MY179699A - Method for preparing glycol ester using reactive distillation - Google Patents
Method for preparing glycol ester using reactive distillationInfo
- Publication number
- MY179699A MY179699A MYPI2016000302A MYPI2016000302A MY179699A MY 179699 A MY179699 A MY 179699A MY PI2016000302 A MYPI2016000302 A MY PI2016000302A MY PI2016000302 A MYPI2016000302 A MY PI2016000302A MY 179699 A MY179699 A MY 179699A
- Authority
- MY
- Malaysia
- Prior art keywords
- glycol ester
- preparing
- reactive distillation
- carboxylic acid
- glycol
- Prior art date
Links
- LYCAIKOWRPUZTN-UHFFFAOYSA-N ethylene glycol Natural products OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 title abstract 6
- -1 glycol ester Chemical class 0.000 title abstract 6
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 title abstract 6
- 238000000034 method Methods 0.000 title abstract 4
- 238000000066 reactive distillation Methods 0.000 title abstract 3
- 150000001732 carboxylic acid derivatives Chemical class 0.000 abstract 3
- MTHSVFCYNBDYFN-UHFFFAOYSA-N diethylene glycol Chemical compound OCCOCCO MTHSVFCYNBDYFN-UHFFFAOYSA-N 0.000 abstract 3
- 230000003247 decreasing effect Effects 0.000 abstract 2
- 238000010533 azeotropic distillation Methods 0.000 abstract 1
- 238000006243 chemical reaction Methods 0.000 abstract 1
- 239000012535 impurity Substances 0.000 abstract 1
- 238000004519 manufacturing process Methods 0.000 abstract 1
- 238000010992 reflux Methods 0.000 abstract 1
- 238000000926 separation method Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C67/00—Preparation of carboxylic acid esters
- C07C67/48—Separation; Purification; Stabilisation; Use of additives
- C07C67/52—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation
- C07C67/54—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation by distillation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/009—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping in combination with chemical reactions
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/14—Fractional distillation or use of a fractionation or rectification column
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/24—Stationary reactors without moving elements inside
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/24—Stationary reactors without moving elements inside
- B01J19/245—Stationary reactors without moving elements inside placed in series
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C67/00—Preparation of carboxylic acid esters
- C07C67/08—Preparation of carboxylic acid esters by reacting carboxylic acids or symmetrical anhydrides with the hydroxy or O-metal group of organic compounds
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C69/00—Esters of carboxylic acids; Esters of carbonic or haloformic acids
- C07C69/66—Esters of carboxylic acids having esterified carboxylic groups bound to acyclic carbon atoms and having any of the groups OH, O—metal, —CHO, keto, ether, acyloxy, groups, groups, or in the acid moiety
- C07C69/67—Esters of carboxylic acids having esterified carboxylic groups bound to acyclic carbon atoms and having any of the groups OH, O—metal, —CHO, keto, ether, acyloxy, groups, groups, or in the acid moiety of saturated acids
- C07C69/708—Ethers
- C07C69/712—Ethers the hydroxy group of the ester being etherified with a hydroxy compound having the hydroxy group bound to a carbon atom of a six-membered aromatic ring
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00002—Chemical plants
- B01J2219/00027—Process aspects
- B01J2219/0004—Processes in series
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
- B01J2219/00718—Type of compounds synthesised
- B01J2219/0072—Organic compounds
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/10—Process efficiency
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Crystallography & Structural Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| KR1020130098551A KR101349106B1 (ko) | 2013-08-20 | 2013-08-20 | 반응증류를 이용한 글리콜 에스테르의 제조방법 |
| PCT/KR2014/006912 WO2015026073A1 (fr) | 2013-08-20 | 2014-07-29 | Procédé de préparation d'ester de glycol par distillation réactive |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| MY179699A true MY179699A (en) | 2020-11-11 |
Family
ID=50144953
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| MYPI2016000302A MY179699A (en) | 2013-08-20 | 2014-07-29 | Method for preparing glycol ester using reactive distillation |
Country Status (5)
| Country | Link |
|---|---|
| KR (1) | KR101349106B1 (fr) |
| CN (1) | CN104640836B (fr) |
| MY (1) | MY179699A (fr) |
| TW (1) | TWI579266B (fr) |
| WO (1) | WO2015026073A1 (fr) |
Families Citing this family (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105693514B (zh) * | 2016-03-18 | 2018-05-15 | 江苏雷蒙化工科技有限公司 | 一种多元醇的低碳羧酸酯的连续化生产系统及其生产方法 |
| CN109456190A (zh) * | 2018-10-18 | 2019-03-12 | 天津大学 | 一种低温高选择性催化精馏连续合成丙二醇甲醚醋酸酯的方法 |
| CN110305012A (zh) * | 2019-08-16 | 2019-10-08 | 南通百川新材料有限公司 | 一种半导体级丙二醇甲醚乙酸酯的合成工艺 |
| CN110423197B (zh) * | 2019-09-17 | 2023-11-14 | 凯瑞环保科技股份有限公司 | 一种利用低浓度乙二醇生产乙二醇双乙酸酯的装置和方法 |
| US20230024745A1 (en) * | 2019-12-16 | 2023-01-26 | Eastman Chemical Company | Esterification of acetic acid recovered from wood acetylation with ether-alcohols |
| WO2021172898A1 (fr) * | 2020-02-26 | 2021-09-02 | 영남대학교 산학협력단 | Appareil et procédé de production d'acétate de propylèneglycolméthyléther |
| US12522558B2 (en) * | 2020-04-22 | 2026-01-13 | Dsm Ip Assets B.V. | Process for the acylation of an alpha, omega-alkanediol |
| CN112194580B (zh) * | 2020-11-04 | 2021-09-14 | 中建安装集团有限公司 | 一种反应精馏耦合渗透汽化生产丙二醇单甲醚醋酸酯的装置及工艺 |
| KR102399263B1 (ko) * | 2021-08-09 | 2022-05-17 | 에스케이머티리얼즈퍼포먼스 주식회사 | 프로필렌 글리콜 모노메틸 에테르 아세테이트의 제조방법 |
| KR102498772B1 (ko) * | 2021-11-29 | 2023-02-10 | 주식회사 켐트로닉스 | 초고순도 pgmea의 제조방법 |
| CN115745797A (zh) * | 2022-12-03 | 2023-03-07 | 福州大学 | 一种连续反应精馏酯化合成丙二醇单甲醚醋酸酯及副产1,2-二乙酰氧基丙烷的工艺 |
| WO2025143078A1 (fr) * | 2023-12-27 | 2025-07-03 | Khネオケム株式会社 | Composition d'acétate d'éther monométhylique de propylène glycol |
| CN120569362B (zh) * | 2023-12-27 | 2026-02-03 | Kh新化株式会社 | 丙二醇单甲醚乙酸酯组合物 |
Family Cites Families (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2466448A1 (fr) | 1979-10-01 | 1981-04-10 | Propylox Sa | Procede pour la recuperation d'acides carboxyliques a partir de melanges contenant des esters de glycols derives de ces acides |
| US5202463A (en) | 1991-09-10 | 1993-04-13 | Arco Chemical Technology, L.P. | Process for the preparation of a glycol ether ester |
| FR2757156B1 (fr) * | 1996-12-17 | 1999-01-22 | Bp Chemicals Snc | Procede de fabrication en continu d'esters |
| KR100286571B1 (ko) * | 1999-03-11 | 2001-03-15 | 남창우 | 반응증류를 이용한 글리콜 에스테르의 제조방법 |
| JP3763076B2 (ja) * | 2002-12-03 | 2006-04-05 | 株式会社日本触媒 | α−ヒドロキシカルボン酸エステルの製造法 |
| TWI262186B (en) * | 2002-10-09 | 2006-09-21 | Nippon Catalytic Chem Ind | Method for producing alpha-hydroxycarboxylic ester |
| KR100779521B1 (ko) | 2005-07-15 | 2007-11-28 | 주식회사 엘지화학 | 카르복실산 및 에스테르 화합물의 병산 방법 |
-
2013
- 2013-08-20 KR KR1020130098551A patent/KR101349106B1/ko active Active
-
2014
- 2014-07-29 MY MYPI2016000302A patent/MY179699A/en unknown
- 2014-07-29 CN CN201480000762.XA patent/CN104640836B/zh active Active
- 2014-07-29 WO PCT/KR2014/006912 patent/WO2015026073A1/fr not_active Ceased
- 2014-08-20 TW TW103128606A patent/TWI579266B/zh active
Also Published As
| Publication number | Publication date |
|---|---|
| WO2015026073A1 (fr) | 2015-02-26 |
| CN104640836B (zh) | 2016-11-23 |
| TWI579266B (zh) | 2017-04-21 |
| KR101349106B1 (ko) | 2014-01-08 |
| TW201507997A (zh) | 2015-03-01 |
| CN104640836A (zh) | 2015-05-20 |
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