NO813242L - Fremgangsmaate til fremstilling av vinylkloridpolymerer - Google Patents

Fremgangsmaate til fremstilling av vinylkloridpolymerer

Info

Publication number: NO813242L
Authority: NO; Norway
Prior art keywords: oxazoline; weight; percent; propyl; copolymer
Prior art date: 1980-09-25

Application number

NO813242A

Other languages

English (en)

Norwegian (no)

Inventor

Gilberg Sielfeld

Paul Sunder-Plassmann

Original Assignee

Huels Chemische Werke Ag

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1980-09-25

Filing date

1981-09-23

Publication date

1982-03-26

1980-09-25 Priority claimed from DE19803036127 external-priority patent/DE3036127C2/de

1980-09-25 Priority claimed from DE19803036101 external-priority patent/DE3036101A1/de

1981-09-23 Application filed by Huels Chemische Werke Ag filed Critical Huels Chemische Werke Ag

1982-03-26 Publication of NO813242L publication Critical patent/NO813242L/no

Links

238000000034 method Methods 0.000 title claims description 23
BZHJMEDXRYGGRV-UHFFFAOYSA-N Vinyl chloride Chemical compound ClC=C BZHJMEDXRYGGRV-UHFFFAOYSA-N 0.000 title claims description 9
229920000642 polymer Polymers 0.000 title description 4
238000002360 preparation method Methods 0.000 title description 3
229920001577 copolymer Polymers 0.000 claims description 36
KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 claims description 27
239000000725 suspension Substances 0.000 claims description 19
239000003381 stabilizer Substances 0.000 claims description 18
239000000178 monomer Substances 0.000 claims description 15
-1 methylhydroxyethyl Chemical group 0.000 claims description 12
229920002689 polyvinyl acetate Polymers 0.000 claims description 12
239000000203 mixture Substances 0.000 claims description 11
229920005989 resin Polymers 0.000 claims description 11
239000011347 resin Substances 0.000 claims description 11
239000007864 aqueous solution Substances 0.000 claims description 10
IMSODMZESSGVBE-UHFFFAOYSA-N 2-Oxazoline Chemical compound C1CN=CO1 IMSODMZESSGVBE-UHFFFAOYSA-N 0.000 claims description 9
230000007062 hydrolysis Effects 0.000 claims description 8
238000006460 hydrolysis reaction Methods 0.000 claims description 8
239000011118 polyvinyl acetate Substances 0.000 claims description 8
239000000243 solution Substances 0.000 claims description 8
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 8
238000004519 manufacturing process Methods 0.000 claims description 6
125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 claims description 5
229920002678 cellulose Polymers 0.000 claims description 4
239000001913 cellulose Substances 0.000 claims description 4
229920003086 cellulose ether Polymers 0.000 claims description 4
230000000379 polymerizing effect Effects 0.000 claims description 3
239000007900 aqueous suspension Substances 0.000 claims description 2
239000003054 catalyst Substances 0.000 claims description 2
125000001449 isopropyl group Chemical group [H]C([H])([H])C([H])(*)C([H])([H])[H] 0.000 claims description 2
125000004123 n-propyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])* 0.000 claims 1
125000001436 propyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])[H] 0.000 claims 1
229920000915 polyvinyl chloride Polymers 0.000 description 17
239000004800 polyvinyl chloride Substances 0.000 description 17
VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 description 9
239000000084 colloidal system Substances 0.000 description 6
230000001681 protective effect Effects 0.000 description 6
XZIIFPSPUDAGJM-UHFFFAOYSA-N 6-chloro-2-n,2-n-diethylpyrimidine-2,4-diamine Chemical compound CCN(CC)C1=NC(N)=CC(Cl)=N1 XZIIFPSPUDAGJM-UHFFFAOYSA-N 0.000 description 5
229940035044 sorbitan monolaurate Drugs 0.000 description 5
URLKBWYHVLBVBO-UHFFFAOYSA-N Para-Xylene Chemical group CC1=CC=C(C)C=C1 URLKBWYHVLBVBO-UHFFFAOYSA-N 0.000 description 4
238000006116 polymerization reaction Methods 0.000 description 4
241000251468 Actinopterygii Species 0.000 description 3
YMWUJEATGCHHMB-UHFFFAOYSA-N Dichloromethane Chemical compound ClCCl YMWUJEATGCHHMB-UHFFFAOYSA-N 0.000 description 3
BJQHLKABXJIVAM-UHFFFAOYSA-N bis(2-ethylhexyl) phthalate Chemical compound CCCCC(CC)COC(=O)C1=CC=CC=C1C(=O)OCC(CC)CCCC BJQHLKABXJIVAM-UHFFFAOYSA-N 0.000 description 3
235000010980 cellulose Nutrition 0.000 description 3
238000010438 heat treatment Methods 0.000 description 3
239000003999 initiator Substances 0.000 description 3
239000000126 substance Substances 0.000 description 3
238000010557 suspension polymerization reaction Methods 0.000 description 3
IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
239000004803 Di-2ethylhexylphthalate Substances 0.000 description 2
YIVJZNGAASQVEM-UHFFFAOYSA-N Lauroyl peroxide Chemical compound CCCCCCCCCCCC(=O)OOC(=O)CCCCCCCCCCC YIVJZNGAASQVEM-UHFFFAOYSA-N 0.000 description 2
QQONPFPTGQHPMA-UHFFFAOYSA-N Propene Chemical compound CC=C QQONPFPTGQHPMA-UHFFFAOYSA-N 0.000 description 2
XTXRWKRVRITETP-UHFFFAOYSA-N Vinyl acetate Chemical compound CC(=O)OC=C XTXRWKRVRITETP-UHFFFAOYSA-N 0.000 description 2
239000002253 acid Substances 0.000 description 2
QWVBGCWRHHXMRM-UHFFFAOYSA-N hexadecoxycarbonyloxy hexadecyl carbonate Chemical compound CCCCCCCCCCCCCCCCOC(=O)OOC(=O)OCCCCCCCCCCCCCCCC QWVBGCWRHHXMRM-UHFFFAOYSA-N 0.000 description 2
150000002500 ions Chemical class 0.000 description 2
239000012071 phase Substances 0.000 description 2
229920002451 polyvinyl alcohol Polymers 0.000 description 2
235000019422 polyvinyl alcohol Nutrition 0.000 description 2
238000003756 stirring Methods 0.000 description 2
239000004094 surface-active agent Substances 0.000 description 2
AZUYLZMQTIKGSC-UHFFFAOYSA-N 1-[6-[4-(5-chloro-6-methyl-1H-indazol-4-yl)-5-methyl-3-(1-methylindazol-5-yl)pyrazol-1-yl]-2-azaspiro[3.3]heptan-2-yl]prop-2-en-1-one Chemical compound ClC=1C(=C2C=NNC2=CC=1C)C=1C(=NN(C=1C)C1CC2(CN(C2)C(C=C)=O)C1)C=1C=C2C=NN(C2=CC=1)C AZUYLZMQTIKGSC-UHFFFAOYSA-N 0.000 description 1
SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 description 1
OEPOKWHJYJXUGD-UHFFFAOYSA-N 2-(3-phenylmethoxyphenyl)-1,3-thiazole-4-carbaldehyde Chemical compound O=CC1=CSC(C=2C=C(OCC=3C=CC=CC=3)C=CC=2)=N1 OEPOKWHJYJXUGD-UHFFFAOYSA-N 0.000 description 1
NIXOWILDQLNWCW-UHFFFAOYSA-N 2-Propenoic acid Natural products OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 description 1
ATRRKUHOCOJYRX-UHFFFAOYSA-N Ammonium bicarbonate Chemical compound [NH4+].OC([O-])=O ATRRKUHOCOJYRX-UHFFFAOYSA-N 0.000 description 1
229910000013 Ammonium bicarbonate Inorganic materials 0.000 description 1
OMPJBNCRMGITSC-UHFFFAOYSA-N Benzoylperoxide Chemical group C=1C=CC=CC=1C(=O)OOC(=O)C1=CC=CC=C1 OMPJBNCRMGITSC-UHFFFAOYSA-N 0.000 description 1
VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 1
239000004129 EU approved improving agent Substances 0.000 description 1
VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 description 1
239000005977 Ethylene Substances 0.000 description 1
108010010803 Gelatin Proteins 0.000 description 1
229920002153 Hydroxypropyl cellulose Polymers 0.000 description 1
239000004372 Polyvinyl alcohol Substances 0.000 description 1
229920002472 Starch Polymers 0.000 description 1
150000007513 acids Chemical class 0.000 description 1
239000001361 adipic acid Substances 0.000 description 1
235000011037 adipic acid Nutrition 0.000 description 1
229920013820 alkyl cellulose Polymers 0.000 description 1
125000000217 alkyl group Chemical group 0.000 description 1
235000012538 ammonium bicarbonate Nutrition 0.000 description 1
239000001099 ammonium carbonate Substances 0.000 description 1
150000008064 anhydrides Chemical class 0.000 description 1
239000008346 aqueous phase Substances 0.000 description 1
125000000751 azo group Chemical group [*]N=N[*] 0.000 description 1
125000004432 carbon atom Chemical group C* 0.000 description 1
150000001735 carboxylic acids Chemical class 0.000 description 1
238000005119 centrifugation Methods 0.000 description 1
BSVQJWUUZCXSOL-UHFFFAOYSA-N cyclohexylsulfonyl ethaneperoxoate Chemical compound CC(=O)OOS(=O)(=O)C1CCCCC1 BSVQJWUUZCXSOL-UHFFFAOYSA-N 0.000 description 1
238000007872 degassing Methods 0.000 description 1
239000012933 diacyl peroxide Substances 0.000 description 1
125000003438 dodecyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 description 1
238000011156 evaluation Methods 0.000 description 1
230000002349 favourable effect Effects 0.000 description 1
239000007789 gas Substances 0.000 description 1
229920000159 gelatin Polymers 0.000 description 1
239000008273 gelatin Substances 0.000 description 1
235000019322 gelatine Nutrition 0.000 description 1
235000011852 gelatine desserts Nutrition 0.000 description 1
WNLRTRBMVRJNCN-UHFFFAOYSA-N hexanedioic acid Natural products OC(=O)CCCCC(O)=O WNLRTRBMVRJNCN-UHFFFAOYSA-N 0.000 description 1
229920013821 hydroxy alkyl cellulose Polymers 0.000 description 1
235000010977 hydroxypropyl cellulose Nutrition 0.000 description 1
230000003993 interaction Effects 0.000 description 1
150000002605 large molecules Chemical class 0.000 description 1
FPYJFEHAWHCUMM-UHFFFAOYSA-N maleic anhydride Chemical compound O=C1OC(=O)C=C1 FPYJFEHAWHCUMM-UHFFFAOYSA-N 0.000 description 1
238000010907 mechanical stirring Methods 0.000 description 1
VUQUOGPMUUJORT-UHFFFAOYSA-N methyl 4-methylbenzenesulfonate Chemical compound COS(=O)(=O)C1=CC=C(C)C=C1 VUQUOGPMUUJORT-UHFFFAOYSA-N 0.000 description 1
238000002156 mixing Methods 0.000 description 1
150000005673 monoalkenes Chemical class 0.000 description 1
125000004108 n-butyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 description 1
229910052757 nitrogen Inorganic materials 0.000 description 1
239000012299 nitrogen atmosphere Substances 0.000 description 1
125000005634 peroxydicarbonate group Chemical group 0.000 description 1
239000004014 plasticizer Substances 0.000 description 1
238000010992 reflux Methods 0.000 description 1
239000002904 solvent Substances 0.000 description 1
229910001220 stainless steel Inorganic materials 0.000 description 1
239000010935 stainless steel Substances 0.000 description 1
239000008107 starch Substances 0.000 description 1
235000019698 starch Nutrition 0.000 description 1
OPQYOFWUFGEMRZ-UHFFFAOYSA-N tert-butyl 2,2-dimethylpropaneperoxoate Chemical compound CC(C)(C)OOC(=O)C(C)(C)C OPQYOFWUFGEMRZ-UHFFFAOYSA-N 0.000 description 1
GJBRNHKUVLOCEB-UHFFFAOYSA-N tert-butyl benzenecarboperoxoate Chemical compound CC(C)(C)OOC(=O)C1=CC=CC=C1 GJBRNHKUVLOCEB-UHFFFAOYSA-N 0.000 description 1
229920001567 vinyl ester resin Polymers 0.000 description 1
125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F14/00—Homopolymers and copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen
- C08F14/02—Monomers containing chlorine
- C08F14/04—Monomers containing two carbon atoms
- C08F14/06—Vinyl chloride

Landscapes

Chemical & Material Sciences (AREA)
Health & Medical Sciences (AREA)
Chemical Kinetics & Catalysis (AREA)
Medicinal Chemistry (AREA)
Polymers & Plastics (AREA)
Organic Chemistry (AREA)
Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)

NO813242A 1980-09-25 1981-09-23 Fremgangsmaate til fremstilling av vinylkloridpolymerer NO813242L (no)

Applications Claiming Priority (2)

Application Number	Priority Date	Filing Date	Title
DE19803036127 DE3036127C2 (de)	1980-09-25	1980-09-25	Verfahren zur Herstellung von Vinylchlorid-Polymeren
DE19803036101 DE3036101A1 (de)	1980-09-25	1980-09-25	Verfahren zur herstellung von vinylchlorid-polymeren

Publications (1)

Publication Number	Publication Date
NO813242L true NO813242L (no)	1982-03-26

Family

ID=25788069

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
NO813242A NO813242L (no)	1980-09-25	1981-09-23	Fremgangsmaate til fremstilling av vinylkloridpolymerer

Country Status (5)

Country	Link
US (1)	US4368307A (pt)
EP (1)	EP0048842B1 (pt)
BR (1)	BR8106113A (pt)
DE (1)	DE3167717D1 (pt)
NO (1)	NO813242L (pt)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
DE3120358A1 (de)	1981-05-22	1982-12-09	Chemische Werke Hüls AG, 4370 Marl	Verfahren zur herstellung von polymeren und copolymeren des vinylchlorids
US5849831A (en) *	1996-04-19	1998-12-15	Kuraray Co., Ltd.	Process for producing vinyl resin
JP5081623B2 (ja) *	2005-09-01	2012-11-28	独立行政法人科学技術振興機構	オキサゾリンのランダム共重合体

Family Cites Families (7)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
GB991134A (en)	1961-03-23	1965-05-05	Wacker Chemie Gmbh	Process for the manufacture of vinyl chloride polymers
DE1263300B (de)	1965-10-13	1968-03-14	Huels Chemische Werke Ag	Verfahren zur Polymerisation von delta 2-Oxazolinen
FR1530343A (fr) *	1966-07-07	1968-06-21	Commercial Solvents Corp	Composition à base de résine halogénure de vinyle et procédé pour sa préparation
GB1165570A (en) *	1966-12-08	1969-10-01	Agfa Gevaert Nv	Photopolymerization of Ethylenically Unsaturated Compounds
DE2227887A1 (de) *	1972-06-08	1973-12-20	Huels Chemische Werke Ag	Verfahren zur herstellung von vinylchlorid-copolymerisaten in waessriger suspension
DE2234038C3 (de) *	1972-07-11	1978-05-18	Wacker-Chemie Gmbh, 8000 Muenchen	Verfahren zur Polymerisation von Vinylchlorid
DE2629880B2 (de)	1976-07-02	1980-10-16	Wacker-Chemie Gmbh, 8000 Muenchen	Verfahren zur Herstellung von Polyvinylchlorid nach dem Suspensionsverfahren

1981
- 1981-09-07 EP EP81106996A patent/EP0048842B1/de not_active Expired
- 1981-09-07 DE DE8181106996T patent/DE3167717D1/de not_active Expired
- 1981-09-11 US US06/301,270 patent/US4368307A/en not_active Expired - Fee Related
- 1981-09-23 NO NO813242A patent/NO813242L/no unknown
- 1981-09-24 BR BR8106113A patent/BR8106113A/pt unknown

Also Published As

Publication number	Publication date
EP0048842A2 (de)	1982-04-07
EP0048842A3 (en)	1982-05-12
DE3167717D1 (en)	1985-01-24
US4368307A (en)	1983-01-11
EP0048842B1 (de)	1984-12-12
BR8106113A (pt)	1982-06-15

Publication	Publication Date	Title
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AU689621B2 (en)	1998-04-02	Suspending agent for suspension polymerization of vinyl compound
US3701742A (en)	1972-10-31	Vinyl chloride polymers and method of preparing same
JPS582962B2 (ja)	1983-01-19	塩化ビニル系樹脂の製造方法
NO813242L (no)	1982-03-26	Fremgangsmaate til fremstilling av vinylkloridpolymerer
EP0421150B1 (en)	1994-08-17	Dispersant system for making low-colour chlorinated polyvinyl chloride
JP3339257B2 (ja)	2002-10-28	塩化ビニル系樹脂組成物
CN109843946A (zh)	2019-06-04	偏二氟乙烯聚合物
US5908905A (en)	1999-06-01	Polymerization of vinyl chloride with t-butyl peroxyneoheptanoate and perester peroxide
US3627853A (en)	1971-12-14	Chlorination of vinyl chloride block copolymers
US4438244A (en)	1984-03-20	Process for the production of polymers and copolymers of vinyl chloride
US3836510A (en)	1974-09-17	Vinyl halide terpolymer and bulk process for preparation
NO864121L (no)	1987-04-21	Fremgangsmaate til fremstilling av polyvinylklorid.
US4001482A (en)	1977-01-04	Preparation of vinyl halide-containing polymers
US3838138A (en)	1974-09-24	Short cycle,thermally stable vinyl chloride-propylene copolymers
US4885333A (en)	1989-12-05	Polyvinyl chloride resin composition having improved thermal stability and a method for the preparation thereof
EP0177974B1 (en)	1990-09-12	A method for the preparation of a polyvinyl chloride resin
JPH06211909A (ja)	1994-08-02	塩化ビニル系重合体の製造方法およびその組成物
US3328365A (en)	1967-06-27	Acrylonitrile, vinyl chloride 1, 2-dichloroethylene terpolymer and process of preparing same
JP3663500B2 (ja)	2005-06-22	塩化ビニル系重合体の製造方法
JPH06172410A (ja)	1994-06-21	エチレン−塩化ビニル共重合体の製造方法およびその組成物
CA1178747A (en)	1984-11-27	Vinyl halide polymer of enhanced plasticizer uptake
JPS5964607A (ja)	1984-04-12	塩化ビニル樹脂の製造方法
JPH09221505A (ja)	1997-08-26	塩化ビニル系重合体の製造方法
JPH10251311A (ja)	1998-09-22	塩化ビニル系重合体の製造方法