AR122563A1 - Formas cristalinas de ciantraniliprol y proceso de preparación - Google Patents
Formas cristalinas de ciantraniliprol y proceso de preparaciónInfo
- Publication number
- AR122563A1 AR122563A1 ARP210101554A ARP210101554A AR122563A1 AR 122563 A1 AR122563 A1 AR 122563A1 AR P210101554 A ARP210101554 A AR P210101554A AR P210101554 A ARP210101554 A AR P210101554A AR 122563 A1 AR122563 A1 AR 122563A1
- Authority
- AR
- Argentina
- Prior art keywords
- degrees
- xrpd pattern
- cyantraniliprole
- crystalline
- peaks
- Prior art date
Links
- 238000002360 preparation method Methods 0.000 title 1
- 238000000634 powder X-ray diffraction Methods 0.000 abstract 6
- DVBUIBGJRQBEDP-UHFFFAOYSA-N cyantraniliprole Chemical group CNC(=O)C1=CC(C#N)=CC(C)=C1NC(=O)C1=CC(Br)=NN1C1=NC=CC=C1Cl DVBUIBGJRQBEDP-UHFFFAOYSA-N 0.000 abstract 5
- 239000007787 solid Substances 0.000 abstract 3
- 239000005889 Cyantraniliprole Substances 0.000 abstract 2
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 abstract 2
- BAVYZALUXZFZLV-UHFFFAOYSA-N Methylamine Chemical compound NC BAVYZALUXZFZLV-UHFFFAOYSA-N 0.000 abstract 2
- 238000001035 drying Methods 0.000 abstract 2
- 239000002904 solvent Substances 0.000 abstract 2
- INKMAGKGDPLJDP-UHFFFAOYSA-N 2-[5-bromo-2-(3-chloropyridin-2-yl)pyrazol-3-yl]-8-methyl-4-oxo-3,1-benzoxazine-6-carbonitrile Chemical compound CC1=CC(C#N)=CC(C(O2)=O)=C1N=C2C1=CC(Br)=NN1C1=NC=CC=C1Cl INKMAGKGDPLJDP-UHFFFAOYSA-N 0.000 abstract 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 abstract 1
- 238000009833 condensation Methods 0.000 abstract 1
- 230000005494 condensation Effects 0.000 abstract 1
- 238000001816 cooling Methods 0.000 abstract 1
- 238000001704 evaporation Methods 0.000 abstract 1
- 230000008020 evaporation Effects 0.000 abstract 1
- 238000001914 filtration Methods 0.000 abstract 1
- 238000004519 manufacturing process Methods 0.000 abstract 1
- 230000001376 precipitating effect Effects 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D401/00—Heterocyclic compounds containing two or more hetero rings, having nitrogen atoms as the only ring hetero atoms, at least one ring being a six-membered ring with only one nitrogen atom
- C07D401/02—Heterocyclic compounds containing two or more hetero rings, having nitrogen atoms as the only ring hetero atoms, at least one ring being a six-membered ring with only one nitrogen atom containing two hetero rings
- C07D401/04—Heterocyclic compounds containing two or more hetero rings, having nitrogen atoms as the only ring hetero atoms, at least one ring being a six-membered ring with only one nitrogen atom containing two hetero rings directly linked by a ring-member-to-ring-member bond
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/48—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with two nitrogen atoms as the only ring hetero atoms
- A01N43/56—1,2-Diazoles; Hydrogenated 1,2-diazoles
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01P—BIOCIDAL, PEST REPELLANT, PEST ATTRACTANT OR PLANT GROWTH REGULATORY ACTIVITY OF CHEMICAL COMPOUNDS OR PREPARATIONS
- A01P7/00—Arthropodicides
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
- C07B2200/00—Indexing scheme relating to specific properties of organic compounds
- C07B2200/13—Crystalline forms, e.g. polymorphs
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Wood Science & Technology (AREA)
- Engineering & Computer Science (AREA)
- Environmental Sciences (AREA)
- Zoology (AREA)
- Pest Control & Pesticides (AREA)
- Plant Pathology (AREA)
- General Health & Medical Sciences (AREA)
- Agronomy & Crop Science (AREA)
- Health & Medical Sciences (AREA)
- Dentistry (AREA)
- General Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Insects & Arthropods (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Plural Heterocyclic Compounds (AREA)
- Saccharide Compounds (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Pyrrole Compounds (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Abstract
Reivindicación 1: Una Forma C de ciantraniliprol cristalina, caracterizada por datos seleccionados de uno o más de los siguientes: un patrón de XRPD que tiene picos a 7,3, 8,2, 8,9, 14,7 y 20,3 grados 2 q ± 0,2 grados 2 q; un patrón de XRPD como se ilustra en la Figura 1. Reivindicación 3: Una Forma D de ciantraniliprol cristalina, caracterizada por datos seleccionados de uno o más de los siguientes: un patrón de XRPD que tiene picos a 6,6, 11,4, 15,7 y 22,4 grados 2 q ± 0,2 grados 2 q; un patrón de XRPD como se ilustra en la Figura 2. Reivindicación 5: Una Forma F de ciantraniliprol cristalina, caracterizada por datos seleccionados de uno o más de los siguientes: un patrón de XRPD que tiene picos a 9,6, 11,3, 18,6, 21,5 y 25,9 grados 2 q ± 0,2 grados 2 q; un patrón de XRPD como se ilustra en la Figura 3. Reivindicación 16: Un proceso de preparación de la forma cristalina de ciantraniliprol de acuerdo con la reivindicación 3 o la reivindicación 4, que comprende someter una solución de 2-[3-bromo-1-(3-cloro-2-piridinil)-1H-pirazol-5-ilo]-6-ciano-8-metilo-4H-3,1-benzoxazin-4-ona en un sistema de disolvente de éter a una reacción de condensación con metilamina seguida de evaporación, secando al vacío para obtener un sólido, en donde dicho sólido se disuelve además en un disolvente de alcohol, seguido por enfriamiento, precipitado, filtrado y secado al vacío para obtener dicha forma en estado sólido de ciantraniliprol.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US202063035865P | 2020-06-08 | 2020-06-08 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| AR122563A1 true AR122563A1 (es) | 2022-09-21 |
Family
ID=78845357
Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ARP210101554A AR122563A1 (es) | 2020-06-08 | 2021-06-08 | Formas cristalinas de ciantraniliprol y proceso de preparación |
| ARP210101555A AR122564A1 (es) | 2020-06-08 | 2021-06-08 | Proceso para la preparación de antranilamidas |
Family Applications After (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ARP210101555A AR122564A1 (es) | 2020-06-08 | 2021-06-08 | Proceso para la preparación de antranilamidas |
Country Status (12)
| Country | Link |
|---|---|
| US (2) | US20230312505A1 (es) |
| EP (2) | EP4165030A4 (es) |
| CN (2) | CN116490492A (es) |
| AR (2) | AR122563A1 (es) |
| AU (2) | AU2021287782A1 (es) |
| BR (2) | BR112022025068A2 (es) |
| CA (2) | CA3181797A1 (es) |
| CO (2) | CO2023000040A2 (es) |
| IL (2) | IL298905A (es) |
| MX (2) | MX2022015596A (es) |
| PE (2) | PE20231426A1 (es) |
| WO (2) | WO2021249396A1 (es) |
Families Citing this family (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113896714A (zh) * | 2021-11-23 | 2022-01-07 | 江西汇和化工有限公司 | 一种氯虫苯甲酰胺的合成方法 |
| AR131889A1 (es) * | 2023-02-21 | 2025-05-14 | Upl Ltd | Un proceso para la preparación de un compuesto de antranilamida e intermedios del mismo |
| WO2024189625A1 (en) | 2023-03-15 | 2024-09-19 | Adama Makhteshim Ltd. | Aqueous suspension composition of cyantraniliprole and acetamiprid |
| CN118812502A (zh) * | 2023-04-17 | 2024-10-22 | 利尔化学股份有限公司 | 一种双酰胺类杀虫剂及其中间体的制备方法 |
| WO2025104727A1 (en) | 2023-11-16 | 2025-05-22 | Adama Makhteshim Ltd. | Solid state forms of cyantraniliprole and uses thereof |
| CN118146190A (zh) * | 2024-02-01 | 2024-06-07 | 南开大学 | 溴氰虫酰胺的新晶型及其制备方法和应用 |
Family Cites Families (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| IN243219B (es) * | 2003-01-28 | 2010-10-01 | Du Pont | |
| MY140912A (en) * | 2004-07-26 | 2010-01-29 | Du Pont | Mixtures of anthranilamide invertebrate pest control agents |
| TWI363756B (en) * | 2004-12-07 | 2012-05-11 | Du Pont | Method for preparing n-phenylpyrazole-1-carboxamides |
| TWI395728B (zh) * | 2006-12-06 | 2013-05-11 | Du Pont | 製備２-胺基-５-氰基苯甲酸衍生物之方法 |
| BRPI0817168A2 (pt) * | 2007-11-08 | 2015-03-31 | Du Pont | "método para a preparação de um composto" |
| CN101550130B (zh) * | 2008-04-01 | 2012-11-07 | 中国中化股份有限公司 | 一种制备3-卤代-1-(3-氯-2-吡啶基)-1h-吡唑-5-甲酰卤的方法 |
| RU2500676C2 (ru) * | 2008-11-14 | 2013-12-10 | Е.И.Дюпон Де Немур Энд Компани | Способ получения негидратируемой кристаллической формы |
| CN102020633B (zh) * | 2009-09-21 | 2013-08-07 | 中国中化股份有限公司 | 一种1-(3,5-二氯吡啶-2-基)-吡唑甲酰胺类化合物的制备方法 |
| CN110028489B (zh) * | 2018-01-12 | 2021-08-06 | 沈阳中化农药化工研发有限公司 | 一种减压法制备苯甲酰胺类化合物的方法 |
| WO2019207595A1 (en) * | 2018-04-23 | 2019-10-31 | Natco Pharma Limited | An improved process for the preparation of anthranilamide derivatives |
| CN112552284B (zh) * | 2020-12-18 | 2022-08-12 | 重庆华歌生物化学有限公司 | 一种氯虫苯甲酰胺的制备方法 |
-
2021
- 2021-06-08 CN CN202180058429.4A patent/CN116490492A/zh active Pending
- 2021-06-08 AR ARP210101554A patent/AR122563A1/es unknown
- 2021-06-08 IL IL298905A patent/IL298905A/en unknown
- 2021-06-08 US US18/009,066 patent/US20230312505A1/en active Pending
- 2021-06-08 PE PE2022002884A patent/PE20231426A1/es unknown
- 2021-06-08 BR BR112022025068A patent/BR112022025068A2/pt unknown
- 2021-06-08 IL IL298908A patent/IL298908A/en unknown
- 2021-06-08 WO PCT/CN2021/098904 patent/WO2021249396A1/en not_active Ceased
- 2021-06-08 AU AU2021287782A patent/AU2021287782A1/en not_active Abandoned
- 2021-06-08 US US18/009,072 patent/US20230348414A1/en active Pending
- 2021-06-08 CA CA3181797A patent/CA3181797A1/en active Pending
- 2021-06-08 CN CN202180058527.8A patent/CN116490491A/zh active Pending
- 2021-06-08 PE PE2022002880A patent/PE20231381A1/es unknown
- 2021-06-08 AR ARP210101555A patent/AR122564A1/es unknown
- 2021-06-08 AU AU2021286610A patent/AU2021286610A1/en active Pending
- 2021-06-08 EP EP21820820.5A patent/EP4165030A4/en active Pending
- 2021-06-08 MX MX2022015596A patent/MX2022015596A/es unknown
- 2021-06-08 WO PCT/CN2021/098903 patent/WO2021249395A1/en not_active Ceased
- 2021-06-08 EP EP21821439.3A patent/EP4165031A4/en active Pending
- 2021-06-08 CA CA3181785A patent/CA3181785A1/en active Pending
- 2021-06-08 MX MX2022015597A patent/MX2022015597A/es unknown
- 2021-06-08 BR BR112022025066A patent/BR112022025066A2/pt unknown
-
2023
- 2023-01-03 CO CONC2023/0000040A patent/CO2023000040A2/es unknown
- 2023-01-03 CO CONC2023/0000039A patent/CO2023000039A2/es unknown
Also Published As
| Publication number | Publication date |
|---|---|
| WO2021249396A1 (en) | 2021-12-16 |
| EP4165030A4 (en) | 2024-07-31 |
| MX2022015597A (es) | 2023-02-01 |
| EP4165030A1 (en) | 2023-04-19 |
| MX2022015596A (es) | 2023-02-01 |
| IL298905A (en) | 2023-02-01 |
| AU2021287782A1 (en) | 2023-02-02 |
| BR112022025066A2 (pt) | 2023-03-07 |
| CA3181797A1 (en) | 2021-12-16 |
| CN116490491A (zh) | 2023-07-25 |
| CA3181785A1 (en) | 2021-12-16 |
| BR112022025068A2 (pt) | 2023-03-07 |
| CO2023000040A2 (es) | 2023-03-27 |
| US20230348414A1 (en) | 2023-11-02 |
| EP4165031A1 (en) | 2023-04-19 |
| PE20231426A1 (es) | 2023-09-13 |
| CN116490492A (zh) | 2023-07-25 |
| US20230312505A1 (en) | 2023-10-05 |
| WO2021249395A1 (en) | 2021-12-16 |
| EP4165031A4 (en) | 2024-09-25 |
| AR122564A1 (es) | 2022-09-21 |
| AU2021286610A1 (en) | 2023-01-19 |
| PE20231381A1 (es) | 2023-09-07 |
| IL298908A (en) | 2023-02-01 |
| CO2023000039A2 (es) | 2023-03-27 |
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