт, получен с алкален разтвор на етанол: хлороформ от борова вършина и екстракт от плод хвойна, която може да се използва за производство като на безалкохолни, така и на алкохолни напитки , бонбони, кексове, сладолед.2.0 Field of application - The invention relates to a food additive concentrate containing terpenoids and flavonoids of an extract obtained with an alkaline solution of ethanol: chloroform from pine and juniper extract, which can be used for the production of non-alcoholic, and alcoholic beverages, candy, cakes, ice cream.
З.Литературни данни за използвани до сега подобни хранителни добавки :H. Literature data on similar food additives used so far:
Известни са концентрати от сок на млади филизи на иглолистни дървета / Silviu Corlateanu, T.Florica, Е. Stefanescu; Bui. Univ. Brasov B 20, 11-116, (1978) /.Недостатък на известните концентрати като х ранителни добавки е, че освен вкусови и ароматични качества, те нямат изразен лечебен и емулсионен ефект.Juice concentrates of young shoots of conifers are known / Silviu Corlateanu, T.Florica, E. Stefanescu; Bui. Univ. Brasov B 20, 11-116, (1978) /. The disadvantage of known concentrates such as dietary supplements is that, in addition to their taste and aromatic qualities, they have no pronounced healing and emulsion effect.
Известен е екстракт с хексан от борова смола съдържащ дитерпенови киселини с антиникотиново действие, който се използва за производство на бонбони икато добавка към цигари / Isolation of Pimaric and Dehydroabietic Acids from pine oleoresin as Antinicotinic Substances, A.Suzuki, M. Azano, c. Ohkubo, S. Tamura; Agr. Biol. Chem. 1972q 36, No 11,1051 - 1053 /A boron resin hexane extract containing diterpenic acids with antinicotinic action is known, which is used for the production of candies and as an additive to cigarettes / A.Suzuki, M. Azano, c. Ohkubo, S. Tamura; Agr. Biol. Chem. 1972q 36, No 11.1051 - 1053 /
U.S.Pat. No.5,690,984 описва напитка, направена от борови иглички чрез варене с вода , полезна при високо кръвно налягане.U.S.Pat. No. 5,690,984 describes a beverage made from pine needles by boiling with water, useful at high blood pressure.
Флавоноидните компоненти на бора - процианидини и проделфинидини показват антивъзпалителна , антиалергична активност, антивирусно , имунозащитно и подтискащо тумори действие / Carconogenesis, 1999, Sep. USA /.Те допринасят за кардиотоничното действие на иглолистните екстракти / Discover the Amazing Power of Pine Needle Oil, http://www.nanume.net/wp/category/health/alternative medicines/The flavonoid components of boron - procyanidins and prodelphinidins show anti-inflammatory, anti-allergic activity, antiviral, immunosuppressive and tumor-suppressing activity / Carconogenesis, 1999, Sep. USA /.They contribute to the cardiotonic action of coniferous extracts / Discover the Amazing Power of Pine Needle Oil, http://www.nanume.net/wp/category/health/alternative medicines /
4. Задача на изобретението е да се създаде хранителна добавка като концентрат за напитки, бонбони , кексове, сладолед, обогатени с биологично активни и емулгиращи вещества с изразен лечебен ефект и високи технологични качества.4. The object of the invention is to provide a nutritional supplement such as concentrate for beverages, sweets, cakes, ice cream, enriched with biologically active and emulsifying substances with pronounced healing effect and high technological qualities.
Съгласно изобретението хранителната добавка - концентрат съдържа в обемни % от 0, 031 до 0,23 % смес от терпеноиди и флавоноиди от екстракт от борова вършина , получен с алкален разтвор на етанол-хлороформ, изпаряване на разтворителя, извличане с разтвор на натриев бикарбонат , подкисляване,екстракция с хлороформ и изпаряване на разтворителя ; хлороформ-етанолен или етанолен екстракт от плод хвойна- от 6,2 5до21,72%; ароматен дестилат за производство на джин - от 78,33 до 93,72 % ; спомагателни вещества консервант, билкови екстракти, есенции, етерични масла , плодови концентрати, глицерин, соли, метилцелулоза, витамини, хранителни киселини.According to the invention, the nutritional concentrate contains, by volume, from 0, 031 to 0.23%, a mixture of terpenoids and flavonoids from a boron tip extract obtained with an alkaline solution of ethanol-chloroform, evaporation of the solvent, extraction with sodium bicarbonate solution, acidification, chloroform extraction and solvent evaporation; chloroform-ethanol or ethanolic extract of juniper fruit - from 6.2 to 21.72%; aromatic distillate for the production of gin - from 78,33 to 93,72%; excipients preservative, herbal extracts, essences, essential oils, fruit concentrates, glycerin, salts, methylcellulose, vitamins, nutritional acids.
Сместа от терпеноиди и флавоноиди от боровия екстракт се използва като концентрат за хранителна добавка във вид на пропиленгликолов, етанолен или пропиленгликолов - етанолен разтвор.The mixture of terpenoids and flavonoids from boron extract is used as a concentrate for a nutritional supplement in the form of propylene glycol, ethanol or propylene glycol ethanol solution.
Хлороформ-етанолният и етанолният екстракт от плод хвойна се получават чрез многократна екстракция на плод хвойна и зпаряване на разтворителя.Хлороформ-етанолният екстракт от плод хвойна се използва за хранителната добавка във вид на пропиленгликолов, етанолен или пропиленгликолов - етанолен разтвор.Етанолният екстракт от плод хвойна се използва във вид на концентриран етанолен разтвор, който допълнително може да се разреди с пропиленгликол.Chloroform-ethanol and ethanolic extract of juniper fruit are obtained by repeated extraction of juniper fruit and evaporation of the solvent. Juniper is used as a concentrated ethanol solution that can be further diluted with propylene glycol.
Хранителната добавка - концентрат се получава чрез смесване на така получените разтвори на екстрактите с ароматичния дестилат за джин в обемните проценти, описани по-горе и филтруване на разтвора.The food additive concentrate is obtained by mixing the extracts thus obtained with the aromatic gin distillate in the volume percentages described above and filtering the solution.
Предимсво на предлаганата хранителна добавка е , че освен вкусови и ароматични свойства притежава биостимулиращо и антиникотиново действие, както и добре изразен емулсионен ефект, който в случаите на приложение за производство на безалкохолни напитки води до избягване на необходимостта от използване на синтетичен емулгатор.The advantage of the food additive is that in addition to its taste and aromatic properties, it has a biostimulating and antinicotinic effect, as well as a well-pronounced emulsion effect, which, in the case of soft drinks, avoids the need to use a synthetic emulsifier.
Изобретението се илюстрира със следните примерни приложения:The invention is illustrated by the following exemplary applications:
Пример 1.Example 1.
Смес от терпеноиди и флавоноиди от борова вършина / екстракт получен с алкален разтвор на етанол:хлороформ 1:1, изпаряване на разтворителя и по процедурата, описана по-горе - 0,056 об.%/ разтвор/; хлороформ - етанолен екстракт от плод хвойна или хвойново масло 15,484%об./разтвор/; ароматен дестилат за производство на джин 84,45%дб.Mixture of terpenoids and flavonoids from boron / extract obtained with an alkaline solution of ethanol: chloroform 1: 1, evaporation of the solvent and by the procedure described above - 0.056% (solution); chloroform - ethanol extract of juniper fruit or juniper oil 15,484% v / v /; aromatic distillate for the production of gin 84.45% dB.
Боровият екстракт и този от плод хвойна се разтварят в пропилен гликол-етанол и се смесват с ароматния дестилат за производство на джин.Бтанолният екстракт от плод хвойна се използва във вид на концентрат при смесването с ароматния дестилат за джин.Получените смеси се филтруват и се влагат в газирани безалкохолни напитки със съдържание на захар - 7-9% и винена киселина от 0,18 до 0,35% или се използват за приготвяне на сиропи за консумация със захар от 65 - 67° R и лимонтозу / винена киселина /1,5 - 3,5 %.The boron extract and juniper fruit extract were dissolved in propylene glycol-ethanol and mixed with the aromatic distillate to produce gin. used in carbonated soft drinks with a sugar content of 7-9% and tartaric acid from 0,18 to 0,35% or used for the preparation of syrups for consumption with sugar from 65 - 67 ° R and limontose / tartaric acid / 1 , 5 - 3.5%.
Пример2.Example 2.
Смес от терпеноиди и флавоноиди от екстракт от борова вършина с етанол-хлороформ /алкален разтвор/, получен след изпаряване на разтворителя , подкисляване , повторна екстракция с органичен разтворител / хлороформ /, - 0.055%об./разтвор/; етанолов екстракт от плод хвойна или хвойново масло - 16,65% /разтвор/ и ароматен дестилат за производство на сух джин - 77,73%об.Mixture of terpenoids and flavonoids from boron extract with ethanol-chloroform (alkaline solution), obtained after evaporation of the solvent, acidification, re-extraction with organic solvent (chloroform), 0.055% v / v /; ethanol extract of juniper fruit or juniper oil - 16.65% (solution) and aromatic distillate for the production of dry gin - 77.73% vol.
Смесванеето се осъществява както в Пример1.Mixing was carried out as in Example 1.
Пример З.Боровият екстракт е от 1-3 Mg / dm3, прибавен към водно-етанолен разтвор с концентрация на етанола 40% об . При желание може да се добави 1 - 2,5g/dm3 глицерин и захар l-5g/dm3 .Понататък се действа както в Пример!.Example 3. The boron extract is from 1-3 Mg / dm 3 added to an aqueous-ethanol solution with an ethanol concentration of 40% vol. If desired, may be added 1 - 2,5g / dm 3 glycerin and sugar l-5g / dm 3 .Ponatatak proceeding as in Example !.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| BG10110975A BG110975A (en) | 2011-06-17 | 2011-06-17 | Food supplement containing terpenoids and flavonoids from essential oil raw materials - extracts of pine twigs and juniper fruit |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| BG10110975A BG110975A (en) | 2011-06-17 | 2011-06-17 | Food supplement containing terpenoids and flavonoids from essential oil raw materials - extracts of pine twigs and juniper fruit |
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| Publication Number | Publication Date |
|---|---|
| BG110975A true BG110975A (en) | 2013-05-31 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| BG10110975A BG110975A (en) | 2011-06-17 | 2011-06-17 | Food supplement containing terpenoids and flavonoids from essential oil raw materials - extracts of pine twigs and juniper fruit |
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| Country | Link |
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| BG (1) | BG110975A (en) |
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