AR098942A1 - Procedimiento de preparación de un material adsorbente conformado en ausencia de aglutinante, y procedimiento de extracción de litio a partir de soluciones salinas que utilizan dicho material - Google Patents
Procedimiento de preparación de un material adsorbente conformado en ausencia de aglutinante, y procedimiento de extracción de litio a partir de soluciones salinas que utilizan dicho materialInfo
- Publication number
- AR098942A1 AR098942A1 ARP140104889A ARP140104889A AR098942A1 AR 098942 A1 AR098942 A1 AR 098942A1 AR P140104889 A ARP140104889 A AR P140104889A AR P140104889 A ARP140104889 A AR P140104889A AR 098942 A1 AR098942 A1 AR 098942A1
- Authority
- AR
- Argentina
- Prior art keywords
- stage
- procedure
- lithium
- binder
- absence
- Prior art date
Links
- WHXSMMKQMYFTQS-UHFFFAOYSA-N Lithium Chemical compound [Li] WHXSMMKQMYFTQS-UHFFFAOYSA-N 0.000 title abstract 4
- 229910052744 lithium Inorganic materials 0.000 title abstract 4
- 238000000034 method Methods 0.000 title abstract 4
- 239000000463 material Substances 0.000 title abstract 3
- 238000000605 extraction Methods 0.000 title abstract 2
- 239000003463 adsorbent Substances 0.000 title 1
- KWGKDLIKAYFUFQ-UHFFFAOYSA-M lithium chloride Chemical compound [Li+].[Cl-] KWGKDLIKAYFUFQ-UHFFFAOYSA-M 0.000 abstract 6
- 238000001035 drying Methods 0.000 abstract 3
- 239000011343 solid material Substances 0.000 abstract 3
- 239000000725 suspension Substances 0.000 abstract 2
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 abstract 1
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 abstract 1
- 239000012736 aqueous medium Substances 0.000 abstract 1
- 239000011230 binding agent Substances 0.000 abstract 1
- 238000001125 extrusion Methods 0.000 abstract 1
- 238000001914 filtration Methods 0.000 abstract 1
- 238000004519 manufacturing process Methods 0.000 abstract 1
- 238000002156 mixing Methods 0.000 abstract 1
- 239000011780 sodium chloride Substances 0.000 abstract 1
Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
- B01J20/06—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising oxides or hydroxides of metals not provided for in group B01J20/04
- B01J20/08—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising oxides or hydroxides of metals not provided for in group B01J20/04 comprising aluminium oxide or hydroxide; comprising bauxite
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
- B01D15/08—Selective adsorption, e.g. chromatography
- B01D15/26—Selective adsorption, e.g. chromatography characterised by the separation mechanism
- B01D15/36—Selective adsorption, e.g. chromatography characterised by the separation mechanism involving ionic interaction, e.g. ion-exchange, ion-pair, ion-suppression or ion-exclusion
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
- B01J20/04—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising compounds of alkali metals, alkaline earth metals or magnesium
- B01J20/046—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising compounds of alkali metals, alkaline earth metals or magnesium containing halogens, e.g. halides
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/30—Processes for preparing, regenerating, or reactivating
- B01J20/3007—Moulding, shaping or extruding
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/30—Processes for preparing, regenerating, or reactivating
- B01J20/3078—Thermal treatment, e.g. calcining or pyrolizing
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/30—Processes for preparing, regenerating, or reactivating
- B01J20/3085—Chemical treatments not covered by groups B01J20/3007 - B01J20/3078
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
- C01D15/00—Lithium compounds
- C01D15/04—Halides
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
- C01F7/00—Compounds of aluminium
- C01F7/02—Aluminium oxide; Aluminium hydroxide; Aluminates
- C01F7/04—Preparation of alkali metal aluminates; Aluminium oxide or hydroxide therefrom
- C01F7/043—Lithium aluminates
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/28—Treatment of water, waste water, or sewage by sorption
- C02F1/281—Treatment of water, waste water, or sewage by sorption using inorganic sorbents
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2220/00—Aspects relating to sorbent materials
- B01J2220/50—Aspects relating to the use of sorbent or filter aid materials
- B01J2220/58—Use in a single column
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2002/00—Crystal-structural characteristics
- C01P2002/70—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
- C01P2002/72—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data by d-values or two theta-values, e.g. as X-ray diagram
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/12—Surface area
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Analytical Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Life Sciences & Earth Sciences (AREA)
- Thermal Sciences (AREA)
- Physics & Mathematics (AREA)
- Geology (AREA)
- Hydrology & Water Resources (AREA)
- Environmental & Geological Engineering (AREA)
- Water Supply & Treatment (AREA)
- Solid-Sorbent Or Filter-Aiding Compositions (AREA)
- Nitrogen And Oxygen Or Sulfur-Condensed Heterocyclic Ring Systems (AREA)
Abstract
Se describe un procedimiento de preparación de un material sólido cristalizado de fórmula LiCl.2AI(OH)₃,nH₂O con n que está comprendido entre 0,01 y 10, donde dicho procedimiento comprende al menos las etapas siguientes: a) una etapa de mezcla, en medio acuoso, de al menos una fuente de alúmina y de, al menos, una fuente de litio, para obtener una suspensión, b) una etapa de filtración de la suspensión obtenida en la etapa a) para obtener una pasta, c) una etapa de secado de la pasta obtenida como resultado de la etapa b), a una temperatura comprendida entre 20 y 80ºC durante un lapso comprendido entre 1 h y 12 h, d) una etapa de conformado por extrusión de dicha pasta secada, directamente después de la etapa c) de secado para obtener extruídos. donde dicha etapa d) de conformado se realiza en ausencia de aglutinante, y e) el secado de los extruídos obtenidos a una temperatura comprendida entre 20 y 200ºC durante un lapso comprendido entre 1 hora y 20 horas, para obtener el material sólido cristalizado de fórmula LiCl.2AI(OH)₃,nH₂O en forma de extruídos. La presente se refiere también a un procedimiento de extracción de litio a partir de soluciones salinas que utilizan el material así preparado. La presente se refiere a un material sólido cristalizado de fórmula LiCl.2Al(OH)₃,nH₂O con n que está comprendido entre 0.01 y 10, conformado. La presente se refiere también a un dispositivo que emplea el procedimiento de extracción de litio.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR1363465A FR3015456B1 (fr) | 2013-12-23 | 2013-12-23 | Procede de preparation d'un materiau adsorbant mis en forme en l'absence de liant et procede d'extraction de lithium a partir de solutions salines utilisant ledit materiau |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| AR098942A1 true AR098942A1 (es) | 2016-06-22 |
Family
ID=50290058
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ARP140104889A AR098942A1 (es) | 2013-12-23 | 2014-12-23 | Procedimiento de preparación de un material adsorbente conformado en ausencia de aglutinante, y procedimiento de extracción de litio a partir de soluciones salinas que utilizan dicho material |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US20160317998A1 (es) |
| EP (1) | EP3086874B1 (es) |
| CN (1) | CN106102902A (es) |
| AR (1) | AR098942A1 (es) |
| CL (1) | CL2016001601A1 (es) |
| FR (1) | FR3015456B1 (es) |
| WO (1) | WO2015097202A1 (es) |
Families Citing this family (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR3051787B1 (fr) | 2016-05-25 | 2022-07-08 | Eramet | Procede de preparation d'un materiau adsorbant et procede d'extraction de lithium utilisant ledit materiau |
| US11365128B2 (en) | 2017-06-15 | 2022-06-21 | Energysource Minerals Llc | Process for selective adsorption and recovery of lithium from natural and synthetic brines |
| US10604414B2 (en) | 2017-06-15 | 2020-03-31 | Energysource Minerals Llc | System and process for recovery of lithium from a geothermal brine |
| CN109759006B (zh) * | 2017-11-09 | 2022-05-13 | 比亚迪股份有限公司 | 一种锂吸附剂及其制备方法和应用以及一种从盐湖卤水中提取锂的方法 |
| CN110102273B (zh) * | 2018-02-01 | 2022-06-10 | 比亚迪股份有限公司 | 一种锂吸附剂及其制备方法和应用以及一种从含锂溶液中提取锂的方法 |
| CN110961070A (zh) * | 2018-09-30 | 2020-04-07 | 比亚迪股份有限公司 | 一种锂吸附剂及其制备方法 |
| CN111111603B (zh) * | 2018-10-31 | 2021-09-21 | 比亚迪股份有限公司 | 锂吸附体复合颗粒及其制备方法 |
| WO2020219625A1 (en) * | 2019-04-25 | 2020-10-29 | Saint-Gobain Ceramics & Plastics, Inc. | Adsorbent particles and methods of forming thereof |
| US11904297B1 (en) | 2023-01-11 | 2024-02-20 | Iliad Ip Company, Llc | Process for manufacturing lithium selective adsorption/separation media |
| JP2023006193A (ja) * | 2021-06-30 | 2023-01-18 | 住友金属鉱山株式会社 | リチウム吸着用造粒体の製造方法 |
| CN115739004B (zh) * | 2022-11-25 | 2024-04-16 | 中国科学院青海盐湖研究所 | 利用高镁锂比盐湖卤水制备的锂铝吸附材料及其方法 |
| WO2025018907A1 (ru) * | 2023-07-17 | 2025-01-23 | Акционерное общество "Аксион - Редкие и Драгоценные Металлы" | Сорбент для извлечения лития из литийсодержащих растворов и способ его получения |
Family Cites Families (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5114689A (en) * | 1987-10-05 | 1992-05-19 | Uop | Integrated process for the removal of sulfur compounds from fluid streams |
| WO1994019280A1 (fr) * | 1993-02-16 | 1994-09-01 | Nauchno-Proizvodstvennoe Aktsionernoe Obschestvo 'ekostar' | Procede d'obtention de chlorure de lithium a partir de solutions et son dispositif de mise en ×uvre |
| US5599516A (en) | 1993-05-24 | 1997-02-04 | Fmc Corporation | Recovery of lithium values from brines |
| US6280963B1 (en) * | 1997-11-07 | 2001-08-28 | Millennium Pharmaceuticals, Inc. | Essential fungal genes and their use |
| CN1243112A (zh) | 1999-08-23 | 2000-02-02 | 李凤杰 | 多元增效氮肥添加剂及其制备方法 |
| DE10197095D2 (de) * | 2001-10-25 | 2004-09-16 | Eurosina Technology Consulting | Verfahren zur Herstellung von granuliertem Sorbensmittel und Anlage zur Durchführung des Verfahrens |
| RU2234367C1 (ru) * | 2002-12-15 | 2004-08-20 | Закрытое акционерное общество "Экостар-Наутех" | Способ получения сорбента для извлечения лития из рассолов |
| CN1243112C (zh) * | 2002-12-27 | 2006-02-22 | 中国科学院青海盐湖研究所 | 吸附法从盐湖卤水中提取锂的方法 |
| CN101821201A (zh) * | 2007-09-17 | 2010-09-01 | 阿海珐联合服务有限责任公司 | 从含水介质中去除铝氧化物的方法 |
| US8753594B1 (en) * | 2009-11-13 | 2014-06-17 | Simbol, Inc. | Sorbent for lithium extraction |
| CN101829538B (zh) * | 2010-05-19 | 2013-06-26 | 浙江海虹控股集团有限公司 | 一种高性能锂吸附剂的制备方法 |
| CN102631897B (zh) * | 2012-02-14 | 2015-03-25 | 西安蓝晓科技新材料股份有限公司 | 一种制备锂吸附剂树脂的方法 |
-
2013
- 2013-12-23 FR FR1363465A patent/FR3015456B1/fr not_active Expired - Fee Related
-
2014
- 2014-12-23 EP EP14816318.1A patent/EP3086874B1/fr active Active
- 2014-12-23 WO PCT/EP2014/079118 patent/WO2015097202A1/fr not_active Ceased
- 2014-12-23 AR ARP140104889A patent/AR098942A1/es active IP Right Grant
- 2014-12-23 CN CN201480070791.3A patent/CN106102902A/zh active Pending
- 2014-12-23 US US15/107,453 patent/US20160317998A1/en not_active Abandoned
-
2016
- 2016-06-21 CL CL2016001601A patent/CL2016001601A1/es unknown
Also Published As
| Publication number | Publication date |
|---|---|
| US20160317998A1 (en) | 2016-11-03 |
| FR3015456B1 (fr) | 2017-05-19 |
| EP3086874A1 (fr) | 2016-11-02 |
| CL2016001601A1 (es) | 2016-12-09 |
| FR3015456A1 (fr) | 2015-06-26 |
| WO2015097202A1 (fr) | 2015-07-02 |
| CN106102902A (zh) | 2016-11-09 |
| EP3086874B1 (fr) | 2018-11-28 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FG | Grant, registration |