MX2022015387A - Produccion y purificacion de acido acetico. - Google Patents
Produccion y purificacion de acido acetico.Info
- Publication number
- MX2022015387A MX2022015387A MX2022015387A MX2022015387A MX2022015387A MX 2022015387 A MX2022015387 A MX 2022015387A MX 2022015387 A MX2022015387 A MX 2022015387A MX 2022015387 A MX2022015387 A MX 2022015387A MX 2022015387 A MX2022015387 A MX 2022015387A
- Authority
- MX
- Mexico
- Prior art keywords
- acetic acid
- production
- purification
- carbonylation
- dimethoxyethane
- Prior art date
Links
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 title abstract 12
- 238000004519 manufacturing process Methods 0.000 title abstract 3
- 238000000746 purification Methods 0.000 title abstract 3
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 abstract 3
- SPEUIVXLLWOEMJ-UHFFFAOYSA-N 1,1-dimethoxyethane Chemical compound COC(C)OC SPEUIVXLLWOEMJ-UHFFFAOYSA-N 0.000 abstract 2
- 230000006315 carbonylation Effects 0.000 abstract 2
- 238000005810 carbonylation reaction Methods 0.000 abstract 2
- 238000000034 method Methods 0.000 abstract 2
- DHKHKXVYLBGOIT-UHFFFAOYSA-N acetaldehyde Diethyl Acetal Natural products CCOC(C)OCC DHKHKXVYLBGOIT-UHFFFAOYSA-N 0.000 abstract 1
- 150000001241 acetals Chemical group 0.000 abstract 1
- 230000015572 biosynthetic process Effects 0.000 abstract 1
- 239000003054 catalyst Substances 0.000 abstract 1
- 239000012535 impurity Substances 0.000 abstract 1
- 239000002184 metal Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/10—Preparation of carboxylic acids or their salts, halides or anhydrides by reaction with carbon monoxide
- C07C51/12—Preparation of carboxylic acids or their salts, halides or anhydrides by reaction with carbon monoxide on an oxygen-containing group in organic compounds, e.g. alcohols
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/42—Separation; Purification; Stabilisation; Use of additives
- C07C51/43—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
- C07C51/44—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation by distillation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/42—Separation; Purification; Stabilisation; Use of additives
- C07C51/47—Separation; Purification; Stabilisation; Use of additives by solid-liquid treatment; by chemisorption
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C53/00—Saturated compounds having only one carboxyl group bound to an acyclic carbon atom or hydrogen
- C07C53/08—Acetic acid
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Crystallography & Structural Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
En el presente documento se proporciona un proceso para la producción y purificación de ácido acético. En particular, la presente divulgación se refiere a procesos mejorados para producir y purificar ácido acético mediante la carbonilación de metanol en presencia de un catalizador de carbonilación metálico del Grupo VIII. El proceso de producción y purificación de ácido acético descrito en el presente documento controla la formación y la composición en masa de las impurezas de acetal, tales como 1,1-dimetoxietano.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US202063034078P | 2020-06-03 | 2020-06-03 | |
| PCT/US2021/035688 WO2021247854A1 (en) | 2020-06-03 | 2021-06-03 | Production and purification of acetic acid |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| MX2022015387A true MX2022015387A (es) | 2023-01-16 |
Family
ID=76695845
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| MX2022015387A MX2022015387A (es) | 2020-06-03 | 2021-06-03 | Produccion y purificacion de acido acetico. |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US20230202957A1 (es) |
| EP (1) | EP4161894A1 (es) |
| JP (1) | JP2023528451A (es) |
| KR (1) | KR20230019134A (es) |
| CN (1) | CN115916735B (es) |
| MX (1) | MX2022015387A (es) |
| SA (1) | SA522441550B1 (es) |
| WO (1) | WO2021247854A1 (es) |
Family Cites Families (34)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5001259A (en) | 1984-05-03 | 1991-03-19 | Hoechst Celanese Corporation | Methanol carbonylation process |
| US5144068A (en) | 1984-05-03 | 1992-09-01 | Hoechst Celanese Corporation | Methanol carbonylation process |
| US5026908A (en) | 1984-05-03 | 1991-06-25 | Hoechst Celanese Corporation | Methanol carbonylation process |
| US4615806B1 (en) | 1985-03-07 | 1994-05-03 | Hoechst Co American | Removal of iodide compounds from non-aqueous organic media |
| CN1043525C (zh) | 1992-08-13 | 1999-06-02 | 化学工业部西南化工研究院 | 甲醇低压液相羰基合成醋酸反应方法 |
| US5672743A (en) | 1993-09-10 | 1997-09-30 | Bp Chemicals Limited | Process for the production of acetic acid |
| JP3377555B2 (ja) | 1993-05-31 | 2003-02-17 | ダイセル化学工業株式会社 | カルボニル化反応生成物に含有されるヨウ素化合物の除去方法 |
| US5374774A (en) | 1994-03-11 | 1994-12-20 | Hoechst Celanese Corporation | Control system for an acetic acid manufacturing process |
| JP3308392B2 (ja) | 1994-06-02 | 2002-07-29 | ダイセル化学工業株式会社 | カルボニル化反応方法 |
| JP3581725B2 (ja) * | 1994-06-30 | 2004-10-27 | ダイセル化学工業株式会社 | アセトアルデヒドとヨウ化メチルの分離方法 |
| US5696284A (en) | 1995-06-21 | 1997-12-09 | Bp Chemicals Limited | Process for the carbonylation of alkyl alcohols and/or reactive derivatives thereof |
| NZ321758A (en) | 1995-10-27 | 1999-05-28 | Hoechst Celanese Corp | Process for purifying a rhodium containing catalyst solution |
| GB9625335D0 (en) | 1996-12-05 | 1997-01-22 | Bp Chem Int Ltd | Process |
| GB9626429D0 (en) | 1996-12-19 | 1997-02-05 | Bp Chem Int Ltd | Process |
| GB9626428D0 (en) | 1996-12-19 | 1997-02-05 | Bp Chem Int Ltd | Process |
| GB9626317D0 (en) | 1996-12-19 | 1997-02-05 | Bp Chem Int Ltd | Process |
| US6225498B1 (en) | 2000-03-24 | 2001-05-01 | Celanese International Corporation | Method of removing organic iodides from organic media |
| US6677480B2 (en) | 2002-01-28 | 2004-01-13 | Celanese International Corporation | Process control in production of acetic acid via use of heavy phase density measurement |
| US7005541B2 (en) | 2002-12-23 | 2006-02-28 | Celanese International Corporation | Low water methanol carbonylation process for high acetic acid production and for water balance control |
| US7902398B2 (en) | 2007-04-25 | 2011-03-08 | Celanese International Corporation | Method and apparatus for carbonylation with reduced catalyst loss |
| US8017802B2 (en) | 2007-05-21 | 2011-09-13 | Celanese International Corporation | Control of impurities in reaction product of rhodium-catalyzed methanol carbonylation |
| US7390919B1 (en) * | 2007-10-01 | 2008-06-24 | Lyondell Chemical Technology, L.P. | Methyl acetate purification and carbonylation |
| US8062482B2 (en) * | 2007-10-30 | 2011-11-22 | Celanese International Corporation | Acetaldehyde removal from methyl acetate by distillation at elevated pressure |
| KR101584387B1 (ko) | 2008-04-29 | 2016-01-13 | 셀라니즈 인터내셔날 코포레이션 | 다수의 용매 옵션을 가진 흡수 장치를 갖는 메탄올 카보닐화 시스템 |
| US7884237B2 (en) * | 2008-11-07 | 2011-02-08 | Celanese International Corp. | Methanol carbonylation with improved aldehyde removal |
| US8076512B2 (en) * | 2009-08-27 | 2011-12-13 | Equistar Chemicals, L.P. | Preparation of acetic acid |
| ES2645007T3 (es) | 2010-07-26 | 2017-12-01 | Daicel Corporation | Procedimiento para la producción de ácido acético |
| US8530696B2 (en) | 2010-09-24 | 2013-09-10 | Celanese International Corporation | Pump around reactor for production of acetic acid |
| US8697908B2 (en) | 2011-05-05 | 2014-04-15 | Celanese International Corporation | Removal of amine compounds from carbonylation process stream containing corrosion metal contaminants |
| WO2013070212A1 (en) * | 2011-11-09 | 2013-05-16 | Celanese International Corporation | Producing ethanol using two different streams from acetic acid carbonylation process |
| US8859810B2 (en) * | 2012-08-21 | 2014-10-14 | Celanese International Corporation | Process for recovering permanganate reducing compounds from an acetic acid production process |
| KR102467611B1 (ko) * | 2014-11-14 | 2022-11-16 | 셀라니즈 인터내셔날 코포레이션 | 낮은 요오드화에틸 함량을 갖는 반응 매질로부터 아세트산을 제조하기 위한 방법 |
| WO2016194850A1 (ja) * | 2015-06-01 | 2016-12-08 | 株式会社ダイセル | 酢酸の製造方法 |
| US10807935B2 (en) * | 2018-11-02 | 2020-10-20 | Celanese International Corporation | Process for continuous acetic acid production |
-
2021
- 2021-06-03 KR KR1020227045633A patent/KR20230019134A/ko active Pending
- 2021-06-03 EP EP21736101.3A patent/EP4161894A1/en active Pending
- 2021-06-03 CN CN202180040032.2A patent/CN115916735B/zh active Active
- 2021-06-03 US US17/928,567 patent/US20230202957A1/en active Pending
- 2021-06-03 MX MX2022015387A patent/MX2022015387A/es unknown
- 2021-06-03 WO PCT/US2021/035688 patent/WO2021247854A1/en not_active Ceased
- 2021-06-03 JP JP2022574391A patent/JP2023528451A/ja not_active Ceased
-
2022
- 2022-11-30 SA SA522441550A patent/SA522441550B1/ar unknown
Also Published As
| Publication number | Publication date |
|---|---|
| WO2021247854A1 (en) | 2021-12-09 |
| JP2023528451A (ja) | 2023-07-04 |
| SA522441550B1 (ar) | 2025-06-29 |
| CN115916735B (zh) | 2025-03-25 |
| CN115916735A (zh) | 2023-04-04 |
| TW202208315A (zh) | 2022-03-01 |
| KR20230019134A (ko) | 2023-02-07 |
| EP4161894A1 (en) | 2023-04-12 |
| US20230202957A1 (en) | 2023-06-29 |
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