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MX2023000044A - Nuevos procesos e intermediarios para la preparacion de estimulantes de guanilato ciclasa soluble. - Google Patents

Nuevos procesos e intermediarios para la preparacion de estimulantes de guanilato ciclasa soluble.

Info

Publication number
MX2023000044A
MX2023000044A MX2023000044A MX2023000044A MX2023000044A MX 2023000044 A MX2023000044 A MX 2023000044A MX 2023000044 A MX2023000044 A MX 2023000044A MX 2023000044 A MX2023000044 A MX 2023000044A MX 2023000044 A MX2023000044 A MX 2023000044A
Authority
MX
Mexico
Prior art keywords
preparation
guanylate cyclase
soluble guanylate
intermediaries
compounds
Prior art date
Application number
MX2023000044A
Other languages
English (en)
Inventor
Takashi Nakai
Ahmad Hashash
Song Xue
Vishnu Vardhan Reddy Karnati
Wayne C Schairer
Debra Jane Wallace
Fenger Zhou
Yuguang Wang
William Kissel
Original Assignee
Cyclerion Therapeutics Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from PCT/CN2018/076982 external-priority patent/WO2019161534A1/en
Application filed by Cyclerion Therapeutics Inc filed Critical Cyclerion Therapeutics Inc
Publication of MX2023000044A publication Critical patent/MX2023000044A/es

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Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D413/00Heterocyclic compounds containing two or more hetero rings, at least one ring having nitrogen and oxygen atoms as the only ring hetero atoms
    • C07D413/14Heterocyclic compounds containing two or more hetero rings, at least one ring having nitrogen and oxygen atoms as the only ring hetero atoms containing three or more hetero rings
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C237/00Carboxylic acid amides, the carbon skeleton of the acid part being further substituted by amino groups
    • C07C237/02Carboxylic acid amides, the carbon skeleton of the acid part being further substituted by amino groups having the carbon atoms of the carboxamide groups bound to acyclic carbon atoms of the carbon skeleton
    • C07C237/04Carboxylic acid amides, the carbon skeleton of the acid part being further substituted by amino groups having the carbon atoms of the carboxamide groups bound to acyclic carbon atoms of the carbon skeleton the carbon skeleton being acyclic and saturated
    • C07C237/06Carboxylic acid amides, the carbon skeleton of the acid part being further substituted by amino groups having the carbon atoms of the carboxamide groups bound to acyclic carbon atoms of the carbon skeleton the carbon skeleton being acyclic and saturated having the nitrogen atoms of the carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C237/00Carboxylic acid amides, the carbon skeleton of the acid part being further substituted by amino groups
    • C07C237/02Carboxylic acid amides, the carbon skeleton of the acid part being further substituted by amino groups having the carbon atoms of the carboxamide groups bound to acyclic carbon atoms of the carbon skeleton
    • C07C237/04Carboxylic acid amides, the carbon skeleton of the acid part being further substituted by amino groups having the carbon atoms of the carboxamide groups bound to acyclic carbon atoms of the carbon skeleton the carbon skeleton being acyclic and saturated
    • C07C237/08Carboxylic acid amides, the carbon skeleton of the acid part being further substituted by amino groups having the carbon atoms of the carboxamide groups bound to acyclic carbon atoms of the carbon skeleton the carbon skeleton being acyclic and saturated having the nitrogen atom of at least one of the carboxamide groups bound to an acyclic carbon atom of a hydrocarbon radical substituted by singly-bound oxygen atoms
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C59/00Compounds having carboxyl groups bound to acyclic carbon atoms and containing any of the groups OH, O—metal, —CHO, keto, ether, groups, groups, or groups
    • C07C59/235Saturated compounds containing more than one carboxyl group
    • C07C59/245Saturated compounds containing more than one carboxyl group containing hydroxy or O-metal groups
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D403/00Heterocyclic compounds containing two or more hetero rings, having nitrogen atoms as the only ring hetero atoms, not provided for by group C07D401/00
    • C07D403/02Heterocyclic compounds containing two or more hetero rings, having nitrogen atoms as the only ring hetero atoms, not provided for by group C07D401/00 containing two hetero rings
    • C07D403/04Heterocyclic compounds containing two or more hetero rings, having nitrogen atoms as the only ring hetero atoms, not provided for by group C07D401/00 containing two hetero rings directly linked by a ring-member-to-ring-member bond
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D413/00Heterocyclic compounds containing two or more hetero rings, at least one ring having nitrogen and oxygen atoms as the only ring hetero atoms
    • C07D413/02Heterocyclic compounds containing two or more hetero rings, at least one ring having nitrogen and oxygen atoms as the only ring hetero atoms containing two hetero rings
    • C07D413/12Heterocyclic compounds containing two or more hetero rings, at least one ring having nitrogen and oxygen atoms as the only ring hetero atoms containing two hetero rings linked by a chain containing hetero atoms as chain links
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K31/00Medicinal preparations containing organic active ingredients
    • A61K31/33Heterocyclic compounds
    • A61K31/395Heterocyclic compounds having nitrogen as a ring hetero atom, e.g. guanethidine or rifamycins
    • A61K31/495Heterocyclic compounds having nitrogen as a ring hetero atom, e.g. guanethidine or rifamycins having six-membered rings with two or more nitrogen atoms as the only ring heteroatoms, e.g. piperazine or tetrazines
    • A61K31/505Pyrimidines; Hydrogenated pyrimidines, e.g. trimethoprim
    • A61K31/506Pyrimidines; Hydrogenated pyrimidines, e.g. trimethoprim not condensed and containing further heterocyclic rings
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07BGENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
    • C07B2200/00Indexing scheme relating to specific properties of organic compounds
    • C07B2200/13Crystalline forms, e.g. polymorphs

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
  • Plural Heterocyclic Compounds (AREA)
  • Health & Medical Sciences (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Medicinal Chemistry (AREA)
  • Acyclic And Carbocyclic Compounds In Medicinal Compositions (AREA)
  • Pharmacology & Pharmacy (AREA)
  • Epidemiology (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Nitrogen Condensed Heterocyclic Rings (AREA)
  • Preparation Of Compounds By Using Micro-Organisms (AREA)

Abstract

Procesos nuevos para la preparación de compuestos de Fórmula I. Algunos de estos compuestos son de utilidad como estimulantes de la guanilato ciclasa soluble (sGC). Otros son intermediarios para usar en la preparación de los estimulantes. Estos procesos son adecuados para preparaciones a gran escala y producen 3-(2-pirimidinil)pirazoles de la Fórmula I estables, de gran pureza y rendimientos elevados. La invención ofrece la ventaja adicional de comprender condiciones de reacción sencillas, adecuadas para aumentar la escala en una producción a gran escala. También se proveen nuevos intermediarios para usar en la preparación de los compuestos. (ver Fórmula).
MX2023000044A 2018-01-10 2020-07-13 Nuevos procesos e intermediarios para la preparacion de estimulantes de guanilato ciclasa soluble. MX2023000044A (es)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US201862615678P 2018-01-10 2018-01-10
PCT/CN2018/076982 WO2019161534A1 (en) 2018-02-22 2018-02-22 Novel processes and intermediates for preparation of soluble guanylate cyclase stimulators

Publications (1)

Publication Number Publication Date
MX2023000044A true MX2023000044A (es) 2023-02-01

Family

ID=65279655

Family Applications (3)

Application Number Title Priority Date Filing Date
MX2020007364A MX2020007364A (es) 2018-01-10 2019-01-10 Nuevos procesos e intermediarios para la preparación de estimulantes de guanilato ciclasa soluble.
MX2023000045A MX2023000045A (es) 2018-01-10 2020-07-13 Nuevos procesos e intermediarios para la preparacion de estimulantes de guanilato ciclasa soluble.
MX2023000044A MX2023000044A (es) 2018-01-10 2020-07-13 Nuevos procesos e intermediarios para la preparacion de estimulantes de guanilato ciclasa soluble.

Family Applications Before (2)

Application Number Title Priority Date Filing Date
MX2020007364A MX2020007364A (es) 2018-01-10 2019-01-10 Nuevos procesos e intermediarios para la preparación de estimulantes de guanilato ciclasa soluble.
MX2023000045A MX2023000045A (es) 2018-01-10 2020-07-13 Nuevos procesos e intermediarios para la preparacion de estimulantes de guanilato ciclasa soluble.

Country Status (17)

Country Link
US (5) US11274096B2 (es)
EP (3) EP4570797A3 (es)
JP (2) JP7357621B2 (es)
KR (3) KR102739727B1 (es)
CN (3) CN111902410B (es)
AU (2) AU2019206560B2 (es)
BR (1) BR112020013985A2 (es)
CA (1) CA3087943A1 (es)
CL (3) CL2020001814A1 (es)
ES (1) ES2963447T3 (es)
IL (3) IL314714A (es)
JO (1) JOP20200165A1 (es)
MA (2) MA71753A (es)
MX (3) MX2020007364A (es)
SG (1) SG11202006311SA (es)
TW (2) TWI888947B (es)
WO (1) WO2019140095A1 (es)

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
MA45603A (fr) * 2016-07-07 2019-05-15 Ironwood Pharmaceuticals Inc Nouveaux procédés de préparation de stimulateurs de la guanylate cyclase soluble
JOP20200165A1 (ar) 2018-01-10 2022-10-30 Cyclerion Therapeutics Inc عمليات ووسائط جديدة لتحضير محفزات إنزيم حلقي جوانيلات قابلة للذوبان
WO2024131850A1 (zh) * 2022-12-21 2024-06-27 广东东阳光药业股份有限公司 氟取代的吲唑化合物的晶型及其用途
EP4640677A1 (en) * 2022-12-21 2025-10-29 Sunshine Lake Pharma Co., Ltd. Crystal form of fluorine-substituted indazole compound and use thereof

Family Cites Families (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107021951B (zh) * 2010-06-30 2020-10-20 赛克里翁治疗有限公司 sGC刺激物
CN109369635B (zh) * 2013-03-15 2023-06-30 赛克里翁治疗有限公司 化合物或其药学上可接受的盐及其应用和药物组合物
WO2015106268A1 (en) * 2014-01-13 2015-07-16 Ironwood Pharmaceuticals, Inc. USE OF sGC STIMULATORS FOR THE TREATMENT OF NEUROMUSCULAR DISORDERS
EP3194382B1 (en) * 2014-09-17 2021-09-08 Cyclerion Therapeutics, Inc. Pyrazole derivatives as sgc stimulators
KR20170055531A (ko) * 2014-09-17 2017-05-19 아이언우드 파마슈티컬스, 인코포레이티드 에스지씨 자극제
CN116637076A (zh) * 2015-11-30 2023-08-25 赛克里翁治疗有限公司 包含sGC刺激剂的固体分散体
SG11201900125PA (en) 2016-07-07 2019-02-27 Ironwood Pharmaceuticals Inc Novel processes for preparation of soluble guanylate cyclase stimulators
MA45603A (fr) 2016-07-07 2019-05-15 Ironwood Pharmaceuticals Inc Nouveaux procédés de préparation de stimulateurs de la guanylate cyclase soluble
JOP20200165A1 (ar) 2018-01-10 2022-10-30 Cyclerion Therapeutics Inc عمليات ووسائط جديدة لتحضير محفزات إنزيم حلقي جوانيلات قابلة للذوبان

Also Published As

Publication number Publication date
AU2019206560A1 (en) 2020-07-30
MA51565A (fr) 2020-11-18
TWI821237B (zh) 2023-11-11
TW202402741A (zh) 2024-01-16
CN111902410B (zh) 2024-04-19
ES2963447T3 (es) 2024-03-27
AU2019206560B2 (en) 2023-08-24
IL319883A (en) 2025-05-01
US20250361228A1 (en) 2025-11-27
CL2022000907A1 (es) 2022-10-21
JOP20200165A1 (ar) 2022-10-30
WO2019140095A8 (en) 2020-06-18
WO2019140095A1 (en) 2019-07-18
EP4570797A2 (en) 2025-06-18
US11274096B2 (en) 2022-03-15
US20230339928A1 (en) 2023-10-26
IL314714A (en) 2024-10-01
JP2023182647A (ja) 2023-12-26
CA3087943A1 (en) 2019-07-18
CL2020001814A1 (es) 2020-11-06
TWI888947B (zh) 2025-07-01
EP3737679B1 (en) 2023-09-06
BR112020013985A2 (pt) 2020-12-01
US20220024909A1 (en) 2022-01-27
JP7744955B2 (ja) 2025-09-26
IL275748B1 (en) 2024-09-01
MA71753A (fr) 2025-05-30
CN118221665A (zh) 2024-06-21
CL2022000904A1 (es) 2022-10-21
TW201932450A (zh) 2019-08-16
US12275724B2 (en) 2025-04-15
MX2020007364A (es) 2020-11-18
AU2025202281A1 (en) 2025-04-17
EP3737679A1 (en) 2020-11-18
CN118184645A (zh) 2024-06-14
US20210053962A1 (en) 2021-02-25
JP7357621B2 (ja) 2023-10-06
JP2021511299A (ja) 2021-05-06
AU2025202281A9 (en) 2025-05-15
KR20250002720A (ko) 2025-01-07
US12030874B2 (en) 2024-07-09
IL275748A (en) 2020-08-31
SG11202006311SA (en) 2020-07-29
CN111902410A (zh) 2020-11-06
MX2023000045A (es) 2023-02-01
EP4249469A2 (en) 2023-09-27
EP3737679C0 (en) 2023-09-06
KR20250048609A (ko) 2025-04-09
AU2023270260A1 (en) 2023-12-07
KR20200106920A (ko) 2020-09-15
US11708361B2 (en) 2023-07-25
EP4570797A3 (en) 2025-09-03
KR102739727B1 (ko) 2024-12-05
EP4249469A3 (en) 2023-12-27
IL275748B2 (en) 2025-01-01
US20240391911A1 (en) 2024-11-28

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