AT52847B - Process for the preparation of bromine diethyl acetylurea. - Google Patents
Process for the preparation of bromine diethyl acetylurea.Info
- Publication number
- AT52847B AT52847B AT52847DA AT52847B AT 52847 B AT52847 B AT 52847B AT 52847D A AT52847D A AT 52847DA AT 52847 B AT52847 B AT 52847B
- Authority
- AT
- Austria
- Prior art keywords
- preparation
- acetylurea
- bromine
- diethyl
- bromine diethyl
- Prior art date
Links
- -1 bromine diethyl acetylurea Chemical compound 0.000 title claims description 4
- 238000000034 method Methods 0.000 title description 3
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims description 4
- 229910021529 ammonia Inorganic materials 0.000 claims description 2
- OOGCXXAIEROJOL-UHFFFAOYSA-N CCN(CC)C(N(C1=NC=C1)Br)=O Chemical compound CCN(CC)C(N(C1=NC=C1)Br)=O OOGCXXAIEROJOL-UHFFFAOYSA-N 0.000 claims 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 description 1
- GDTBXPJZTBHREO-UHFFFAOYSA-N bromine Substances BrBr GDTBXPJZTBHREO-UHFFFAOYSA-N 0.000 description 1
- 229910052794 bromium Inorganic materials 0.000 description 1
- 239000004202 carbamide Substances 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
Landscapes
- Acyclic And Carbocyclic Compounds In Medicinal Compositions (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Description
<Desc/Clms Page number 1>
Verfahren zur Darstellung von Bromdiäthylazetylharnstoff. Das Stammpatent betrifft ein Verfahren zur Darstellung des Hromdiäthylazetytharn- stoffes der Formel :
EMI1.1
welches darin besteht, dass man Bromdiäthylazetylhaloide auf Harnstoff einwirken lässt. Es wurde nun gefunden, dass man diesen Körper auch dadurch erhalten kann, dass man Bromdiäthylazetylurethan mit Ammoniak behandelt.
EMI1.2
EMI1.3
EMI1.4
und dann mehrfach aus Alkohol umkrtstallisiert. Man erhält Bromdiäthylazetylharnstoff \om Schmelzpunkt 114 bis 118 C.
**WARNUNG** Ende DESC Feld kannt Anfang CLMS uberlappen**.
<Desc / Clms Page number 1>
Process for the preparation of bromine diethyl acetylurea. The parent patent relates to a process for the preparation of the Hromdiethylazetythurea of the formula:
EMI1.1
which consists in allowing bromine diethyl acetyl haloids to act on urea. It has now been found that this body can also be obtained by treating bromodiethylazetylurethane with ammonia.
EMI1.2
EMI1.3
EMI1.4
and then repeatedly converted from alcohol. Bromdiäthylazetylurea \ om melting point 114 to 118 C.
** WARNING ** End of DESC field may overlap beginning of CLMS **.
Claims (1)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE52845X | 1909-07-09 | ||
| DE52847X | 1909-07-09 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| AT52847B true AT52847B (en) | 1912-03-26 |
Family
ID=25749212
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| AT52847D AT52847B (en) | 1909-07-09 | 1910-06-06 | Process for the preparation of bromine diethyl acetylurea. |
Country Status (1)
| Country | Link |
|---|---|
| AT (1) | AT52847B (en) |
-
1910
- 1910-06-06 AT AT52847D patent/AT52847B/en active
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